R&R Roll-On Premix

Certificate of Analysis

OFFICIAL COMPLIANCE: COLORADO HEMP

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Sample Name:

R&R Roll-On Premix

Concentrate, Colorado Concentrate/Extract

Total THC 1.119%

Total CBD 69.851%

Sum Cannabinoids 86.40%

Total Cannabinoids 86.35%

Total Terpenoids 0.6823%
PhytoFacts^®

Top 3 Terpenoids

α-Bisabolol 0.2142%
Guaiol 0.1810%
β-Caryophyllene 0.1428%

Sample Information

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Sample Details

Sample ID:240604P023

Batch Number:1-10A-918-02060

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Cultivator / Manufacturer

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Distributor

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PhytoFacts® Report

aroma

flavor

effect

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The PhytoFacts chemometric report provides additional cannabinoid and terpenoid details, including dominant terpenes, entourage effects, aroma, flavor, and more.

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Cannabinoid Analysis - Summary

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Total THC: 1.119%

Total CBD: 69.851%

Sum of Cannabinoids: 86.40%

Total Cannabinoids: 86.35%

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ⁹-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ⁹-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ⁸-THC + CBL + CBN

Total Cannabinoids = (Δ⁹-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ⁸-THC + CBL + CBN

Why are Sum of Cannabinoids and Total Cannabinoids calculated separately?

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

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Total Terpenoids: 0.6823%

α-Bisabolol (0.2142%)

Guaiol (0.1810%)

β-Caryophyllene (0.1428%)

Safety Analysis - Summary

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Pesticides: Tested

Mycotoxins: Pass

Residual Solvents: Tested

Heavy Metals: Pass

Microbiology: Pass

Foreign Material: NT

View Complete Test Results:

Expand All

Cannabinoid Analysis

Tested

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 1.119%

(Δ⁹-THC+0.877*THCa)

Total CBD: 69.851%

(CBD+0.877*CBDa)

Total Cannabinoids: 86.35%

Total CBG: 13.09%

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 1.68%

Total CBC (CBC+0.877*CBCa)

Total CBDV: 0.445%

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

06/07/2024

Result Views

Table Pie Chart

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Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
Cannabidiol (CBD)	0.07 / 0.29	±25.068	696.34	69.634
Cannabigerol (CBG)	0.06 / 0.19	±3.988	129.89	12.989
Cannabichromene (CBC)	0.2 / 0.5	±0.38	16.8	1.68
Δ9 Tetrahydrocannabinol (Δ9THC)	0.06 / 0.26	±0.300	11.19	1.119
Cannabidivarin (CBDV)	0.04 / 0.15	±0.151	4.45	0.445
Cannabidiolic Acid (CBDa)	0.02 / 0.19	±0.057	2.48	0.248
Cannabinol (CBN)	0.1 / 0.3	±0.08	1.6	0.16
Cannabigerolic Acid (CBGa)	0.1 / 0.2	±0.05	1.2	0.12
Cannabicyclol (CBL)	0.06 / 0.24	N/A	ND	ND
Cannabichromenic Acid (CBCa)	0.07 / 0.28	N/A	ND	ND
Tetrahydrocannabivarin (THCV)	0.1 / 0.2	N/A	ND	ND
Tetrahydrocannabinolic Acid (THCa)	0.05 / 0.14	N/A	ND	ND
Cannabidivarinic Acid (CBDVa)	0.03 / 0.53	N/A	ND	ND
Tetrahydrocannabivarinic Acid (THCVa)	0.07 / 0.20	N/A	ND	ND
∆8 Tetrahydrocannabinol (Δ8THC)	0.1 / 0.4	N/A	ND	ND
Total THC		±0.374	11.19 mg/g	1.119%
SUM OF CANNABINOIDS			864.0 mg/g	86.40%

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpenoid Analysis

Tested

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

View PhytoFacts COA

See a visual representation of this sample's cannabinoid and terpenoid properties, including entourage effects, aroma, and flavor profile.

Summary

Total Terpenoids (mg/g): 6.823 mg/g

Total Terpenoids (%): 0.6823%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume. To see more detail for terpenoid content, view the PhytoFacts report.

α-Bisabolol 0.2142%
A sesquiterpene alcohol with a fragrance that can be described as floral, peppery, sweet and clean. Found in chamomile, figwort, yarrow, skullcaps, lavender, ironwort, germander...etc.

Guaiol 0.1810%
A sesquiterpene alcohol with a fragrance that can be described as floral, piney, herbal and woody. Found in guaiacum, cypress pine, ginseng, melaleuca, goatweed, incense grass...etc.

