Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

Live Resin (LR) 1

Concentrate, Product Inhalable

Date Issued:

01/06/2020

Total THC 0.187%
Total CBD 62.4844%
Sum Cannabinoids 63.5221%
Total Cannabinoids 63.5221%
Total Terpenoids 1.8367%
Top 3 Terpenoids
  1. α-Bisabolol 1.0787%
  2. Guaiol 0.3088%
  3. β-Caryophyllene 0.2156%

Sample Information

Sample Details

Sample ID:191004P012

Batch Number:

Cultivator / Manufacturer

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Distributor / Tested For

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Cannabinoid Analysis - Summary

Total THC: 0.187%

Total CBD: 62.4844%

Sum of Cannabinoids: 63.5221%

Total Cannabinoids: 63.5221%

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

36 tested, Top 3 Highlighted

Total Terpenoids: 1.8367%

 
 
 

1

α-Bisabolol (1.0787%)

2

Guaiol (0.3088%)

3

β-Caryophyllene (0.2156%)

Safety Analysis - Summary

Pesticides: Pass

Residual Solvents: Pass

Heavy Metals: Pass

Microbiology (PCR): Pass

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 0.187%

9-THC+0.877*THCa)

Total CBD: 62.4844%

(CBD+0.877*CBDa)

Total Cannabinoids: 63.5221%

Total CBG: 0.0893%

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 0.3044%

Total CBC (CBC+0.877*CBCa)

Total CBDV: 0.457%

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

10/06/2019

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Result
(mg/g)
Result
(%)
CBD 0.052 / 0.158 624.844 62.4844
CBDV 0.021 / 0.063 4.570 0.4570
CBC 0.031 / 0.094 3.044 0.3044
Δ9-THC 0.052 / 0.158 1.870 0.1870
CBG 0.030 / 0.092 0.893 0.0893
Δ8-THC 0.053 / 0.162 ND ND
THCa 0.052 / 0.156 ND ND
THCV 0.023 / 0.069 ND ND
THCVa 0.091 / 0.276 ND ND
CBDa 0.052 / 0.156 ND ND
CBDVa 0.037 / 0.111 ND ND
CBGa 0.044 / 0.133 ND ND
CBL 0.130 / 0.393 ND ND
CBN 0.052 / 0.157 ND ND
CBCa 0.129 / 0.392 ND ND
SUM OF CANNABINOIDS 635.221 mg/g 63.5221%
Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

Summary

Total Terpenoids (mg/g): 18.367 mg/g

Total Terpenoids (%): 1.8367%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume.

  1. α-Bisabolol 1.0787%

    A sesquiterpene alcohol with a fragrance that can be described as floral, peppery, sweet and clean. Found in chamomile, figwort, yarrow, skullcaps, lavender, ironwort, germander...etc.

  2. Guaiol 0.3088%

    A sesquiterpene alcohol with a fragrance that can be described as floral, piney, herbal and woody. Found in guaiacum, cypress pine, ginseng, melaleuca, goatweed, incense grass...etc.

  3. β-Caryophyllene 0.2156%

    A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB2 receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

