Frosted Kush 13

Certificate of Analysis

HEMP QUALITY ASSURANCE TEST

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Sample Name:

Frosted Kush 13

Flower, Inhalable

Total THC 0.6512%

Total CBD 17.2166%

Sum Cannabinoids 22.4745%

Total Cannabinoids 19.7739%

Total Terpenoids 2.2873%

Top 3 Terpenoids

Myrcene 0.9587%
β-Caryophyllene 0.6589%
α-Humulene 0.1656%

Sample Information

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Sample Details

Sample ID:191119D005

Batch Number:

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Cannabinoid Analysis - Summary

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Total THC: 0.6512%

Total CBD: 17.2166%

Sum of Cannabinoids: 22.4745%

Total Cannabinoids: 19.7739%

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ⁹-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ⁹-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ⁸-THC + CBL + CBN

Total Cannabinoids = (Δ⁹-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ⁸-THC + CBL + CBN

Why are Sum of Cannabinoids and Total Cannabinoids calculated separately?

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

36 tested, Top 3 Highlighted

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Total Terpenoids: 2.2873%

Myrcene (0.9587%)

β-Caryophyllene (0.6589%)

α-Humulene (0.1656%)

Safety Analysis - Summary

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Pesticides: Pass

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Cannabinoid Analysis

Tested

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 0.6512%

(Δ⁹-THC+0.877*THCa)

Total CBD: 17.2166%

(CBD+0.877*CBDa)

Total Cannabinoids: 19.7739%

Total CBG: 0.5082%

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 1.3316%

Total CBC (CBC+0.877*CBCa)

Total CBDV: 0.0663%

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

11/22/2019

Result Views

Table Pie Chart

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Compound	LOD/LOQ (mg/g)	Result (mg/g)	Result (%)
Cannabidiolic Acid (CBDa)	0.052 / 0.156	192.269	19.2269
Cannabichromenic Acid (CBCa)	0.233 / 0.705	14.540	1.4540
Tetrahydrocannabinolic Acid (THCa)	0.052 / 0.156	6.877	0.6877
Cannabigerolic Acid (CBGa)	0.034 / 0.102	5.121	0.5121
Cannabidiol (CBD)	0.059 / 0.180	3.546	0.3546
Cannabidivarinic Acid (CBDVa)	0.030 / 0.090	0.756	0.0756
Cannabigerol (CBG)	0.048 / 0.144	0.591	0.0591
Cannabichromene (CBC)	0.048 / 0.146	0.564	0.0564
Δ9 Tetrahydrocannabinol (Δ9THC)	0.052 / 0.158	0.481	0.0481
∆8 Tetrahydrocannabinol (Δ8THC)	0.074 / 0.224	ND	ND
Tetrahydrocannabivarin (THCV)	0.045 / 0.137	ND	ND
Tetrahydrocannabivarinic Acid (THCVa)	0.088 / 0.267	ND	ND
Cannabidivarin (CBDV)	0.027 / 0.080	ND	ND
Cannabicyclol (CBL)	0.114 / 0.346	ND	ND
Cannabinol (CBN)	0.052 / 0.157	ND	ND
SUM OF CANNABINOIDS		224.745 mg/g	22.4745%

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpenoid Analysis

Tested

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

Summary

Total Terpenoids (mg/g): 22.873 mg/g

Total Terpenoids (%): 2.2873%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume.

Myrcene 0.9587%
A monoterpene with a fragrance that can be described as peppery, spicy, herbal, floral and woody. Although it has a pleasant odor, it is typically used by the perfume industry as precursor for developing other fragrances. Found in hops, houttuynia, bay, thyme, lemon grass, mango, verbena, cardamom, citrus...etc.

