Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

Full Spec C02 Oil

Infused, Liquid Edible

Date Issued:

01/06/2020

Total THC 1.791 mg/unit
Total CBD 54.842 mg/unit
Sum Cannabinoids 60.777 mg/unit
Total Cannabinoids 58.130 mg/unit
Total Terpenoids 0.113%
Top 3 Terpenoids
  1. α-Bisabolol 0.049%
  2. Guaiol 0.022%
  3. β-Caryophyllene 0.020%

Sample Information

Sample Details

Sample ID:190219T034

Batch Number:

Cultivator / Manufacturer

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Distributor / Tested For

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Cannabinoid Analysis - Summary

Total THC: 1.791 mg/unit

Total CBD: 54.842 mg/unit

Sum of Cannabinoids: 60.777 mg/unit

Total Cannabinoids: 58.130 mg/unit

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

35 tested, Top 3 Highlighted

Total Terpenoids: 0.113%

 
 
 

1

α-Bisabolol (0.049%)

2

Guaiol (0.022%)

3

β-Caryophyllene (0.020%)

Safety Analysis - Summary

Δ9-THC per Unit: Pass

Pesticides: Pass

Residual Solvents: Pass

Heavy Metals: Pass

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 1.791 mg/unit

9-THC+0.877*THCa)

Total CBD: 54.842 mg/unit

(CBD+0.877*CBDa)

Total Cannabinoids: 58.130 mg/unit

Total CBG: 0.995 mg/unit

Total CBG (CBG+0.877*CBGa)

Total CBDV: 0.387 mg/unit

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

02/22/2019

Result Views

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Compound LOD/LOQ
(mg/g)
Result
(mg/g)
Result
(%)
CBD 0.000057 / 0.001 50.300 5.0300
CBDa 0.000038 / 0.001 5.179 0.5179
CBC 0.000095 / 0.001 2.006 0.2006
Δ9-THC 0.000034 / 0.001 1.791 0.1791
CBG 0.000086 / 0.001 0.970 0.0970
CBDV 0.000065 / 0.001 0.387 0.0387
CBN 0.000029 / 0.001 0.115 0.0115
CBGa 0.000072 / 0.001 0.029 0.0029
Δ8-THC 0.000083 / 0.001 ND ND
THCa 0.000066 / 0.001 ND ND
THCV 0.000035 / 0.001 ND ND
CBDVa 0.00003 / 0.001 ND ND
SUM OF CANNABINOIDS 60.777 mg/g 6.0777%
Unit Mass:

1 grams

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Δ9-THC per Unit 1000.0 per-package limit 1.791 mg/unit Pass
Total THC per Unit 1.791 mg/unit
CBD per Unit 50.300 mg/unit
Total CBD per Unit 54.842 mg/unit
Sum of Cannabinoids per Unit 60.777 mg/unit
Total Cannabinoids per Unit 58.130 mg/unit
Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

Summary

Total Terpenoids (mg/g): 1.13 mg/g

Total Terpenoids (%): 0.113%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume.

  1. α-Bisabolol 0.049%

    A sesquiterpene alcohol with a fragrance that can be described as floral, peppery, sweet and clean. Found in chamomile, figwort, yarrow, skullcaps, lavender, ironwort, germander...etc.

  2. Guaiol 0.022%

    A sesquiterpene alcohol with a fragrance that can be described as floral, piney, herbal and woody. Found in guaiacum, cypress pine, ginseng, melaleuca, goatweed, incense grass...etc.

