440.022924.01B.Chunk

Certificate of Analysis

QUALITY ASSURANCE TEST ONLY - Not for retail sale

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Sample Name:

440.022924.01B.Chunk

Concentrate, Product Inhalable

Sum Cannabinoids 74.99%

Total Cannabinoids 66.60%

Total THC 64.798%

Total CBD 0.162%

Total Terpenoids 4.9911%
PhytoFacts^®

Top 3 Terpenoids

β-Caryophyllene 1.7354%
Linalool 0.5789%
α-Humulene 0.5556%

Sample Information

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Sample Details

Sample ID:240304N003

Batch Number:Live BHO (01)

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Cultivator / Manufacturer

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PhytoFacts® Report

aroma

flavor

effect

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The PhytoFacts chemometric report provides additional cannabinoid and terpenoid details, including dominant terpenes, entourage effects, aroma, flavor, and more.

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Cannabinoid Analysis - Summary

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Sum of Cannabinoids: 74.99%

Total Cannabinoids: 66.60%

Total THC: 64.798%

Total CBD: 0.162%

Sum of Cannabinoids = Δ⁹-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ⁸-THC + CBL + CBN

Total Cannabinoids = (Δ⁹-THC+0.877*THCa+Δ⁸-THC) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + CBL + CBN

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ⁹-THC + (THCa (0.877)) + Δ⁸-THC
Total CBD = CBD + (CBDa (0.877))

Why are Sum of Cannabinoids and Total Cannabinoids calculated separately?

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

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Total Terpenoids: 4.9911%

β-Caryophyllene (1.7354%)

Linalool (0.5789%)

α-Humulene (0.5556%)

Safety Analysis - Summary

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Pesticides: Pass

Heavy Metals: Pass

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Cannabinoid Analysis

Tested

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total Cannabinoids: 66.60%

Total THC: 64.798%

(Δ⁹-THC+0.877*THCa+Δ⁸-THC)

Total CBD: 0.162%

(CBD+0.877*CBDa)

Total CBG: 0.64%

Total CBG (CBG+0.877*CBGa)

Total THCV: 0.339%

Total THCV (THCV+0.877*THCVa)

Total CBC: 0.59%

Total CBC (CBC+0.877*CBCa)

Total CBDV: ND

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

03/07/2024

Result Views

Table Pie Chart

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Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
Tetrahydrocannabinolic Acid (THCa)	0.05 / 0.14	±13.299	664.96	66.496
Δ9 Tetrahydrocannabinol (Δ9THC)	0.06 / 0.26	±1.737	64.81	6.481
Cannabigerolic Acid (CBGa)	0.1 / 0.2	±0.24	5.9	0.59
Cannabichromenic Acid (CBCa)	0.07 / 0.28	±0.218	5.73	0.573
Tetrahydrocannabivarinic Acid (THCVa)	0.07 / 0.20	±0.143	3.86	0.386
Cannabidiolic Acid (CBDa)	0.02 / 0.19	±0.042	1.85	0.185
Cannabigerol (CBG)	0.06 / 0.19	±0.038	1.23	0.123
Cannabichromene (CBC)	0.2 / 0.5	±0.02	0.9	0.09
Cannabinol (CBN)	0.1 / 0.3	±0.04	0.7	0.07
Cannabidiol (CBD)	0.07 / 0.29	N/A	ND	ND
Cannabicyclol (CBL)	0.06 / 0.24	N/A	ND	ND
Cannabidivarin (CBDV)	0.04 / 0.15	N/A	ND	ND
Tetrahydrocannabivarin (THCV)	0.1 / 0.2	N/A	ND	ND
Cannabidivarinic Acid (CBDVa)	0.03 / 0.53	N/A	ND	ND
∆8 Tetrahydrocannabinol (Δ8THC)	0.1 / 0.4	N/A	ND	ND
SUM OF CANNABINOIDS			749.9 mg/g	74.99%

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpenoid Analysis

Tested

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

View PhytoFacts COA

See a visual representation of this sample's cannabinoid and terpenoid properties, including entourage effects, aroma, and flavor profile.

Summary

Total Terpenoids (mg/g): 49.911 mg/g

Total Terpenoids (%): 4.9911%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume. To see more detail for terpenoid content, view the PhytoFacts report.

β-Caryophyllene 1.7354%
A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB² receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

Linalool 0.5789%
A monoterpenoid alcohol with a fragrance that can be described as spicy, waxy, citrus and floral. It is commonly used as an insecticide against cockroaches, flies, fleas and other insects. Found in bail, lavender, cinnamon, hops, mugwort, goldenrods...etc.