β-Caryophyllene 0.6589%
A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB² receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

α-Humulene 0.1656%
Also known as α-caryophyllene, it is an isomer of the sesquiterpene β-Caryophyllene which frequently occurs in nature with many aromatic plants across the globe. It has a fragrance that can be described as earthy or musky with spicy undertones. Found in hops, forskohlii, skullcaps, basil, nutmeg, cloves, sage, cotton, tamarind, black pepper, guava, Scotch pine...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

11/23/2019

Result Views

Table Bar Graph

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Compound	LOD/LOQ (mg/g)	Result (mg/g)	Result (%)
Myrcene	0.03 / 0.092	9.587	0.9587
β-Caryophyllene	0.029 / 0.087	6.589	0.6589
α-Humulene	0.017 / 0.051	1.656	0.1656
Limonene	0.04 / 0.12	1.35	0.135
α-Bisabolol	0.057 / 0.172	1.188	0.1188
Guaiol	0.035 / 0.106	0.827	0.0827
Linalool	0.043 / 0.13	0.35	0.035
β-Pinene	0.016 / 0.048	0.221	0.0221
Caryophyllene Oxide	0.011 / 0.034	0.209	0.0209
Nerolidol	0.05 / 0.15	0.19	0.019
Fenchol	0.051 / 0.153	0.186	0.0186
α-Pinene	0.028 / 0.084	0.164	0.0164
Terpineol	0.029 / 0.087	0.162	0.0162
α-Cedrene	0.012 / 0.035	0.137	0.0137
Valencene	0.018 / 0.055	0.057	0.0057
Borneol	0.063 / 0.19	<LOQ	<LOQ
Camphene	0.038 / 0.116	ND	ND
Sabinene	0.024 / 0.073	ND	ND
α-Phellandrene	0.048 / 0.144	ND	ND
Δ³-Carene	0.028 / 0.085	ND	ND
α-Terpinene	0.051 / 0.155	ND	ND
Eucalyptol	0.051 / 0.155	ND	ND
β-Ocimene	0.053 / 0.16	ND	ND
γ-Terpinene	0.038 / 0.114	ND	ND
Sabinene Hydrate	0.046 / 0.138	ND	ND
Fenchone	0.06 / 0.181	ND	ND
Terpinolene	0.042 / 0.128	ND	ND
Isopulegol	0.026 / 0.08	ND	ND
Camphor	0.08 / 0.242	ND	ND
Isoborneol	0.028 / 0.085	ND	ND
Menthol	0.043 / 0.129	ND	ND
Nerol	0.042 / 0.128	ND	ND
Pulegone	0.016 / 0.047	ND	ND
Geraniol	0.037 / 0.112	ND	ND
Geranyl Acetate	0.025 / 0.076	ND	ND
Cedrol	0.022 / 0.066	ND	ND
TOTAL		22.873 mg/g	2.2873%

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Pesticide Analysis

Pass

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

11/22/2019

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Result (μg/g)	Result
Abamectin	0.030 / 0.091	0.1	ND	Pass
Bifenazate	0.012 / 0.035	0.1	ND	Pass
Bifenthrin	0.013 / 0.038	3.0	ND	Pass
Boscalid	0.008 / 0.023	0.1	ND	Pass
Etoxazole	0.007 / 0.022	0.1	ND	Pass
Imidacloprid	0.017 / 0.050	5.0	ND	Pass
Myclobutanil	0.015 / 0.044	0.1	ND	Pass
Piperonyl Butoxide	0.007 / 0.020	3.0	ND	Pass
Pyrethrins	0.012 / 0.036	0.5	ND	Pass
Spinosad	0.010 / 0.031	0.1	ND	Pass
Spiromesifen	0.005 / 0.015	0.1	ND	Pass
Spirotetramat	0.014 / 0.042	0.1	ND	Pass

COA ID: 191119D005-003

For quality assurance purposes. Not a Regulatory Hemp Lab Test Report. These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

Sample Certification: California Code of Regulations Title 4 Division 19. Department of Cannabis Control Business and Professions Code. Reference: Sections 26100, 26104 and 26110, Business and Professions Code.

Decision Rule: Statements of conformity (e.g. Pass/Fail) to specifications are made in this report without taking measurement uncertainty into account. Where statements of conformity are made in this report, the following decision rules are applied: PASS - Results within limits/specifications, FAIL - Results exceed limits/specifications.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT)