Certificate of Analysis
QUALITY ASSURANCE TEST ONLY - Not for retail sale

Sample Name:

Ultra Refined

Concentrate, Product Inhalable

Date Issued:

04/02/2020

Overall Batch Result:

Pass

Sum Cannabinoids 92.7035%
Total Cannabinoids 92.7035%
Total THC 83.709%
Total CBD 1.6257%

Sample Information

Sample Details

Sample ID:200331N011

Batch Number:GLDSR2020003

Cultivator / Manufacturer

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Distributor / Tested For

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Cannabinoid Analysis - Summary

Sum of Cannabinoids: 92.7035%

Total Cannabinoids: 92.7035%

Total THC: 83.709%

Total CBD: 1.6257%

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Safety Analysis - Summary

Pesticides: Pass

Mycotoxins: Pass

Residual Solvents: Pass

Heavy Metals: Pass

Microbiology (PCR): Pass

Foreign Material: Pass

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total Cannabinoids: 92.7035%

Total THC: 83.709%

9-THC+0.877*THCa)

Total CBD: 1.6257%

(CBD+0.877*CBDa)

Total CBG: 3.4514%

Total CBG (CBG+0.877*CBGa)

Total THCV: 1.0825%

Total THCV (THCV+0.877*THCVa)

Total CBC: 1.8025%

Total CBC (CBC+0.877*CBCa)

Total CBDV: ND

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

04/02/2020

Result Views

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Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
Δ9 Tetrahydrocannabinol (Δ9THC) 0.052 / 0.158 ±28.7959 837.090 83.7090
Cannabigerol (CBG) 0.03 / 0.092 ±1.3599 34.514 3.4514
Cannabichromene (CBC) 0.031 / 0.094 ±0.5299 18.025 1.8025
Cannabidiol (CBD) 0.052 / 0.158 ±0.7527 16.257 1.6257
Tetrahydrocannabivarin (THCV) 0.023 / 0.069 ±0.5391 10.825 1.0825
Cannabinol (CBN) 0.052 / 0.157 ±0.6742 10.324 1.0324
∆8 Tetrahydrocannabinol (Δ8THC) 0.053 / 0.162 N/A ND ND
Tetrahydrocannabinolic Acid (THCa) 0.052 / 0.156 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.091 / 0.276 N/A ND ND
Cannabidiolic Acid (CBDa) 0.052 / 0.156 N/A ND ND
Cannabidivarin (CBDV) 0.021 / 0.063 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.037 / 0.111 N/A ND ND
Cannabigerolic Acid (CBGa) 0.044 / 0.133 N/A ND ND
Cannabicyclol (CBL) 0.13 / 0.393 N/A ND ND
Cannabichromenic Acid (CBCa) 0.129 / 0.392 N/A ND ND
SUM OF CANNABINOIDS 927.035 mg/g 92.7035%
Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Category 1 Pesticide Test Results

04/02/2020

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Aldicarb 0.030 / 0.091 ≥ LOD N/A ND Pass
Carbofuran 0.029 / 0.089 ≥ LOD N/A ND Pass
Chlordane* 0.032 / 0.097 ≥ LOD N/A ND Pass
Chlorfenapyr* 0.030 / 0.090 ≥ LOD N/A ND Pass
Chlorpyrifos 0.029 / 0.089 ≥ LOD N/A ND Pass
Coumaphos 0.029 / 0.089 ≥ LOD N/A ND Pass
Daminozide 0.030 / 0.091 ≥ LOD N/A ND Pass
Dichlorvos (DDVP) 0.029 / 0.089 ≥ LOD N/A ND Pass
Dimethoate 0.029 / 0.089 ≥ LOD N/A ND Pass
Ethoprophos 0.029 / 0.089 ≥ LOD N/A ND Pass
Etofenprox 0.029 / 0.089 ≥ LOD N/A ND Pass
Fenoxycarb 0.029 / 0.089 ≥ LOD N/A ND Pass
Fipronil 0.029 / 0.089 ≥ LOD N/A ND Pass
Imazalil 0.029 / 0.089 ≥ LOD N/A ND Pass
Methiocarb 0.029 / 0.089 ≥ LOD N/A ND Pass
Parathion-methyl 0.029 / 0.089 ≥ LOD N/A ND Pass
Mevinphos 0.029 / 0.089 ≥ LOD N/A ND Pass
Paclobutrazol 0.029 / 0.089 ≥ LOD N/A ND Pass
Propoxur 0.029 / 0.089 ≥ LOD N/A ND Pass
Spiroxamine 0.029 / 0.089 ≥ LOD N/A ND Pass
Thiacloprid 0.029 / 0.089 ≥ LOD N/A ND Pass
Category 2 Pesticide Test Results

04/02/2020

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Abamectin 0.030 / 0.091 0.1 N/A ND Pass
Acephate 0.013 / 0.039 0.1 N/A ND Pass
Acequinocyl 0.010 / 0.031 0.1 N/A ND Pass
Acetamiprid 0.013 / 0.038 0.1 N/A ND Pass
Azoxystrobin 0.015 / 0.047 0.1 N/A ND Pass
Bifenazate 0.012 / 0.035 0.1 N/A ND Pass
Bifenthrin 0.013 / 0.038 3 N/A ND Pass
Boscalid 0.008 / 0.023 0.1 N/A <LOQ Pass
Captan 0.099 / 0.300 0.7 N/A ND Pass
Carbaryl 0.014 / 0.043 0.5 N/A ND Pass
Chlorantraniliprole 0.020 / 0.061 10 N/A ND Pass
Clofentezine 0.009 / 0.027 0.1 N/A ND Pass
Cyfluthrin 0.099 / 0.299 2 N/A ND Pass
Cypermethrin 0.030 / 0.091 1 N/A ND Pass
Diazinon 0.009 / 0.027 0.1 N/A ND Pass
Dimethomorph 0.018 / 0.055 2 N/A ND Pass
Etoxazole 0.007 / 0.022 0.1 N/A ND Pass
Fenhexamid 0.015 / 0.045 0.1 N/A ND Pass
Fenpyroximate 0.012 / 0.036 0.1 N/A ND Pass
Flonicamid 0.022 / 0.066 0.1 N/A ND Pass
Fludioxonil 0.020 / 0.061 0.1 N/A ND Pass
Hexythiazox 0.009 / 0.027 0.1 N/A ND Pass
Imidacloprid 0.017 / 0.050 5 N/A ND Pass
Kresoxim-methyl 0.010 / 0.029 0.1 N/A ND Pass
Malathion 0.006 / 0.019 0.5 N/A ND Pass
Metalaxyl 0.011 / 0.033 2 N/A ND Pass
Methomyl 0.022 / 0.067 1 N/A ND Pass
Myclobutanil 0.015 / 0.044 0.1 N/A ND Pass
Naled 0.010 / 0.031 0.1 N/A ND Pass
Oxamyl 0.014 / 0.042 0.5 N/A ND Pass
Pentachloronitrobenzene* 0.020 / 0.061 0.1 N/A ND Pass
Permethrin 0.027 / 0.082 0.5 N/A ND Pass
Phosmet 0.010 / 0.030 0.1 N/A ND Pass
Piperonyl Butoxide 0.007 / 0.020 3 N/A ND Pass
Prallethrin 0.011 / 0.032 0.1 N/A ND Pass
Propiconazole 0.004 / 0.013 0.1 N/A ND Pass
Pyrethrins 0.012 / 0.036 0.5 N/A ND Pass
Pyridaben 0.007 / 0.020 0.1 N/A ND Pass
Spinetoram 0.006 / 0.017 0.1 N/A ND Pass
Spinosad 0.010 / 0.031 0.1 N/A ND Pass
Spiromesifen 0.005 / 0.015 0.1 N/A ND Pass
Spirotetramat 0.014 / 0.042 0.1 N/A ND Pass
Tebuconazole 0.006 / 0.018 0.1 N/A ND Pass
Thiamethoxam 0.011 / 0.033 5 N/A ND Pass
Trifloxystrobin 0.007 / 0.020 0.1 N/A ND Pass

