R&R Sleep Softgel Premix

Certificate of Analysis

OFFICIAL COMPLIANCE: COLORADO HEMP

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Sample Name:

R&R Sleep Softgel Premix

Infused, Colorado Infused

Total THC 11.680 mg/mL

Total CBD 364.558 mg/mL

Sum Cannabinoids 453.164 mg/mL

Total Cannabinoids 452.275 mg/mL

Total Terpenoids 0.3950%

Top 3 Terpenoids

α-Bisabolol 0.1496%
Guaiol 0.1402%
β-Caryophyllene 0.0526%

Sample Information

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Sample Details

Sample ID:240528R024

Batch Number:1-10A-917-70048

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Cannabinoid Analysis - Summary

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Total THC: 11.680 mg/mL

Total CBD: 364.558 mg/mL

Sum of Cannabinoids: 453.164 mg/mL

Total Cannabinoids: 452.275 mg/mL

Density:0.9952 g/mL

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ⁹-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ⁹-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ⁸-THC + CBL + CBN

Total Cannabinoids = (Δ⁹-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ⁸-THC + CBL + CBN

Why are Sum of Cannabinoids and Total Cannabinoids calculated separately?

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

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Total Terpenoids: 0.3950%

α-Bisabolol (0.1496%)

Guaiol (0.1402%)

β-Caryophyllene (0.0526%)

Safety Analysis - Summary

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Pesticides: Tested

Mycotoxins: Pass

Residual Solvents: Tested

Heavy Metals: Pass

Microbiology: Pass

Foreign Material: NT

Water Activity: NT

View Complete Test Results:

Expand All

Cannabinoid Analysis

Tested

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 11.680 mg/mL

(Δ⁹-THC+0.877*THCa)

Total CBD: 364.558 mg/mL

(CBD+0.877*CBDa)

Total Cannabinoids: 452.275 mg/mL

Total CBG: 6.854 mg/mL

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 19.023 mg/mL

Total CBC (CBC+0.877*CBCa)

Total CBDV: 3.622 mg/mL

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

05/31/2024

Result Views

Table Pie Chart

Swipe left on table to see additional columns

Compound	LOD/LOQ (mg/mL)	Measurement Uncertainty (mg/mL)	Result (mg/mL)	Result (%)
Cannabidiol (CBD)	0.080 / 0.220	±13.3734	358.537	36.0266
Cannabinol (CBN)	0.020 / 0.140	±1.3127	45.739	4.5960
Cannabichromene (CBC)	0.060 / 0.200	±0.6022	18.701	1.8791
Δ9 Tetrahydrocannabinol (Δ9THC)	0.040 / 0.280	±0.6412	11.680	1.1736
Cannabidiolic Acid (CBDa)	0.020 / 0.520	±0.1950	6.865	0.6898
Cannabigerol (CBG)	0.040 / 0.120	±0.3324	6.854	0.6887
Cannabidivarin (CBDV)	0.040 / 0.240	±0.1478	3.622	0.3639
Cannabicyclol (CBL)	0.060 / 0.200	±0.0295	0.799	0.0803
Cannabichromenic Acid (CBCa)	0.020 / 0.300	±0.0140	0.367	0.0369
Cannabigerolic Acid (CBGa)	0.040 / 0.140	N/A	ND	ND
Tetrahydrocannabivarin (THCV)	0.040 / 0.240	N/A	ND	ND
Tetrahydrocannabinolic Acid (THCa)	0.020 / 0.100	N/A	ND	ND
Cannabidivarinic Acid (CBDVa)	0.020 / 0.360	N/A	ND	ND
Tetrahydrocannabivarinic Acid (THCVa)	0.040 / 0.380	N/A	ND	ND
∆8 Tetrahydrocannabinol (Δ8THC)	0.20 / 0.40	N/A	ND	ND
Total THC		±0.6739	11.680 mg/g	1.1736%
SUM OF CANNABINOIDS			453.164 mg/mL	45.5350%

Density Test Result

0.9952 g/mL Tested 05/31/2024 Method: QSP 7870 - Sample Preparation

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpenoid Analysis

Tested

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

Summary

Total Terpenoids (mg/g): 3.950 mg/g

Total Terpenoids (%): 0.3950%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume.

α-Bisabolol 0.1496%
A sesquiterpene alcohol with a fragrance that can be described as floral, peppery, sweet and clean. Found in chamomile, figwort, yarrow, skullcaps, lavender, ironwort, germander...etc.

Guaiol 0.1402%
A sesquiterpene alcohol with a fragrance that can be described as floral, piney, herbal and woody. Found in guaiacum, cypress pine, ginseng, melaleuca, goatweed, incense grass...etc.