β-Caryophyllene 0.1428%
A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB² receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

06/07/2024

Result Views

Table Bar Graph

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Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
α-Bisabolol	0.008 / 0.026	±0.0889	2.142	0.2142
Guaiol	0.009 / 0.030	±0.0664	1.810	0.1810
β-Caryophyllene	0.004 / 0.012	±0.0396	1.428	0.1428
α-Humulene	0.009 / 0.029	±0.0150	0.598	0.0598
Nerolidol	0.006 / 0.019	±0.0109	0.222	0.0222
Caryophyllene Oxide	0.010 / 0.033	±0.0040	0.112	0.0112
Terpineol	0.009 / 0.031	±0.0038	0.079	0.0079
Fenchol	0.010 / 0.034	±0.0022	0.074	0.0074
Linalool	0.009 / 0.032	±0.0019	0.065	0.0065
Borneol	0.005 / 0.016	±0.0017	0.053	0.0053
Valencene	0.009 / 0.030	±0.0028	0.053	0.0053
Terpinolene	0.008 / 0.026	±0.0008	0.049	0.0049
Limonene	0.005 / 0.016	±0.0004	0.039	0.0039
trans-β-Farnesene	0.008 / 0.025	±0.0009	0.033	0.0033
α-Pinene	0.005 / 0.017	±0.0002	0.027	0.0027
Sabinene	0.004 / 0.014	±0.0002	0.022	0.0022
p-Cymene	0.005 / 0.016	±0.0004	0.017	0.0017
Myrcene	0.008 / 0.025	N/A	<LOQ	<LOQ
Fenchone	0.009 / 0.028	N/A	<LOQ	<LOQ
Eucalyptol	0.006 / 0.018	N/A	<LOQ	<LOQ
Citronellol	0.003 / 0.010	N/A	<LOQ	<LOQ
β-Pinene	0.004 / 0.014	N/A	<LOQ	<LOQ
α-Terpinene	0.005 / 0.017	N/A	<LOQ	<LOQ
α-Phellandrene	0.006 / 0.020	N/A	<LOQ	<LOQ
Nerol	0.003 / 0.011	N/A	ND	ND
Cedrol	0.008 / 0.027	N/A	ND	ND
Camphor	0.006 / 0.019	N/A	ND	ND
Menthol	0.008 / 0.025	N/A	ND	ND
Camphene	0.005 / 0.015	N/A	ND	ND
Geraniol	0.002 / 0.007	N/A	ND	ND
Pulegone	0.003 / 0.011	N/A	ND	ND
Isoborneol	0.004 / 0.012	N/A	ND	ND
Isopulegol	0.005 / 0.016	N/A	ND	ND
β-Ocimene	0.006 / 0.020	N/A	ND	ND
Δ³-Carene	0.005 / 0.018	N/A	ND	ND
α-Cedrene	0.005 / 0.016	N/A	ND	ND
Geranyl Acetate	0.004 / 0.014	N/A	ND	ND
γ-Terpinene	0.006 / 0.018	N/A	ND	ND
Sabinene Hydrate	0.006 / 0.022	N/A	ND	ND
TOTAL			6.823 mg/g	0.6823%