α-Humulene 0.5556%
Also known as α-caryophyllene, it is an isomer of the sesquiterpene β-Caryophyllene which frequently occurs in nature with many aromatic plants across the globe. It has a fragrance that can be described as earthy or musky with spicy undertones. Found in hops, forskohlii, skullcaps, basil, nutmeg, cloves, sage, cotton, tamarind, black pepper, guava, Scotch pine...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

03/07/2024

Result Views

Table Bar Graph

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Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
β-Caryophyllene	0.004 / 0.012	±0.4807	17.354	1.7354
Linalool	0.009 / 0.032	±0.1714	5.789	0.5789
α-Humulene	0.009 / 0.029	±0.1389	5.556	0.5556
α-Bisabolol	0.008 / 0.026	±0.1831	4.412	0.4412
Limonene	0.005 / 0.016	±0.0464	4.177	0.4177
Myrcene	0.008 / 0.025	±0.0234	2.341	0.2341
Terpineol	0.009 / 0.031	±0.0964	2.016	0.2016
Fenchol	0.010 / 0.034	±0.0572	1.900	0.1900
β-Pinene	0.004 / 0.014	±0.0126	1.418	0.1418
Caryophyllene Oxide	0.010 / 0.033	±0.0346	0.966	0.0966
Valencene	0.009 / 0.030	±0.0438	0.818	0.0818
α-Pinene	0.005 / 0.017	±0.0052	0.777	0.0777
Borneol	0.005 / 0.016	±0.0193	0.590	0.0590
Citronellol	0.003 / 0.010	±0.0130	0.342	0.0342
trans-β-Farnesene	0.008 / 0.025	±0.0083	0.300	0.0300
Terpinolene	0.008 / 0.026	±0.0046	0.291	0.0291
Camphene	0.005 / 0.015	±0.0024	0.267	0.0267
Geraniol	0.002 / 0.007	±0.0072	0.210	0.0210
Fenchone	0.009 / 0.028	±0.0034	0.150	0.0150
Geranyl Acetate	0.004 / 0.014	±0.0028	0.085	0.0085
β-Ocimene	0.006 / 0.020	±0.0013	0.053	0.0053
Sabinene Hydrate	0.006 / 0.022	±0.0012	0.040	0.0040
Nerol	0.003 / 0.011	±0.0013	0.039	0.0039
γ-Terpinene	0.006 / 0.018	±0.0003	0.020	0.0020
Menthol	0.008 / 0.025	N/A	<LOQ	<LOQ
Isoborneol	0.004 / 0.012	N/A	<LOQ	<LOQ
α-Terpinene	0.005 / 0.017	N/A	<LOQ	<LOQ
α-Phellandrene	0.006 / 0.020	N/A	<LOQ	<LOQ
Cedrol	0.008 / 0.027	N/A	ND	ND
Guaiol	0.009 / 0.030	N/A	ND	ND
Camphor	0.006 / 0.019	N/A	ND	ND
Pulegone	0.003 / 0.011	N/A	ND	ND
Sabinene	0.004 / 0.014	N/A	ND	ND
p-Cymene	0.005 / 0.016	N/A	ND	ND
Nerolidol	0.006 / 0.019	N/A	ND	ND
Eucalyptol	0.006 / 0.018	N/A	ND	ND
Isopulegol	0.005 / 0.016	N/A	ND	ND
Δ³-Carene	0.005 / 0.018	N/A	ND	ND
α-Cedrene	0.005 / 0.016	N/A	ND	ND
TOTAL			49.911 mg/g	4.9911%

