Certificate of Analysis
REGULATORY COMPLIANCE

Sample Name:

R&R Sleep Softgel 45mg CBD / 5mg CBN (per serv) Full-Spectrum Softgel

Infused, Product Inhalable

Date Issued:

09/26/2024

Serving Size:

1.634 grams

Total THC 1.296 mg/unit
Total CBD 45.311 mg/unit
Sum Cannabinoids 54.393 mg/unit
Total Cannabinoids 54.306 mg/unit
Total Terpenoids 0.0217%
Top 3 Terpenoids
  1. Guaiol 0.0086%
  2. α-Bisabolol 0.0074%
  3. β-Caryophyllene 0.0057%

Sample Information

Sample Details

Sample ID:240912M022

Batch Number:9200S

Cultivator / Manufacturer

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Distributor

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Cannabinoid Analysis - Summary

Total THC: 1.296 mg/unit

Total CBD: 45.311 mg/unit

Sum of Cannabinoids: 54.393 mg/unit

Total Cannabinoids: 54.306 mg/unit

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

Total Terpenoids: 0.0217%

 
 
 

1

Guaiol (0.0086%)

2

α-Bisabolol (0.0074%)

3

β-Caryophyllene (0.0057%)

Safety Analysis - Summary

Pesticides: Pass

Mycotoxins: Pass

Residual Solvents: Pass

Heavy Metals: Pass

Microbiology: Pass

Foreign Material: NT

Water Activity: NT

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 1.296 mg/unit

(Δ9-THC+0.877*THCa)

Total CBD: 45.311 mg/unit

(CBD+0.877*CBDa)

Total Cannabinoids: 54.306 mg/unit

Total CBG: 0.706 mg/unit

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 1.902 mg/unit

Total CBC (CBC+0.877*CBCa)

Total CBDV: 0.430 mg/unit

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

09/16/2024

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
Cannabidiol (CBD) 0.004 / 0.011 ±1.0211 27.375 2.7375
Cannabinol (CBN) 0.001 / 0.007 ±0.0806 2.810 0.2810
Cannabichromene (CBC) 0.003 / 0.010 ±0.0369 1.145 0.1145
Δ9 Tetrahydrocannabinol (Δ9THC) 0.002 / 0.014 ±0.0435 0.793 0.0793
Cannabigerol (CBG) 0.002 / 0.006 ±0.0210 0.432 0.0432
Cannabidiolic Acid (CBDa) 0.001 / 0.026 ±0.0115 0.405 0.0405
Cannabidivarin (CBDV) 0.002 / 0.012 ±0.0107 0.263 0.0263
Cannabicyclol (CBL) 0.003 / 0.010 ±0.0016 0.043 0.0043
Cannabichromenic Acid (CBCa) 0.001 / 0.015 ±0.0008 0.022 0.0022
Cannabigerolic Acid (CBGa) 0.002 / 0.007 N/A ND ND
Tetrahydrocannabivarin (THCV) 0.002 / 0.012 N/A ND ND
Tetrahydrocannabinolic Acid (THCa) 0.001 / 0.005 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.001 / 0.018 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.002 / 0.019 N/A ND ND
∆8 Tetrahydrocannabinol (Δ8THC) 0.01 / 0.02 N/A ND ND
SUM OF CANNABINOIDS 33.288 mg/g 3.3288%
Unit Mass:

1.634 grams

/

Serving Size:

1.634 grams

Swipe left on table to see additional columns

Δ9-THC per Unit 1.296 mg/unit
Δ9-THC per Serving 1.296 mg/serving
Total THC per Unit 1.296 mg/unit
Total THC Per Serving 1.296 mg/serving
CBD per Unit 44.731 mg/unit
CBD per Serving 44.731 mg/serving
Total CBD per Unit 45.311 mg/unit
Total CBD per Serving 45.311 mg/serving
Sum of Cannabinoids per Unit 54.393 mg/unit
Sum of Cannabinoids per Serving 54.393 mg/serving
Total Cannabinoids per Unit 54.306 mg/unit
Total Cannabinoids per Serving 54.306 mg/serving
Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

Summary

Total Terpenoids (mg/g): 0.217 mg/g

Total Terpenoids (%): 0.0217%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume.

  1. Guaiol 0.0086%

    A sesquiterpene alcohol with a fragrance that can be described as floral, piney, herbal and woody. Found in guaiacum, cypress pine, ginseng, melaleuca, goatweed, incense grass...etc.

  2. α-Bisabolol 0.0074%

    A sesquiterpene alcohol with a fragrance that can be described as floral, peppery, sweet and clean. Found in chamomile, figwort, yarrow, skullcaps, lavender, ironwort, germander...etc.

  3. β-Caryophyllene 0.0057%

    A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB2 receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

09/17/2024

Result Views

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Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
Guaiol 0.009 / 0.030 ±0.0032 0.086 0.0086
α-Bisabolol 0.008 / 0.026 ±0.0031 0.074 0.0074
β-Caryophyllene 0.004 / 0.012 ±0.0016 0.057 0.0057
α-Humulene 0.009 / 0.180 N/A <LOQ <LOQ
Nerol 0.003 / 0.036 N/A ND ND
Cedrol 0.008 / 0.027 N/A ND ND
Borneol 0.005 / 0.016 N/A ND ND
Camphor 0.006 / 0.036 N/A ND ND
Fenchol 0.010 / 0.036 N/A ND ND
Menthol 0.008 / 0.025 N/A ND ND
Myrcene 0.008 / 0.025 N/A ND ND
Camphene 0.005 / 0.015 N/A ND ND
Fenchone 0.009 / 0.036 N/A ND ND
Geraniol 0.002 / 0.036 N/A ND ND
Limonene 0.005 / 0.036 N/A ND ND
Linalool 0.009 / 0.036 N/A ND ND
Pulegone 0.003 / 0.011 N/A ND ND
Sabinene 0.004 / 0.014 N/A ND ND
p-Cymene 0.005 / 0.016 N/A ND ND
Nerolidol 0.006 / 0.021 N/A ND ND
Terpineol 0.009 / 0.031 N/A ND ND
Valencene 0.009 / 0.180 N/A ND ND
Eucalyptol 0.006 / 0.018 N/A ND ND
Isoborneol 0.004 / 0.012 N/A ND ND
Isopulegol 0.005 / 0.036 N/A ND ND
Citronellol 0.003 / 0.036 N/A ND ND
Terpinolene 0.008 / 0.036 N/A ND ND
β-Pinene 0.004 / 0.014 N/A ND ND
α-Pinene 0.005 / 0.036 N/A ND ND
β-Ocimene 0.006 / 0.025 N/A ND ND
Δ3-Carene 0.005 / 0.018 N/A ND ND
α-Cedrene 0.005 / 0.016 N/A ND ND
Geranyl Acetate 0.004 / 0.036 N/A ND ND
α-Terpinene 0.005 / 0.017 N/A ND ND
γ-Terpinene 0.006 / 0.018 N/A ND ND
Sabinene Hydrate 0.006 / 0.036 N/A ND ND
α-Phellandrene 0.006 / 0.036 N/A ND ND
Caryophyllene Oxide 0.010 / 0.033 N/A ND ND
trans-β-Farnesene 0.008 / 0.025 N/A ND ND
TOTAL 0.217 mg/g 0.0217%
Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

09/16/2024

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Abamectin 0.032 / 0.097 0.1 N/A ND Pass
Acephate 0.006 / 0.018 0.1 N/A ND Pass
Acequinocyl 0.009 / 0.027 0.1 N/A ND Pass
Acetamiprid 0.016 / 0.049 0.1 N/A ND Pass
Aldicarb 0.030 / 0.090 ≥ LOD N/A ND Pass
Allethrin 0.030 / 0.092 N/A ND
Atrazine 0.006 / 0.019 N/A ND
Azadirachtin 0.082 / 0.248 N/A ND
Azoxystrobin 0.003 / 0.009 0.1 N/A ND Pass
Benzovindiflupyr 0.003 / 0.009 N/A ND
Bifenazate 0.003 / 0.009 0.1 N/A ND Pass
Bifenthrin 0.021 / 0.064 3 N/A ND Pass
Boscalid 0.003 / 0.009 0.1 N/A ND Pass
Buprofezin‡ 0.006 / 0.019 N/A ND
Carbaryl 0.007 / 0.020 0.5 N/A ND Pass
Carbofuran 0.003 / 0.008 ≥ LOD N/A ND Pass
Chlorantraniliprole 0.006 / 0.018 10 N/A ND Pass
Chlorfenapyr* 0.005 / 0.015 ≥ LOD N/A ND Pass
Chlorpyrifos 0.013 / 0.039 ≥ LOD N/A ND Pass
cis-Permethrin ± 0.00
Clofentezine 0.003 / 0.009 0.1 N/A ND Pass
Clothianidin 0.008 / 0.025 N/A ND
Coumaphos 0.003 / 0.010 ≥ LOD N/A ND Pass
Cyantraniliprole 0.003 / 0.010 N/A ND
Cyfluthrin 0.052 / 0.159 2 N/A ND Pass
Cypermethrin 0.051 / 0.153 1 N/A ND Pass
Cyprodinil‡ 0.003 / 0.008 N/A ND
Daminozide 0.026 / 0.077 ≥ LOD N/A ND Pass
Deltamethrin 0.059 / 0.180 N/A ND
Diazinon 0.006 / 0.017 0.1 N/A ND Pass
Dichlorvos (DDVP) 0.012 / 0.038 ≥ LOD N/A ND Pass
Dimethoate 0.003 / 0.009 ≥ LOD N/A ND Pass
Dimethomorph 0.016 / 0.050 2 N/A ND Pass
Dinotefuran 0.010 / 0.030 N/A ND
Diuron 0.013 / 0.040 N/A ND
Dodemorph 0.012 / 0.035 N/A ND
Endosulfan sulfate†‡ 0.016 / 0.048 N/A ND
Endosulfan-α*†‡ 0.004 / 0.014 N/A ND
Endosulfan-β*†‡ 0.006 / 0.019 N/A ND
Ethoprophos 0.003 / 0.009 ≥ LOD N/A ND Pass
Etofenprox 0.014 / 0.042 ≥ LOD N/A ND Pass
Etoxazole 0.007 / 0.020 0.1 N/A ND Pass
Etridiazole* 0.002 / 0.005 N/A ND
Fenhexamid 0.003 / 0.008 0.1 N/A ND Pass
Fenoxycarb 0.003 / 0.010 ≥ LOD N/A ND Pass
Fenpyroximate 0.007 / 0.020 0.1 N/A ND Pass
Fensulfothion 0.003 / 0.010 N/A ND
Fenthion 0.003 / 0.010 N/A ND
Fenvalerate‡ 0.033 / 0.099 N/A ND
Fipronil 0.003 / 0.010 ≥ LOD N/A ND Pass
Flonicamid 0.007 / 0.022 0.1 N/A ND Pass
Fludioxonil 0.003 / 0.010 0.1 N/A ND Pass
Fluopyram‡ 0.003 / 0.009 N/A ND
Hexythiazox 0.003 / 0.010 0.1 N/A ND Pass
Imazalil 0.003 / 0.009 ≥ LOD N/A ND Pass
Imidacloprid 0.003 / 0.010 5 N/A ND Pass
Iprodione 0.077 / 0.233 N/A ND
Kinoprene 0.077 / 0.233 N/A ND
Kresoxim-methyl 0.006 / 0.019 0.1 N/A ND Pass
λ-Cyhalothrin 0.068 / 0.206 N/A ND
Malathion 0.003 / 0.009 0.5 N/A ND Pass
Metalaxyl 0.003 / 0.010 2 N/A ND Pass
Methiocarb 0.003 / 0.008 ≥ LOD N/A ND Pass
Methomyl 0.008 / 0.025 1 N/A ND Pass
Methoprene 0.172 / 0.521 N/A ND
Mevinphos 0.008 / 0.024 ≥ LOD N/A ND Pass
MGK-264 0.015 / 0.047 N/A ND
Myclobutanil 0.003 / 0.009 0.1 N/A ND Pass
Naled 0.021 / 0.064 0.1 N/A ND Pass
Novaluron 0.002 / 0.005 N/A ND
Oxamyl 0.017 / 0.051 0.5 N/A ND Pass
Paclobutrazol 0.003 / 0.010 ≥ LOD N/A ND Pass
Parathion-methyl 0.016 / 0.050 ≥ LOD N/A ND Pass
Pentachloronitrobenzene (Quintozene)* 0.004 / 0.012 0.1 N/A ND Pass
Permethrin 0.056 / 0.168 0.5 N/A ND Pass
Phenothrin 0.016 / 0.047 N/A ND
Phosmet 0.007 / 0.020 0.1 N/A ND Pass
Piperonyl Butoxide 0.010 / 0.029 3 N/A ND Pass
Pirimicarb 0.003 / 0.009 N/A ND
Prallethrin 0.015 / 0.046 0.1 N/A ND Pass
Propiconazole 0.027 / 0.080 0.1 N/A ND Pass
Propoxur 0.003 / 0.008 ≥ LOD N/A ND Pass
Pyraclostrobin 0.003 / 0.010 N/A ND
Pyrethrins 0.016 / 0.049 0.5 N/A ND Pass
Pyridaben 0.005 / 0.017 0.1 N/A ND Pass
Pyriproxyfen 0.003 / 0.009 N/A ND
Resmethrin 0.013 / 0.039 N/A ND
Spinetoram 0.003 / 0.010 0.1 N/A ND Pass
Spinosad 0.003 / 0.010 0.1 N/A ND Pass
Spirodiclofen 0.031 / 0.093 N/A ND
Spiromesifen 0.016 / 0.050 0.1 N/A ND Pass
Spirotetramat 0.003 / 0.010 0.1 N/A ND Pass
Spiroxamine 0.020 / 0.062 ≥ LOD N/A ND Pass
Tebuconazole 0.003 / 0.010 0.1 N/A ND Pass
Tebufenozide 0.003 / 0.008 N/A ND
Teflubenzuron 0.007 / 0.022 N/A ND
Tetrachlorvinphos 0.003 / 0.008 N/A ND
Tetramethrin 0.021 / 0.063 N/A ND
Thiabendazole 0.006 / 0.020 N/A ND
Thiacloprid 0.003 / 0.009 ≥ LOD N/A ND Pass
Thiamethoxam 0.003 / 0.010 5 N/A ND Pass
Thiophanate-methyl 0.013 / 0.040 N/A ND
trans-Permethrin ± 0.00
Trifloxystrobin 0.003 / 0.009 0.1 N/A ND Pass