  3. β-Caryophyllene 0.020%

    A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB2 receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

02/24/2019

Result Views

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Compound LOD/LOQ
(mg/g)
Result
(mg/g)
Result
(%)
α-Bisabolol 0.02 / 0.07 0.49 0.049
Guaiol 0.02 / 0.07 0.22 0.022
β-Caryophyllene 0.02 / 0.07 0.20 0.020
Phytol 0.02 / 0.07 0.12 0.012
α-Humulene 0.02 / 0.07 0.10 0.010
Nerolidol 0.02 / 0.07 <LOQ <LOQ
Caryophyllene Oxide 0.02 / 0.07 <LOQ <LOQ
α-Pinene 0.02 / 0.07 ND ND
Camphene 0.02 / 0.07 ND ND
Sabinene 0.02 / 0.07 ND ND
β-Pinene 0.02 / 0.07 ND ND
Myrcene 0.02 / 0.07 ND ND
α-Phellandrene 0.02 / 0.07 ND ND
Δ3-Carene 0.02 / 0.07 ND ND
α-Terpinene 0.02 / 0.07 ND ND
Limonene 0.02 / 0.07 ND ND
Eucalyptol 0.02 / 0.07 ND ND
β-Ocimene 0.02 / 0.07 ND ND
γ-Terpinene 0.02 / 0.07 ND ND
Terpinolene 0.02 / 0.07 ND ND
Linalool 0.02 / 0.07 ND ND
Fenchol 0.02 / 0.07 ND ND
Isopulegol 0.02 / 0.07 ND ND
Camphor 0.02 / 0.07 ND ND
Isoborneol 0.02 / 0.07 ND ND
Borneol 0.02 / 0.07 ND ND
Menthol 0.02 / 0.07 ND ND
Terpineol 0.02 / 0.07 ND ND
Pulegone 0.02 / 0.07 ND ND
Geraniol 0.02 / 0.07 ND ND
Geranyl Acetate 0.02 / 0.07 ND ND
α-Cedrene 0.02 / 0.07 ND ND
Valencene 0.02 / 0.07 ND ND
p-Cymene 0.02 / 0.07 ND ND
Citronellol 0.02 / 0.07 ND ND
TOTAL 1.13 mg/g 0.113%
Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

02/27/2019

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Result
(μg/g)
Result
Abamectin 0.018935714 / 0.05 0.3 ND Pass
Bifenazate 0.037841667 / 0.05 5.0 ND Pass
Bifenthrin 0.002467857 / 0.25 0.5 ND Pass
Boscalid 0.000589252 / 0.05 10.0 ND Pass
Etoxazole 0.0000809524 / 0.05 1.5 ND Pass
Imidacloprid 0.01730119 / 1.5 3.0 ND Pass
Myclobutanil 0.00497619 / 0.05 9.0 ND Pass
Piperonyl Butoxide 0.000960714 / 1.5 8.0 ND Pass
Pyrethrins 0.005771429 / 0.25 1.0 ND Pass
Spinosad 0.016063095 / 0.05 3.0 ND Pass
Spiromesifen 0.047424914 / 0.05 12.0 ND Pass
Spirotetramat 0.056707143 / 0.05 13.0 ND Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

02/21/2019

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Result
(μg/g)
Result
2-Propanol (Isopropyl Alcohol) 74.61 / 218.59 5000.0 ND Pass
Acetone 371.43 / 1088.28 5000.0 ND Pass
Acetonitrile 0.657 / 1.925 410.0 ND Pass
Ethanol 149.81 / 438.94 5000.0 ND Pass
Ethyl Acetate 149.48 / 437.97 5000.0 ND Pass
Ethyl Ether 375.12 / 1099.1 5000.0 ND Pass
Methanol 96.47 / 282.66 3000.0 ND Pass
n-Butane 107.06 / 313.69 5000.0 ND Pass
n-Heptane 149.21 / 437.17 5000.0 ND Pass
n-Hexane 18.5 / 54.22 290.0 ND Pass
n-Pentane 149.25 / 437.31 5000.0 ND Pass
Propane 106.66 / 312.5 5000.0 ND Pass
Toluene 7.107 / 20.82 890.0 ND Pass
Total Xylenes 1.387 / 4.065 2170.0 ND Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

02/23/2019

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Result
(μg/g)
Result
Arsenic 0.0032 / 0.01 1.5 ND Pass
Cadmium 0.0032 / 0.01 0.5 ND Pass
Lead 0.0080 / 0.025 0.5 ND Pass
Mercury 0.0025 / 0.008 3.0 ND Pass

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