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Pesticide Analysis

Tested

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

06/09/2024

TESTED

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Compound	LOD/LOQ (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)
Abamectin	0.032 / 0.097	N/A	ND
Acephate	0.006 / 0.018	N/A	ND
Acequinocyl	0.009 / 0.027	N/A	ND
Acetamiprid	0.016 / 0.049	N/A	ND
Aldicarb	0.030 / 0.090	N/A	ND
Allethrin	0.030 / 0.092	N/A	ND
Atrazine	0.006 / 0.019	N/A	ND
Azadirachtin	0.082 / 0.248	N/A	ND
Azoxystrobin	0.003 / 0.009	N/A	ND
Benzovindiflupyr	0.003 / 0.009	N/A	ND
Bifenazate	0.003 / 0.009	N/A	ND
Bifenthrin	0.021 / 0.064	N/A	<LOQ
Boscalid	0.003 / 0.009	N/A	ND
Buprofezin^‡	0.006 / 0.019	N/A	ND
Carbaryl	0.007 / 0.020	N/A	ND
Carbofuran	0.003 / 0.008	N/A	ND
Chlorantraniliprole	0.006 / 0.018	N/A	ND
Chlorfenapyr*	0.005 / 0.015	N/A	ND
Chlorpyrifos	0.013 / 0.039	N/A	ND
cis-Permethrin		±	0.00
Clofentezine	0.003 / 0.009	N/A	ND
Clothianidin	0.008 / 0.025	N/A	ND
Coumaphos	0.003 / 0.010	N/A	ND
Cyantraniliprole	0.003 / 0.010	N/A	ND
Cyfluthrin	0.052 / 0.159	N/A	ND
Cypermethrin	0.051 / 0.153	N/A	ND
Cyprodinil^‡	0.003 / 0.008	N/A	ND
Daminozide	0.026 / 0.077	N/A	ND
Deltamethrin	0.059 / 0.180	N/A	ND
Diazinon	0.006 / 0.017	N/A	ND
Dichlorvos (DDVP)	0.012 / 0.038	N/A	ND
Dimethoate	0.003 / 0.009	N/A	ND
Dimethomorph	0.016 / 0.050	N/A	ND
Dinotefuran	0.010 / 0.030	N/A	ND
Diuron	0.013 / 0.040	N/A	ND
Dodemorph	0.012 / 0.035	N/A	ND
Endosulfan sulfate^†^‡	0.016 / 0.048	N/A	ND
Endosulfan-α*^†^‡	0.004 / 0.014	N/A	ND
Endosulfan-β*^†^‡	0.006 / 0.019	N/A	ND
Ethoprophos	0.003 / 0.009	N/A	ND
Etofenprox	0.014 / 0.042	N/A	ND
Etoxazole	0.007 / 0.020	N/A	ND
Etridiazole*	0.002 / 0.005	N/A	ND
Fenhexamid	0.003 / 0.008	N/A	ND
Fenoxycarb	0.003 / 0.010	N/A	ND
Fenpyroximate	0.007 / 0.020	N/A	ND
Fensulfothion	0.003 / 0.010	N/A	ND
Fenthion	0.003 / 0.010	N/A	ND
Fenvalerate^‡	0.033 / 0.099	N/A	ND
Fipronil	0.003 / 0.010	N/A	ND
Flonicamid	0.007 / 0.022	N/A	ND
Fludioxonil	0.003 / 0.010	N/A	ND
Fluopyram^‡	0.003 / 0.009	N/A	ND
Hexythiazox	0.003 / 0.010	N/A	ND
Imazalil	0.003 / 0.009	N/A	ND
Imidacloprid	0.003 / 0.010	N/A	ND
Iprodione	0.077 / 0.233	N/A	ND
Kinoprene	0.077 / 0.233	N/A	ND
Kresoxim-methyl	0.006 / 0.019	N/A	ND
λ-Cyhalothrin	0.068 / 0.206	N/A	ND
Malathion	0.003 / 0.009	N/A	ND
Metalaxyl	0.003 / 0.010	N/A	ND
Methiocarb	0.003 / 0.008	N/A	ND
Methomyl	0.008 / 0.025	N/A	ND
Methoprene	0.172 / 0.521	N/A	ND
Mevinphos	0.008 / 0.024	N/A	ND
MGK-264	0.015 / 0.047	N/A	ND
Myclobutanil	0.003 / 0.009	N/A	ND
Naled	0.021 / 0.064	N/A	ND
Novaluron	0.002 / 0.005	N/A	ND
Oxamyl	0.017 / 0.051	N/A	ND
Paclobutrazol	0.003 / 0.010	N/A	ND
Parathion-methyl	0.016 / 0.050	N/A	ND
Pentachloronitrobenzene (Quintozene)*	0.004 / 0.012	N/A	ND
Permethrin	0.056 / 0.168	N/A	ND
Phenothrin	0.016 / 0.047	N/A	ND
Phosmet	0.007 / 0.020	N/A	ND
Piperonyl Butoxide	0.010 / 0.029	N/A	ND
Pirimicarb	0.003 / 0.009	N/A	ND
Prallethrin	0.015 / 0.046	N/A	ND
Propiconazole	0.027 / 0.080	N/A	ND
Propoxur	0.003 / 0.008	N/A	ND
Pyraclostrobin	0.003 / 0.010	N/A	ND
Pyrethrins	0.016 / 0.049	N/A	ND
Pyridaben	0.005 / 0.017	N/A	ND
Pyriproxyfen	0.003 / 0.009	N/A	ND
Resmethrin	0.013 / 0.039	N/A	ND
Spinetoram	0.003 / 0.010	N/A	ND
Spinosad	0.003 / 0.010	N/A	ND
Spirodiclofen	0.031 / 0.093	N/A	ND
Spiromesifen	0.016 / 0.050	N/A	ND
Spirotetramat	0.003 / 0.010	N/A	ND
Spiroxamine	0.020 / 0.062	N/A	ND
Tebuconazole	0.003 / 0.010	N/A	ND
Tebufenozide	0.003 / 0.008	N/A	ND
Teflubenzuron	0.007 / 0.022	N/A	ND
Tetrachlorvinphos	0.003 / 0.008	N/A	ND
Tetramethrin	0.021 / 0.063	N/A	ND
Thiabendazole	0.006 / 0.020	N/A	ND
Thiacloprid	0.003 / 0.009	N/A	ND
Thiamethoxam	0.003 / 0.010	N/A	ND
Thiophanate-methyl	0.013 / 0.040	N/A	ND
trans-Permethrin		±	0.00
Trifloxystrobin	0.003 / 0.009	±0.0007	0.028

