Pie Scream

Certificate of Analysis

HEMP QUALITY ASSURANCE TEST

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Sample Name:

Pie Scream

Flower, Inhalable

Total THC 19.96%

Total CBD <LOQ

Sum Cannabinoids 22.69%

Total Cannabinoids 19.96%

Total Terpenoids 0.2054%
PhytoFacts^®

Top 3 Terpenoids

Limonene 0.0357%
Myrcene 0.0345%
β-Caryophyllene 0.0335%

Sample Information

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Sample Details

Sample ID:240520R008

Batch Number:PS51724

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Cultivator / Manufacturer

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Distributor / Tested For

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PhytoFacts® Report

aroma

flavor

effect

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The PhytoFacts chemometric report provides additional cannabinoid and terpenoid details, including dominant terpenes, entourage effects, aroma, flavor, and more.

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Cannabinoid Analysis - Summary

Calculated using Dry-Weight

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Total THC: 19.96%

Total CBD: <LOQ

Sum of Cannabinoids: 22.69%

Total Cannabinoids: 19.96%

Moisture:80.2%

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ⁹-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ⁹-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ⁸-THC + CBL + CBN

Total Cannabinoids = (Δ⁹-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ⁸-THC + CBL + CBN

What is dry weight, and how is it calculated?

Dry weight: The weight of a sample after it goes through the drying process.

Pursuant to section § 5724 of California Code of Regulations Title 16 Division 42. Department of Cannabis Control, the equation for moisture correction is: Dry-weight percent cannabinoid = wet-weight percent cannabinoid / (1 − percent moisture / 100)

Why are Sum of Cannabinoids and Total Cannabinoids calculated separately?

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

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Total Terpenoids: 0.2054%

Limonene (0.0357%)

Myrcene (0.0345%)

β-Caryophyllene (0.0335%)

Safety Analysis - Summary

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Heavy Metals: Pass

Microbiology (Plating): ND

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Cannabinoid Analysis

Tested

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD). Calculated using Dry-Weight.

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 19.96%

(Δ⁹-THC+0.877*THCa)

Total CBD: <LOQ

(CBD+0.877*CBDa)

Total Cannabinoids: 19.96%

Total CBG: <LOQ

Total CBG (CBG+0.877*CBGa)

Total THCV: <LOQ

Total THCV (THCV+0.877*THCVa)

Total CBC: <LOQ

Total CBC (CBC+0.877*CBCa)

Total CBDV: ND

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

05/23/2024

Result Views

Table Pie Chart

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Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
Tetrahydrocannabinolic Acid (THCa)	0.04 / 0.24	±7.140	222.42	22.242
Δ9 Tetrahydrocannabinol (Δ9THC)	0.1 / 0.4	±0.14	4.5	0.45
Cannabigerol (CBG)	0.2 / 0.5	N/A	<LOQ	<LOQ
Cannabichromenic Acid (CBCa)	0.1 / 0.4	N/A	<LOQ	<LOQ
Cannabidiolic Acid (CBDa)	0.06 / 0.22	N/A	<LOQ	<LOQ
Cannabigerolic Acid (CBGa)	0.1 / 0.4	N/A	<LOQ	<LOQ
Tetrahydrocannabivarinic Acid (THCVa)	0.05 / 0.17	N/A	<LOQ	<LOQ
Cannabichromene (CBC)	0.1 / 0.2	N/A	ND	ND
Cannabidiol (CBD)	0.1 / 0.3	N/A	ND	ND
Cannabicyclol (CBL)	0.1 / 0.4	N/A	ND	ND
Cannabinol (CBN)	0.07 / 0.20	N/A	ND	ND
Cannabidivarin (CBDV)	0.1 / 0.3	N/A	ND	ND
Tetrahydrocannabivarin (THCV)	0.07 / 0.21	N/A	ND	ND
Cannabidivarinic Acid (CBDVa)	0.02 / 0.22	N/A	ND	ND
∆8 Tetrahydrocannabinol (Δ8THC)	0.05 / 0.50	N/A	ND	ND
SUM OF CANNABINOIDS			226.9 mg/g	22.69%

Moisture Test Result

80.2% Tested 06/10/2024 Method: QSP 1224 - Loss on Drying (Moisture)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpenoid Analysis

Tested

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

View PhytoFacts COA

See a visual representation of this sample's cannabinoid and terpenoid properties, including entourage effects, aroma, and flavor profile.

Summary

Total Terpenoids (mg/g): 2.054 mg/g

Total Terpenoids (%): 0.2054%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume. To see more detail for terpenoid content, view the PhytoFacts report.

Limonene 0.0357%
A monoterpene with a fragrance that can be described as orangey, citrusy, sweet and tart. It is most commonly found in nature as D-Limonene and is a primary contributor to the distinct scent of orange peels, from which it is commonly derived. Found in numerous pines, red maple, silver maple, aspens, cottonwoods, hemlocks, sumac, cedar, junipers...etc.