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS

Mycotoxin Test Results

04/01/2020

PASS

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Compound LOD/LOQ
(μg/kg)
Action Limit
(μg/kg)
Measurement
Uncertainty
(μg/kg)
Result
(μg/kg)
Result
Aflatoxin B1 1.0 / 3.0 20 N/A ND Pass
Aflatoxin B2 2.0 / 6.0 20 N/A ND Pass
Aflatoxin G1 1.0 / 3.0 20 N/A ND Pass
Aflatoxin G2 2.0 / 6.0 20 N/A ND Pass
Total Aflatoxin 20 ± ND Pass
Ochratoxin A 6.0 / 18.0 20 N/A ND Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Category 1 Residual Solvents Test Results

04/02/2020

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
1,2-Dichloroethane 0.111 / 0.336 1 N/A ND Pass
Benzene 0.043 / 0.132 1 N/A ND Pass
Chloroform 0.064 / 0.195 1 N/A ND Pass
Ethylene Oxide 0.136 / 0.413 1 N/A ND Pass
Dichloromethane (Methylene Chloride) 0.172 / 0.521 1 N/A ND Pass
Trichloroethylene 0.040 / 0.120 1 N/A ND Pass
Category 2 Residual Solvents Test Results

04/02/2020

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Acetone 14.703 / 44.549 5000 N/A ND Pass
Acetonitrile 2.727 / 8.262 410 N/A ND Pass
n-Butane 5.672 / 17.185 5000 N/A ND Pass
Ethanol 11.775 / 35.679 5000 N/A ND Pass
Ethyl Acetate 16.227 / 49.169 5000 N/A ND Pass
Ethyl Ether 11.608 / 35.172 5000 N/A ND Pass
n-Heptane 12.982 / 39.336 5000 N/A ND Pass
n-Hexane 1.816 / 5.502 290 N/A ND Pass
2-Propanol (Isopropyl Alcohol) 15.358 / 46.536 5000 N/A ND Pass
Methanol 15.584 / 47.220 3000 N/A ND Pass
n-Pentane 12.355 / 37.434 5000 N/A ND Pass
Propane 1.359 / 4.117 5000 N/A ND Pass
Toluene 7.174 / 21.736 890 N/A ND Pass
Total Xylenes 34.438 / 104.347 2170 N/A ND Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

04/01/2020

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Arsenic 0.013 / 0.039 0.2 N/A ND Pass
Cadmium 0.012 / 0.035 0.2 N/A ND Pass
Lead 0.031 / 0.095 0.5 N/A ND Pass
Mercury 0.002 / 0.005 0.1 N/A ND Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants

Microbiology Test Results (PCR)

04/02/2020

PASS

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Compound Action Limit Result Result
Shiga toxin-producing Escherichia coli Detect ND Pass
Salmonella spp. Detect ND Pass
Aspergillus fumigatus Detect ND Pass
Aspergillus flavus Detect ND Pass
Aspergillus niger Detect ND Pass
Aspergillus terreus Detect ND Pass

Visual analysis includes, but is not limited to, sand, soil, cinders, dirt, mold, hair, insect fragments, and mammalian excreta.

Method: QSP 1226 - Analysis of Foreign Material in Cannabis and Cannabis Products

Foreign Material Test Results

04/01/2020

PASS

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Compound Action Limit Result Result
Total Sample Area Covered by Sand, Soil, Cinders, or Dirt >25% None Pass
Total Sample Area Covered by Mold >25% None Pass
Total Sample Area Covered by an Imbedded Foreign Material >25% None Pass
Insect Fragment Count > 1 per 3 grams 0.0 Pass
Hair Count > 1 per 3 grams 0.0 Pass
Mammalian Excreta Count > 1 per 3 grams 0.0 Pass

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