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS

Mycotoxin Test Results

09/16/2024

PASS

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Compound LOD/LOQ
(μg/kg)
Action Limit
(μg/kg)
Measurement
Uncertainty
(μg/kg)
Result
(μg/kg)
Result
Aflatoxin B1 1.6 / 5.0 N/A ND
Aflatoxin B2 1.4 / 4.1 N/A ND
Aflatoxin G1 1.6 / 4.9 N/A ND
Aflatoxin G2 1.6 / 5.0 N/A ND
Ochratoxin A 1.6 / 5.0 20 N/A ND Pass
Total Aflatoxin 20 ± ND Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

09/14/2024

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Propane 0.234 / 0.781 5000 N/A ND Pass
2-Methylpropane (Isobutane) 0.052 / 0.173 N/A ND
n-Butane 0.019 / 0.063 5000 N/A ND Pass
Total Butanes ± ND
n-Pentane 0.310 / 1.033 5000 N/A ND Pass
n-Hexane 0.110 / 0.366 290 N/A ND Pass
2,2-Dimethylpentane (Neoheptane) 0.493 / 1.642 N/A ND
2,3-Dimethylpentane 1.009 / 3.365 N/A ND
2,4-Dimethylpentane 0.737 / 2.458 N/A ND
3,3-Dimethylpentane 0.198 / 0.660 N/A ND
2,2,3-Trimethylbutane (Triptane) 0.521 / 1.738 N/A ND
2-Methylhexane (Isoheptane) 0.610 / 2.034 N/A ND
3-Methylhexane 0.235 / 0.785 N/A ND
3-Ethylpentane 0.304 / 1.012 N/A ND
n-Heptane 13.12 / 43.72 5000 N/A ND Pass
Total Heptanes ± ND
Benzene 0.089 / 0.295 1 N/A ND Pass
Toluene 0.115 / 0.382 890 N/A ND Pass
1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene) 0.451 / 1.502 N/A ND
1,2-Dimethylbenzene (o-Xylene) 0.387 / 1.289 N/A ND
Total Xylenes 2170 ± ND Pass
Methanol 53.92 / 163.4 3000 N/A ND Pass
Ethanol 8.984 / 27.23 5000 N/A ND Pass
2-Propanol (Isopropyl Alcohol) 8.421 / 25.52 5000 N/A ND Pass
Acetone 10.59 / 32.08 5000 N/A ND Pass
Ethyl Acetate 1.123 / 3.745 5000 N/A ND Pass

Total Butanes = n-Butane + 2-Methylpropane (Isobutane)

Total Heptanes = 2,2-Dimethylpentane (Neoheptane) + 2,3-Dimethylpentane + 2,4-Dimethylpentane + 3,3-Dimethylpentane + 2,2,3-Trimethylbutane (Triptane) + 2-Methylhexane (Isoheptane) + 3-Methylhexane + 3-Ethylpentane + n-Heptane

Total Xylenes = 1,2-Dimethylbenzene (o-Xylene) + 1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene)

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

09/14/2024

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Arsenic 0.02 / 0.1 0.2 N/A ND Pass
Cadmium 0.02 / 0.05 0.2 N/A ND Pass
Lead 0.04 / 0.1 0.5 N/A ND Pass
Mercury 0.002 / 0.01 0.1 N/A ND Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants. And Analysis conducted by 3MTM PetrifilmTM and plate counts of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants and QSP 6794 - Plating with 3MTM PetrifilmTM

Microbiology Test Results (PCR)

09/16/2024

PASS

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Compound Action Limit Result Result
Salmonella spp. Not Detected in 25g ND Pass
Shiga toxin-producing Escherichia coli Not Detected in 25g ND Pass
Microbiology Test Results (PLATING)

09/16/2024

ND

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Compound Action Limit
(cfu/g)
Result
(cfu/g)
Result
Coliforms ND
Total Yeast and Mold ND
Total Aerobic Bacteria ND

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