β-Caryophyllene 0.0526%
A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB² receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

05/31/2024

Result Views

Table Bar Graph

Swipe left on table to see additional columns

Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
α-Bisabolol	0.008 / 0.026	±0.0621	1.496	0.1496
Guaiol	0.009 / 0.030	±0.0515	1.402	0.1402
β-Caryophyllene	0.004 / 0.012	±0.0146	0.526	0.0526
α-Humulene	0.009 / 0.029	±0.0071	0.283	0.0283
Nerolidol	0.006 / 0.019	±0.0059	0.121	0.0121
Caryophyllene Oxide	0.010 / 0.033	±0.0017	0.047	0.0047
Terpinolene	0.008 / 0.026	±0.0005	0.034	0.0034
Borneol	0.005 / 0.016	±0.0010	0.030	0.0030
Citronellol	0.003 / 0.010	±0.0004	0.011	0.0011
Fenchol	0.010 / 0.034	N/A	<LOQ	<LOQ
Fenchone	0.009 / 0.028	N/A	<LOQ	<LOQ
Limonene	0.005 / 0.016	N/A	<LOQ	<LOQ
p-Cymene	0.005 / 0.016	N/A	<LOQ	<LOQ
Terpineol	0.009 / 0.031	N/A	<LOQ	<LOQ
Valencene	0.009 / 0.030	N/A	<LOQ	<LOQ
Eucalyptol	0.006 / 0.018	N/A	<LOQ	<LOQ
α-Phellandrene	0.006 / 0.020	N/A	<LOQ	<LOQ
Nerol	0.003 / 0.011	N/A	ND	ND
Cedrol	0.008 / 0.027	N/A	ND	ND
Camphor	0.006 / 0.019	N/A	ND	ND
Menthol	0.008 / 0.025	N/A	ND	ND
Myrcene	0.008 / 0.025	N/A	ND	ND
Camphene	0.005 / 0.015	N/A	ND	ND
Geraniol	0.002 / 0.007	N/A	ND	ND
Linalool	0.009 / 0.032	N/A	ND	ND
Pulegone	0.003 / 0.011	N/A	ND	ND
Sabinene	0.004 / 0.014	N/A	ND	ND
Isoborneol	0.004 / 0.012	N/A	ND	ND
Isopulegol	0.005 / 0.016	N/A	ND	ND
β-Pinene	0.004 / 0.014	N/A	ND	ND
α-Pinene	0.005 / 0.017	N/A	ND	ND
β-Ocimene	0.006 / 0.020	N/A	ND	ND
Δ³-Carene	0.005 / 0.018	N/A	ND	ND
α-Cedrene	0.005 / 0.016	N/A	ND	ND
Geranyl Acetate	0.004 / 0.014	N/A	ND	ND
α-Terpinene	0.005 / 0.017	N/A	ND	ND
γ-Terpinene	0.006 / 0.018	N/A	ND	ND
Sabinene Hydrate	0.006 / 0.022	N/A	ND	ND
trans-β-Farnesene	0.008 / 0.025	N/A	ND	ND
TOTAL			3.950 mg/g	0.3950%

Learn more

Pesticide Analysis

Tested

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

06/03/2024

TESTED

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Compound	LOD/LOQ (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)
Abamectin	0.032 / 0.097	N/A	ND
Acephate	0.006 / 0.018	N/A	ND
Acequinocyl	0.009 / 0.027	N/A	ND
Acetamiprid	0.016 / 0.049	N/A	ND
Aldicarb	0.030 / 0.090	N/A	ND
Allethrin	0.030 / 0.092	N/A	ND
Atrazine	0.006 / 0.019	N/A	ND
Azadirachtin	0.082 / 0.248	N/A	ND
Azoxystrobin	0.003 / 0.009	N/A	ND
Benzovindiflupyr	0.003 / 0.009	N/A	ND
Bifenazate	0.003 / 0.009	N/A	ND
Bifenthrin	0.021 / 0.064	N/A	ND
Boscalid	0.003 / 0.009	N/A	ND
Buprofezin^‡	0.006 / 0.019	N/A	ND
Carbaryl	0.007 / 0.020	N/A	ND
Carbofuran	0.003 / 0.008	N/A	ND
Chlorantraniliprole	0.006 / 0.018	N/A	ND
Chlorfenapyr*	0.005 / 0.015	N/A	ND
Chlorpyrifos	0.013 / 0.039	N/A	ND
cis-Permethrin		±	0.00
Clofentezine	0.003 / 0.009	N/A	ND
Clothianidin	0.008 / 0.025	N/A	ND
Coumaphos	0.003 / 0.010	N/A	ND
Cyantraniliprole	0.003 / 0.010	N/A	ND
Cyfluthrin	0.052 / 0.159	N/A	ND
Cypermethrin	0.051 / 0.153	N/A	ND
Cyprodinil^‡	0.003 / 0.008	N/A	ND
Daminozide	0.026 / 0.077	N/A	ND
Deltamethrin	0.059 / 0.180	N/A	ND
Diazinon	0.006 / 0.017	N/A	ND
Dichlorvos (DDVP)	0.012 / 0.038	N/A	ND
Dimethoate	0.003 / 0.009	N/A	ND
Dimethomorph	0.016 / 0.050	N/A	ND
Dinotefuran	0.010 / 0.030	N/A	ND
Diuron	0.013 / 0.040	N/A	ND
Dodemorph	0.012 / 0.035	N/A	ND
Endosulfan sulfate^†^‡	0.016 / 0.048	N/A	ND
Endosulfan-α*^†^‡	0.004 / 0.014	N/A	ND
Endosulfan-β*^†^‡	0.006 / 0.019	N/A	ND
Ethoprophos	0.003 / 0.009	N/A	ND
Etofenprox	0.014 / 0.042	N/A	ND
Etoxazole	0.007 / 0.020	N/A	ND
Etridiazole*	0.002 / 0.005	N/A	ND
Fenhexamid	0.003 / 0.008	N/A	ND
Fenoxycarb	0.003 / 0.010	N/A	ND
Fenpyroximate	0.007 / 0.020	N/A	ND
Fensulfothion	0.003 / 0.010	N/A	ND
Fenthion	0.003 / 0.010	N/A	ND
Fenvalerate^‡	0.033 / 0.099	N/A	ND
Fipronil	0.003 / 0.010	N/A	ND
Flonicamid	0.007 / 0.022	N/A	ND
Fludioxonil	0.003 / 0.010	N/A	ND
Fluopyram^‡	0.003 / 0.009	N/A	ND
Hexythiazox	0.003 / 0.010	N/A	ND
Imazalil	0.003 / 0.009	N/A	ND
Imidacloprid	0.003 / 0.010	N/A	ND
Iprodione	0.077 / 0.233	N/A	ND
Kinoprene	0.077 / 0.233	N/A	ND
Kresoxim-methyl	0.006 / 0.019	N/A	ND
λ-Cyhalothrin	0.068 / 0.206	N/A	ND
Malathion	0.003 / 0.009	N/A	ND
Metalaxyl	0.003 / 0.010	N/A	ND
Methiocarb	0.003 / 0.008	N/A	ND
Methomyl	0.008 / 0.025	N/A	ND
Methoprene	0.172 / 0.521	N/A	ND
Mevinphos	0.008 / 0.024	N/A	ND
MGK-264	0.015 / 0.047	N/A	ND
Myclobutanil	0.003 / 0.009	N/A	ND
Naled	0.021 / 0.064	N/A	ND
Novaluron	0.002 / 0.005	N/A	ND
Oxamyl	0.017 / 0.051	N/A	ND
Paclobutrazol	0.003 / 0.010	N/A	ND
Parathion-methyl	0.016 / 0.050	N/A	ND
Pentachloronitrobenzene (Quintozene)*	0.004 / 0.012	N/A	ND
Permethrin	0.056 / 0.168	N/A	ND
Phenothrin	0.016 / 0.047	N/A	ND
Phosmet	0.007 / 0.020	N/A	ND
Piperonyl Butoxide	0.010 / 0.029	N/A	ND
Pirimicarb	0.003 / 0.009	N/A	ND
Prallethrin	0.015 / 0.046	N/A	ND
Propiconazole	0.027 / 0.080	N/A	ND
Propoxur	0.003 / 0.008	N/A	ND
Pyraclostrobin	0.003 / 0.010	N/A	ND
Pyrethrins	0.016 / 0.049	N/A	ND
Pyridaben	0.005 / 0.017	N/A	ND
Pyriproxyfen	0.003 / 0.009	N/A	ND
Resmethrin	0.013 / 0.039	N/A	ND
Spinetoram	0.003 / 0.010	N/A	ND
Spinosad	0.003 / 0.010	N/A	ND
Spirodiclofen	0.031 / 0.093	N/A	ND
Spiromesifen	0.016 / 0.050	N/A	ND
Spirotetramat	0.003 / 0.010	N/A	ND
Spiroxamine	0.020 / 0.062	N/A	ND
Tebuconazole	0.003 / 0.010	N/A	ND
Tebufenozide	0.003 / 0.008	N/A	ND
Teflubenzuron	0.007 / 0.022	N/A	ND
Tetrachlorvinphos	0.003 / 0.008	N/A	ND
Tetramethrin	0.021 / 0.063	N/A	ND
Thiabendazole	0.006 / 0.020	N/A	ND
Thiacloprid	0.003 / 0.009	N/A	ND
Thiamethoxam	0.003 / 0.010	N/A	ND
Thiophanate-methyl	0.013 / 0.040	N/A	ND
trans-Permethrin		±	0.00
Trifloxystrobin	0.003 / 0.009	±0.0004	0.015

Mycotoxin Analysis

Pass

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS

Mycotoxin Test Results

06/03/2024

PASS

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Compound	LOD/LOQ (μg/kg)	Action Limit (μg/kg)	Measurement Uncertainty (μg/kg)	Result (μg/kg)	Result
Aflatoxin B1	1.6 / 5.0	5	N/A	ND	Pass
Aflatoxin B2	1.4 / 4.1		N/A	ND
Aflatoxin G1	1.6 / 4.9		N/A	ND
Aflatoxin G2	1.6 / 5.0		N/A	ND
Ochratoxin A	1.6 / 5.0	5	N/A	ND	Pass
Total Aflatoxin		20	±	ND	Pass

Residual Solvents Analysis

Tested

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

06/03/2024

TESTED

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Compound	LOD/LOQ (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)
Propane	0.234 / 0.781	N/A	ND
2-Methylpropane (Isobutane)	0.052 / 0.173	N/A	ND
n-Butane	0.019 / 0.063	N/A	ND
Total Butanes		±	ND
n-Pentane	0.310 / 1.033	N/A	ND
n-Hexane	0.110 / 0.366	N/A	ND
2,2-Dimethylpentane (Neoheptane)	0.493 / 1.642	N/A	ND
2,3-Dimethylpentane	1.009 / 3.365	N/A	ND
2,4-Dimethylpentane	0.737 / 2.458	N/A	ND
3,3-Dimethylpentane	0.198 / 0.660	N/A	ND
2,2,3-Trimethylbutane (Triptane)	0.521 / 1.738	N/A	ND
2-Methylhexane (Isoheptane)	0.610 / 2.034	N/A	ND
3-Methylhexane	0.235 / 0.785	N/A	ND
3-Ethylpentane	0.304 / 1.012	N/A	ND
n-Heptane	13.12 / 43.72	N/A	ND
Total Heptanes		±	ND
Benzene	0.089 / 0.295	N/A	ND
Toluene	0.115 / 0.382	N/A	ND
1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene)	0.451 / 1.502	N/A	ND
1,2-Dimethylbenzene (o-Xylene)	0.387 / 1.289	N/A	ND
Total Xylenes		±	ND
Methanol	53.92 / 163.4	N/A	ND
Ethanol	8.984 / 27.23	N/A	ND
2-Propanol (Isopropyl Alcohol)	8.421 / 25.52	N/A	ND
Acetone	10.59 / 32.08	N/A	<LOQ
Ethyl Acetate	1.123 / 3.745	N/A	ND

Total Butanes = n-Butane + 2-Methylpropane (Isobutane)

Total Heptanes = 2,2-Dimethylpentane (Neoheptane) + 2,3-Dimethylpentane + 2,4-Dimethylpentane + 3,3-Dimethylpentane + 2,2,3-Trimethylbutane (Triptane) + 2-Methylhexane (Isoheptane) + 3-Methylhexane + 3-Ethylpentane + n-Heptane

Total Xylenes = 1,2-Dimethylbenzene (o-Xylene) + 1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene)

Heavy Metals Analysis

Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

05/30/2024

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
Arsenic	0.02 / 0.1	1.5	N/A	ND	Pass
Cadmium	0.02 / 0.05	0.5	N/A	ND	Pass
Lead	0.04 / 0.1	0.5	N/A	ND	Pass
Mercury	0.002 / 0.01	1.5	N/A	ND	Pass

Microbiology Analysis

Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants. And Analysis conducted by 3M^TM Petrifilm^TM and plate counts of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants and QSP 6794 - Plating with 3M^TM Petrifilm^TM

Microbiology Test Results (PCR)

06/01/2024

PASS

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Compound	Action Limit	Result	Result
Salmonella spp.	Not Detected in 25g	ND	Pass
Shiga toxin-producing Escherichia coli	Not Detected in 25g	ND	Pass

Microbiology Test Results (PLATING)

06/01/2024

PASS

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Compound	Action Limit (cfu/g)	Result (cfu/g)	Result
Coliforms	100	ND	Pass
Total Yeast and Mold	1000	ND	Pass
Total Aerobic Bacteria	10000	ND	Pass

COA ID: 240528R024-001

These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

Sample Certification: 6 CCR 1010-24 Colorado Hemp Product and Safe Harbor Hemp Product Regulations

Decision Rule: Statements of conformity (e.g. Pass/Fail) to specifications are made in this report without taking measurement uncertainty into account. Where statements of conformity are made in this report, the following decision rules are applied: PASS - Results within limits/specifications, FAIL - Results exceed limits/specifications.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT), μg/g = ppm, μg/kg = ppb, too numerous to count >250 cfu/plate (TNTC), colony-forming unit (cfu)