Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

Mary Jones Orange Cream

Infused, Hemp

Date Issued:

08/10/2024

Total THC 9.734 mg/unit
Total CBD 0.065 mg/unit
Sum Cannabinoids 9.92 mg/unit
Total Cannabinoids 9.92 mg/unit

Sample Information

Sample Details

Sample ID:240805M006

Batch Number:GUM1.080124

Cultivator / Manufacturer

Show Details

Distributor / Tested For

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Cannabinoid Analysis - Summary

Total THC: 9.734 mg/unit

Total CBD: 0.065 mg/unit

Sum of Cannabinoids: 9.92 mg/unit

Total Cannabinoids: 9.92 mg/unit

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Safety Analysis - Summary

Pesticides: ND

Residual Solvents: ND

Heavy Metals: ND

Microbiology (PCR): ND

Microbiology (Plating): ND

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 9.734 mg/unit

9-THC+0.877*THCa)

Total CBD: 0.065 mg/unit

(CBD+0.877*CBDa)

Total Cannabinoids: 9.92 mg/unit

Total CBG: <LOQ

Total CBG (CBG+0.877*CBGa)

Total THCV: <LOQ

Total THCV (THCV+0.877*THCVa)

Total CBC: ND

Total CBC (CBC+0.877*CBCa)

Total CBDV: ND

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

08/07/2024

Result Views

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Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
Δ9 Tetrahydrocannabinol (Δ9THC) 0.002 / 0.014 ±0.1153 2.100 0.2100
∆8 Tetrahydrocannabinol (Δ8THC) 0.01 / 0.02 ±0.001 0.03 0.003
Cannabidiol (CBD) 0.004 / 0.011 ±0.0005 0.014 0.0014
Cannabigerol (CBG) 0.002 / 0.006 N/A <LOQ <LOQ
Cannabinol (CBN) 0.001 / 0.007 N/A <LOQ <LOQ
Tetrahydrocannabivarin (THCV) 0.002 / 0.012 N/A <LOQ <LOQ
Cannabichromene (CBC) 0.003 / 0.010 N/A ND ND
Cannabicyclol (CBL) 0.003 / 0.010 N/A ND ND
Cannabichromenic Acid (CBCa) 0.001 / 0.015 N/A ND ND
Cannabidivarin (CBDV) 0.002 / 0.012 N/A ND ND
Cannabidiolic Acid (CBDa) 0.001 / 0.026 N/A ND ND
Cannabigerolic Acid (CBGa) 0.002 / 0.007 N/A ND ND
Tetrahydrocannabinolic Acid (THCa) 0.001 / 0.005 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.001 / 0.018 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.002 / 0.019 N/A ND ND
SUM OF CANNABINOIDS 2.14 mg/g 0.214%
Unit Mass:

4.635 grams

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Δ9-THC per Unit 9.734 mg/unit
Total THC per Unit 9.734 mg/unit
CBD per Unit 0.065 mg/unit
Total CBD per Unit 0.065 mg/unit
Sum of Cannabinoids per Unit 9.92 mg/unit
Total Cannabinoids per Unit 9.92 mg/unit
Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

08/08/2024

ND

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Compound LOD/LOQ
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Abamectin 0.03 / 0.10 N/A ND
Azoxystrobin 0.02 / 0.07 N/A ND
Bifenazate 0.01 / 0.04 N/A ND
Bifenthrin 0.02 / 0.05 N/A ND
Boscalid 0.03 / 0.09 N/A ND
Chlorpyrifos 0.02 / 0.06 N/A ND
Cypermethrin 0.11 / 0.32 N/A ND
Etoxazole 0.02 / 0.06 N/A ND
Hexythiazox 0.02 / 0.07 N/A ND
Imidacloprid 0.04 / 0.11 N/A ND
Malathion 0.03 / 0.09 N/A ND
Myclobutanil 0.03 / 0.09 N/A ND
Permethrin 0.04 / 0.12 N/A ND
Piperonyl Butoxide 0.02 / 0.07 N/A ND
Propiconazole 0.02 / 0.07 N/A ND
Spiromesifen 0.02 / 0.05 N/A ND
Tebuconazole 0.02 / 0.07 N/A ND
Trifloxystrobin 0.03 / 0.08 N/A ND

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

08/08/2024

ND

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Compound LOD/LOQ
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
1,2-Dichloroethane 0.05 / 0.1 N/A ND
Benzene 0.03 / 0.09 N/A ND
Chloroform 0.1 / 0.2 N/A ND
Dichloromethane (Methylene Chloride) 0.3 / 0.9 N/A ND
Ethylene Oxide 0.3 / 0.8 N/A ND
Trichloroethylene 0.1 / 0.3 N/A ND
2-Propanol (Isopropyl Alcohol) 10 / 40 N/A ND
Acetone 20 / 50 N/A ND
Acetonitrile 2 / 7 N/A ND
Ethanol 20 / 50 N/A ND
Ethyl Acetate 20 / 60 N/A ND
Ethyl Ether 20 / 50 N/A ND
Methanol 50 / 200 N/A ND
n-Butane 10 / 50 N/A ND
n-Heptane 20 / 60 N/A ND
n-Hexane 2 / 5 N/A ND
n-Pentane 20 / 50 N/A ND
Propane 10 / 20 N/A ND
Toluene 7 / 21 N/A ND
Total Xylenes 50 / 160 N/A ND

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

08/09/2024

ND

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Compound LOD/LOQ
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Arsenic 0.02 / 0.1 N/A ND
Cadmium 0.02 / 0.05 N/A ND
Lead 0.04 / 0.1 N/A ND
Mercury 0.002 / 0.01 N/A ND

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants. And Analysis conducted by 3MTM PetrifilmTM and plate counts of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants and QSP 6794 - Plating with 3MTM PetrifilmTM

Microbiology Test Results (PCR)

08/10/2024

ND

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Compound Result
(cfu/g)
Salmonella spp. ND
Staphylococcus aureus ND
Bile-Tolerant Gram-Negative Bacteria ND
Shiga toxin-producing Escherichia coli ND
Microbiology Test Results (PLATING)

08/10/2024

ND

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Compound Result
(cfu/g)
Total Yeast and Mold ND
Total Aerobic Bacteria ND

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