Mycotoxin Analysis

Pass

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS

Mycotoxin Test Results

06/09/2024

PASS

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Compound	LOD/LOQ (μg/kg)	Action Limit (μg/kg)	Measurement Uncertainty (μg/kg)	Result (μg/kg)	Result
Aflatoxin B1	1.6 / 5.0	5	N/A	ND	Pass
Aflatoxin B2	1.4 / 4.1		N/A	ND
Aflatoxin G1	1.6 / 4.9		N/A	ND
Aflatoxin G2	1.6 / 5.0		N/A	ND
Ochratoxin A	1.6 / 5.0	5	N/A	ND	Pass
Total Aflatoxin		20	±	ND	Pass

Residual Solvents Analysis

Tested

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

06/10/2024

TESTED

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Compound	LOD/LOQ (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)
Propane	0.234 / 0.781	N/A	ND
2-Methylpropane (Isobutane)	0.052 / 0.173	N/A	ND
n-Butane	0.019 / 0.063	±0.1493	3.607
Total Butanes		±	3.607
n-Pentane	0.310 / 1.033	N/A	ND
n-Hexane	0.110 / 0.366	N/A	ND
2,2-Dimethylpentane (Neoheptane)	0.493 / 1.642	N/A	ND
2,3-Dimethylpentane	1.009 / 3.365	N/A	ND
2,4-Dimethylpentane	0.737 / 2.458	N/A	ND
3,3-Dimethylpentane	0.198 / 0.660	N/A	ND
2,2,3-Trimethylbutane (Triptane)	0.521 / 1.738	N/A	ND
2-Methylhexane (Isoheptane)	0.610 / 2.034	N/A	ND
3-Methylhexane	0.235 / 0.785	N/A	ND
3-Ethylpentane	0.304 / 1.012	N/A	ND
n-Heptane	13.12 / 43.72	N/A	ND
Total Heptanes		±	ND
Benzene	0.089 / 0.295	N/A	ND
Toluene	0.115 / 0.382	N/A	ND
1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene)	0.451 / 1.502	N/A	ND
1,2-Dimethylbenzene (o-Xylene)	0.387 / 1.289	N/A	ND
Total Xylenes		±	ND
Methanol	53.92 / 163.4	N/A	ND
Ethanol	8.984 / 27.23	N/A	ND
2-Propanol (Isopropyl Alcohol)	8.421 / 25.52	N/A	ND
Acetone	10.59 / 32.08	±1.138	68.16
Ethyl Acetate	1.123 / 3.745	N/A	ND

Total Butanes = n-Butane + 2-Methylpropane (Isobutane)

Total Heptanes = 2,2-Dimethylpentane (Neoheptane) + 2,3-Dimethylpentane + 2,4-Dimethylpentane + 3,3-Dimethylpentane + 2,2,3-Trimethylbutane (Triptane) + 2-Methylhexane (Isoheptane) + 3-Methylhexane + 3-Ethylpentane + n-Heptane

Total Xylenes = 1,2-Dimethylbenzene (o-Xylene) + 1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene)

Heavy Metals Analysis

Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

06/07/2024

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
Arsenic	0.02 / 0.1	1.5	N/A	ND	Pass
Cadmium	0.02 / 0.05	0.5	N/A	ND	Pass
Lead	0.04 / 0.1	0.5	N/A	ND	Pass
Mercury	0.002 / 0.01	1.5	N/A	<LOQ	Pass

Microbiology Analysis

Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants. And Analysis conducted by 3M^TM Petrifilm^TM and plate counts of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants and QSP 6794 - Plating with 3M^TM Petrifilm^TM

Microbiology Test Results (PCR)

06/10/2024

PASS

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Compound	Action Limit	Result	Result
Salmonella spp.	Not Detected in 25g	ND	Pass
Shiga toxin-producing Escherichia coli	Not Detected in 25g	ND	Pass

Microbiology Test Results (PLATING)

06/10/2024

PASS

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Compound	Action Limit (cfu/g)	Result (cfu/g)	Result
Coliforms	100	ND	Pass
Total Yeast and Mold	1000	ND	Pass
Total Aerobic Bacteria	10000	ND	Pass

COA ID: 240604P023-001

These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

Sample Certification: 6 CCR 1010-24 Colorado Hemp Product and Safe Harbor Hemp Product Regulations

Decision Rule: Statements of conformity (e.g. Pass/Fail) to specifications are made in this report without taking measurement uncertainty into account. Where statements of conformity are made in this report, the following decision rules are applied: PASS - Results within limits/specifications, FAIL - Results exceed limits/specifications.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT), μg/g = ppm, μg/kg = ppb, too numerous to count >250 cfu/plate (TNTC), colony-forming unit (cfu)