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Pesticide Analysis

Pass

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

03/07/2024

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
Aldicarb	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Carbofuran	0.02 / 0.05	≥ LOD	N/A	ND	Pass
Chlordane*	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Chlorfenapyr*	0.03 / 0.10	≥ LOD	N/A	ND	Pass
Chlorpyrifos	0.02 / 0.06	≥ LOD	N/A	ND	Pass
Coumaphos	0.02 / 0.07	≥ LOD	N/A	ND	Pass
Daminozide	0.02 / 0.07	≥ LOD	N/A	ND	Pass
Dichlorvos (DDVP)	0.03 / 0.09	≥ LOD	N/A	ND	Pass
Dimethoate	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Ethoprophos	0.03 / 0.10	≥ LOD	N/A	ND	Pass
Etofenprox	0.02 / 0.06	≥ LOD	N/A	ND	Pass
Fenoxycarb	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Fipronil	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Imazalil	0.02 / 0.06	≥ LOD	N/A	ND	Pass
Methiocarb	0.02 / 0.07	≥ LOD	N/A	ND	Pass
Mevinphos	0.03 / 0.09	≥ LOD	N/A	ND	Pass
Paclobutrazol	0.02 / 0.05	≥ LOD	N/A	ND	Pass
Parathion-methyl	0.03 / 0.10	≥ LOD	N/A	ND	Pass
Propoxur	0.03 / 0.09	≥ LOD	N/A	ND	Pass
Spiroxamine	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Thiacloprid	0.03 / 0.10	≥ LOD	N/A	ND	Pass
Abamectin	0.03 / 0.10	0.1	N/A	ND	Pass
Acephate	0.02 / 0.07	0.1	N/A	ND	Pass
Acequinocyl	0.02 / 0.07	0.1	N/A	ND	Pass
Acetamiprid	0.02 / 0.05	0.1	N/A	ND	Pass
Azoxystrobin	0.02 / 0.07	0.1	N/A	ND	Pass
Bifenazate	0.01 / 0.04	0.1	N/A	ND	Pass
Bifenthrin	0.02 / 0.05	3	±0.003	0.07	Pass
Boscalid	0.03 / 0.09	0.1	N/A	ND	Pass
Captan	0.19 / 0.57	0.7	N/A	ND	Pass
Carbaryl	0.02 / 0.06	0.5	N/A	ND	Pass
Chlorantraniliprole	0.04 / 0.12	10	N/A	ND	Pass
Clofentezine	0.03 / 0.09	0.1	N/A	ND	Pass
Cyfluthrin	0.12 / 0.38	2	N/A	ND	Pass
Cypermethrin	0.11 / 0.32	1	N/A	ND	Pass
Diazinon	0.02 / 0.05	0.1	N/A	ND	Pass
Dimethomorph	0.03 / 0.09	2	N/A	ND	Pass
Etoxazole	0.02 / 0.06	0.1	N/A	ND	Pass
Fenhexamid	0.03 / 0.09	0.1	N/A	ND	Pass
Fenpyroximate	0.02 / 0.06	0.1	N/A	ND	Pass
Flonicamid	0.03 / 0.10	0.1	N/A	ND	Pass
Fludioxonil	0.03 / 0.10	0.1	N/A	ND	Pass
Hexythiazox	0.02 / 0.07	0.1	N/A	ND	Pass
Imidacloprid	0.04 / 0.11	5	N/A	ND	Pass
Kresoxim-methyl	0.02 / 0.07	0.1	N/A	ND	Pass
Malathion	0.03 / 0.09	0.5	N/A	ND	Pass
Metalaxyl	0.02 / 0.07	2	N/A	ND	Pass
Methomyl	0.03 / 0.10	1	N/A	ND	Pass
Myclobutanil	0.03 / 0.09	0.1	N/A	ND	Pass
Naled	0.02 / 0.07	0.1	N/A	ND	Pass
Oxamyl	0.04 / 0.11	0.5	N/A	ND	Pass
Pentachloronitrobenzene (Quintozene)*	0.03 / 0.09	0.1	N/A	ND	Pass
Permethrin	0.04 / 0.12	0.5	N/A	ND	Pass
Phosmet	0.03 / 0.10	0.1	N/A	ND	Pass
Piperonyl Butoxide	0.02 / 0.07	3	N/A	ND	Pass
Prallethrin	0.03 / 0.08	0.1	N/A	ND	Pass
Propiconazole	0.02 / 0.07	0.1	N/A	ND	Pass
Pyrethrins	0.04 / 0.12	0.5	N/A	ND	Pass
Pyridaben	0.02 / 0.07	0.1	N/A	ND	Pass
Spinetoram	0.02 / 0.07	0.1	N/A	ND	Pass
Spinosad	0.02 / 0.07	0.1	N/A	ND	Pass
Spiromesifen	0.02 / 0.05	0.1	N/A	ND	Pass
Spirotetramat	0.02 / 0.06	0.1	N/A	ND	Pass
Tebuconazole	0.02 / 0.07	0.1	N/A	ND	Pass
Thiamethoxam	0.03 / 0.10	5	N/A	ND	Pass
Trifloxystrobin	0.03 / 0.08	0.1	N/A	ND	Pass

Heavy Metals Analysis

Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

03/07/2024

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
Arsenic	0.02 / 0.1	0.2	N/A	ND	Pass
Cadmium	0.02 / 0.05	0.2	N/A	ND	Pass
Lead	0.04 / 0.1	0.5	N/A	<LOQ	Pass
Mercury	0.002 / 0.01	0.1	N/A	ND	Pass

COA ID: 240304N003-001

For quality assurance purposes. Not a Regulatory Compliance Testing Certificate. These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

Sample Certification: California Code of Regulations Title 4 Division 19. Department of Cannabis Control Business and Professions Code. Reference: Sections 26100, 26104 and 26110, Business and Professions Code.

Decision Rule: Statements of conformity (e.g. Pass/Fail) to specifications are made in this report without taking measurement uncertainty into account. Where statements of conformity are made in this report, the following decision rules are applied: PASS - Results within limits/specifications, FAIL - Results exceed limits/specifications.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT), μg/g = ppm, μg/kg = ppb