10/08/2019

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Result
(mg/g)
Result
(%)
α-Bisabolol 0.034 / 0.102 10.787 1.0787
Guaiol 0.044 / 0.132 3.088 0.3088
β-Caryophyllene 0.036 / 0.108 2.156 0.2156
α-Humulene 0.025 / 0.076 0.667 0.0667
Myrcene 0.054 / 0.164 0.491 0.0491
Terpineol 0.045 / 0.136 0.308 0.0308
Cedrol 0.057 / 0.173 0.266 0.0266
Nerolidol 0.07 / 0.212 0.247 0.0247
Caryophyllene Oxide 0.055 / 0.167 0.239 0.0239
Limonene 0.026 / 0.078 0.118 0.0118
Eucalyptol 0.042 / 0.126 <LOQ <LOQ
Fenchol 0.045 / 0.138 <LOQ <LOQ
α-Pinene 0.044 / 0.135 ND ND
Camphene 0.053 / 0.16 ND ND
Sabinene 0.054 / 0.165 ND ND
β-Pinene 0.054 / 0.162 ND ND
α-Phellandrene 0.073 / 0.222 ND ND
Δ3-Carene 0.057 / 0.174 ND ND
α-Terpinene 0.06 / 0.18 ND ND
β-Ocimene 0.056 / 0.171 ND ND
γ-Terpinene 0.06 / 0.181 ND ND
Sabinene Hydrate 0.036 / 0.108 ND ND
Fenchone 0.061 / 0.184 ND ND
Terpinolene 0.045 / 0.135 ND ND
Linalool 0.038 / 0.116 ND ND
Isopulegol 0.026 / 0.08 ND ND
Camphor 0.108 / 0.327 ND ND
Isoborneol 0.066 / 0.201 ND ND
Borneol 0.097 / 0.293 ND ND
Menthol 0.044 / 0.135 ND ND
Nerol 0.045 / 0.137 ND ND
Pulegone 0.045 / 0.135 ND ND
Geraniol 0.033 / 0.1 ND ND
Geranyl Acetate 0.031 / 0.095 ND ND
α-Cedrene 0.034 / 0.102 ND ND
Valencene 0.015 / 0.046 ND ND
TOTAL 18.367 mg/g 1.8367%
Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

10/06/2019

PASS

Swipe left on table to see additional columns

Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Result
(μg/g)
Result
Abamectin 0.030 / 0.091 0.1 ND Pass
Bifenazate 0.012 / 0.035 0.1 ND Pass
Bifenthrin 0.013 / 0.038 3.0 ND Pass
Boscalid 0.008 / 0.023 0.1 ND Pass
Etoxazole 0.007 / 0.022 0.1 ND Pass
Imidacloprid 0.017 / 0.050 5.0 ND Pass
Myclobutanil 0.015 / 0.044 0.1 ND Pass
Piperonyl Butoxide 0.007 / 0.020 3.0 ND Pass
Pyrethrins 0.012 / 0.036 0.5 ND Pass
Spinosad 0.010 / 0.031 0.1 ND Pass
Spiromesifen 0.005 / 0.015 0.1 ND Pass
Spirotetramat 0.014 / 0.042 0.1 ND Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

10/06/2019

PASS

Swipe left on table to see additional columns

Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Result
(μg/g)
Result
2-Propanol (Isopropyl Alcohol) 15.358 / 46.536 5000.0 ND Pass
Acetone 14.703 / 44.549 5000.0 <LOQ Pass
Acetonitrile 2.727 / 8.262 410.0 ND Pass
Ethanol 11.775 / 35.679 5000.0 <LOQ Pass
Ethyl Acetate 16.227 / 49.169 5000.0 ND Pass
Ethyl Ether 11.608 / 35.172 5000.0 ND Pass
Methanol 15.584 / 47.220 3000.0 ND Pass
n-Butane 5.672 / 17.185 5000.0 ND Pass
n-Heptane 12.982 / 39.336 5000.0 ND Pass
n-Hexane 1.816 / 5.502 290.0 ND Pass
n-Pentane 12.355 / 37.434 5000.0 ND Pass
Propane 1.359 / 4.117 5000.0 ND Pass
Toluene 7.174 / 21.736 890.0 ND Pass
Total Xylenes 34.438 / 104.347 2170.0 ND Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

10/07/2019

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Result
(μg/g)
Result
Arsenic 0.013 / 0.039 0.2 ND Pass
Cadmium 0.012 / 0.035 0.2 ND Pass
Lead 0.031 / 0.095 0.5 ND Pass
Mercury 0.002 / 0.005 0.1 ND Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants

Microbiology Test Results (PCR)

10/07/2019

PASS

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Compound Action Limit Result Result
Shiga toxin-producing Escherichia coli ND ND Pass
Salmonella spp. ND ND Pass
Aspergillus fumigatus ND ND Pass
Aspergillus flavus ND ND Pass
Aspergillus niger ND ND Pass
Aspergillus terreus ND ND Pass

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