Myrcene 0.0345%
A monoterpene with a fragrance that can be described as peppery, spicy, herbal, floral and woody. Although it has a pleasant odor, it is typically used by the perfume industry as precursor for developing other fragrances. Found in hops, houttuynia, bay, thyme, lemon grass, mango, verbena, cardamom, citrus...etc.

β-Caryophyllene 0.0335%
A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB² receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

05/23/2024

Result Views

Table Bar Graph

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Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
Limonene	0.005 / 0.016	±0.0116	0.357	0.0357
Myrcene	0.007 / 0.025	±0.0122	0.345	0.0345
β-Caryophyllene	0.004 / 0.013	±0.0180	0.335	0.0335
Linalool	0.009 / 0.030	±0.0094	0.240	0.0240
Fenchol	0.009 / 0.029	±0.0060	0.162	0.0162
Terpineol	0.008 / 0.025	±0.0093	0.152	0.0152
α-Humulene	0.009 / 0.031	±0.0058	0.107	0.0107
α-Bisabolol	0.008 / 0.026	±0.0043	0.100	0.0100
β-Pinene	0.004 / 0.015	±0.0028	0.088	0.0088
Borneol	0.004 / 0.014	±0.0021	0.044	0.0044
α-Pinene	0.005 / 0.015	±0.0014	0.038	0.0038
Geraniol	0.002 / 0.007	±0.0017	0.032	0.0032
Nerolidol	0.006 / 0.020	±0.0025	0.032	0.0032
Citronellol	0.003 / 0.010	±0.0006	0.022	0.0022
Nerol	0.003 / 0.011	N/A	<LOQ	<LOQ
Camphene	0.004 / 0.014	N/A	<LOQ	<LOQ
Caryophyllene Oxide	0.011 / 0.038	N/A	<LOQ	<LOQ
trans-β-Farnesene	0.008 / 0.028	N/A	<LOQ	<LOQ
Cedrol	0.009 / 0.032	N/A	ND	ND
Guaiol	0.011 / 0.035	N/A	ND	ND
Camphor	0.005 / 0.015	N/A	ND	ND
Menthol	0.008 / 0.025	N/A	ND	ND
Fenchone	0.008 / 0.026	N/A	ND	ND
Pulegone	0.003 / 0.010	N/A	ND	ND
Sabinene	0.004 / 0.014	N/A	ND	ND
p-Cymene	0.005 / 0.015	N/A	ND	ND
Valencene	0.010 / 0.033	N/A	ND	ND
Eucalyptol	0.005 / 0.018	N/A	ND	ND
Isoborneol	0.003 / 0.011	N/A	ND	ND
Isopulegol	0.004 / 0.013	N/A	ND	ND
Terpinolene	0.008 / 0.027	N/A	ND	ND
β-Ocimene	0.005 / 0.018	N/A	ND	ND
Δ³-Carene	0.005 / 0.018	N/A	ND	ND
α-Cedrene	0.005 / 0.017	N/A	ND	ND
Geranyl Acetate	0.004 / 0.012	N/A	ND	ND
α-Terpinene	0.006 / 0.019	N/A	ND	ND
γ-Terpinene	0.005 / 0.018	N/A	ND	ND
Sabinene Hydrate	0.007 / 0.022	N/A	ND	ND
α-Phellandrene	0.006 / 0.019	N/A	ND	ND
TOTAL			2.054 mg/g	0.2054%

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Heavy Metals Analysis

Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

05/23/2024

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
Arsenic	0.02 / 0.1	0.2	N/A	ND	Pass
Cadmium	0.02 / 0.05	0.2	N/A	ND	Pass
Lead	0.04 / 0.1	0.5	N/A	ND	Pass
Mercury	0.002 / 0.01	0.1	N/A	ND	Pass

Microbiology Analysis

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants. And Analysis conducted by 3M^TM Petrifilm^TM and plate counts of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants and QSP 6794 - Plating with 3M^TM Petrifilm^TM

Microbiology Test Results (PLATING)

05/25/2024

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Compound	Result (cfu/g)
Total Yeast and Mold	ND

COA ID: 240520R008-002

These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

Sample Certification: California Code of Regulations Title 4 Division 19. Department of Cannabis Control Business and Professions Code. Reference: Sections 26100, 26104 and 26110, Business and Professions Code.

Decision Rule: Statements of conformity (e.g. Pass/Fail) to specifications are made in this report without taking measurement uncertainty into account. Where statements of conformity are made in this report, the following decision rules are applied: PASS - Results within limits/specifications, FAIL - Results exceed limits/specifications.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT), μg/g = ppm, μg/kg = ppb, too numerous to count >250 cfu/plate (TNTC), colony-forming unit (cfu)