Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

OBX SHIRLEY UL-L TEMPLE

Infused, Solid Edible

Date Issued:

05/20/2024

Total THC Not Detected
Total CBD 15.039 mg/unit
Sum Cannabinoids 15.332 mg/unit
Total Cannabinoids 15.332 mg/unit

Sample Information

Sample Details

Sample ID:240516M019

Batch Number:L.P.UL.GU.SHR.1.1.5MAY2024

Cultivator / Manufacturer

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Distributor / Tested For

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Cannabinoid Analysis - Summary

Total THC: Not Detected

Total CBD: 15.039 mg/unit

Sum of Cannabinoids: 15.332 mg/unit

Total Cannabinoids: 15.332 mg/unit

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Safety Analysis - Summary

Δ9-THC per Unit: Pass

Residual Solvents: Pass

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: Not Detected

(Δ9-THC+0.877*THCa)

Total CBD: 15.039 mg/unit

(CBD+0.877*CBDa)

Total Cannabinoids: 15.332 mg/unit

Total CBG: ND

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: ND

Total CBC (CBC+0.877*CBCa)

Total CBDV: <LOQ

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

05/19/2024

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
Cannabidiol (CBD) 0.004 / 0.011 ±0.1111 2.978 0.2978
Cannabinol (CBN) 0.001 / 0.007 ±0.0017 0.058 0.0058
Cannabidivarin (CBDV) 0.002 / 0.012 N/A <LOQ <LOQ
Cannabichromene (CBC) 0.003 / 0.010 N/A ND ND
Cannabigerol (CBG) 0.002 / 0.006 N/A ND ND
Cannabicyclol (CBL) 0.003 / 0.010 N/A ND ND
Cannabichromenic Acid (CBCa) 0.001 / 0.015 N/A ND ND
Cannabidiolic Acid (CBDa) 0.001 / 0.026 N/A ND ND
Cannabigerolic Acid (CBGa) 0.002 / 0.007 N/A ND ND
Tetrahydrocannabivarin (THCV) 0.002 / 0.012 N/A ND ND
Tetrahydrocannabinolic Acid (THCa) 0.001 / 0.005 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.001 / 0.018 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.002 / 0.019 N/A ND ND
∆8 Tetrahydrocannabinol (Δ8THC) 0.01 / 0.02 N/A ND ND
Δ9 Tetrahydrocannabinol (Δ9THC) 0.002 / 0.014 N/A ND ND
SUM OF CANNABINOIDS 3.036 mg/g 0.3036%
Unit Mass:

5.05 grams

Swipe left on table to see additional columns

Δ9-THC per Unit 110 per-package limit ND Pass
Total THC per Unit ND
CBD per Unit 15.039 mg/unit
Total CBD per Unit 15.039 mg/unit
Sum of Cannabinoids per Unit 15.332 mg/unit
Total Cannabinoids per Unit 15.332 mg/unit
Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

05/20/2024

PASS

Swipe left on table to see additional columns

Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Propane 0.234 / 0.781 5000 N/A ND Pass
2-Methylpropane (Isobutane) 0.052 / 0.173 N/A ND
n-Butane 0.019 / 0.063 5000 N/A ND Pass
Total Butanes ± ND
2-Methylbutane (Isopentane) 0.310 / 1.035 N/A ND
2,2-Dimethylpropane (Neopentane) 0.035 / 0.117 N/A ND
n-Pentane 0.310 / 1.033 5000 N/A ND Pass
Total Pentanes ± ND
2,2-Dimethylbutane (Neohexane) 9.831 / 32.77 N/A ND
2,3-Dimethylbutane / 2-Methylpentane (Isohexane) 0.381 / 1.271 N/A ND
3-Methylpentane 0.109 / 0.365 N/A ND
n-Hexane 0.110 / 0.366 290 N/A ND Pass
Total Hexanes ± ND
Cyclohexane 0.357 / 1.190 N/A ND
2,2-Dimethylpentane (Neoheptane) 0.493 / 1.642 N/A ND
2,3-Dimethylpentane 1.009 / 3.365 N/A ND
2,4-Dimethylpentane 0.737 / 2.458 N/A ND
3,3-Dimethylpentane 0.198 / 0.660 N/A ND
2,2,3-Trimethylbutane (Triptane) 0.521 / 1.738 N/A ND
2-Methylhexane (Isoheptane) 0.610 / 2.034 N/A ND
3-Methylhexane 0.235 / 0.785 N/A ND
3-Ethylpentane 0.304 / 1.012 N/A ND
n-Heptane 13.12 / 43.72 5000 N/A ND Pass
Total Heptanes ± ND
Cycloheptane 0.597 / 1.989 N/A ND
Benzene 0.089 / 0.295 1 N/A ND Pass
Toluene 0.115 / 0.382 890 N/A ND Pass
Cumene 0.180 / 0.600 N/A ND
1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene) 0.451 / 1.502 N/A ND
1,2-Dimethylbenzene (o-Xylene) 0.387 / 1.289 N/A ND
Ethylbenzene 0.370 / 1.233 N/A ND
Total Xylenes 2170 ± ND Pass
Methanol 53.92 / 163.4 3000 N/A ND Pass
Ethanol 8.984 / 27.23 5000 ±9.275 594.57 Pass
1-Propanol 1.540 / 5.133 N/A ND
2-Propanol (Isopropyl Alcohol) 8.421 / 25.52 5000 N/A ND Pass
1-Butanol 0.475 / 1.582 N/A ND
2-Butanol 7.248 / 24.16 N/A ND
1-Pentanol 1.461 / 4.869 N/A ND
Acetone 10.59 / 32.08 5000 N/A ND Pass
2-Butanone 0.169 / 0.564 N/A ND
Tetrahydrofuran 0.622 / 2.075 N/A ND
Ethyl Ether 0.197 / 0.658 5000 N/A ND Pass
Ethylene Glycol 3.803 / 12.68 N/A ND
2-Ethoxyethanol 1.235 / 4.118 N/A ND
1,2-Dimethoxyethane 2.116 / 7.052 N/A ND
1,4-Dioxane 0.468 / 1.558 N/A ND
Ethylene Oxide 0.253 / 0.844 1 N/A ND Pass
Ethyl Acetate 1.123 / 3.745 5000 N/A ND Pass
Isopropyl Acetate 0.347 / 1.158 N/A ND
Chloroform 0.251 / 0.838 1 N/A ND Pass
Dichloromethane (Methylene Chloride) 2.651 / 8.838 1 N/A ND Pass
Trichloroethylene 0.299 / 0.996 1 N/A ND Pass
1,2-Dichloroethane 0.162 / 0.541 1 N/A ND Pass
1,1-Dichloroethene 0.185 / 0.616 N/A ND
1,2-Dichloroethene 0.428 / 1.427 N/A ND
Sulfolane 47.66 / 158.9 N/A ND
Dimethyl Sulfoxide 6.168 / 20.56 N/A ND
Acetonitrile 1.595 / 4.833 410 N/A ND Pass
Pyridine 0.407 / 1.355 N/A ND
N,N-Dimethylacetamide 0.127 / 0.422 N/A ND
N,N-Dimethylformamide 0.946 / 3.153 N/A ND

Total Butanes = n-Butane + 2-Methylpropane (Isobutane)

Total Pentanes = n-Pentane + 2-Methylbutane (Isopentane) + 2,2-Dimethylpropane (Neopentane)

Total Hexanes = n-Hexane + 2,2-Dimethylbutane (Neohexane) + 2,3-Dimethylbutane / 2-Methylpentane (Isohexane) + 3-Methylpentane

Total Heptanes = 2,2-Dimethylpentane (Neoheptane) + 2,3-Dimethylpentane + 2,4-Dimethylpentane + 3,3-Dimethylpentane + 2,2,3-Trimethylbutane (Triptane) + 2-Methylhexane (Isoheptane) + 3-Methylhexane + 3-Ethylpentane + n-Heptane

Total Xylenes = 1,2-Dimethylbenzene (o-Xylene) + 1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene) + Ethylbenzene

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