Nightly Drops

Certificate of Analysis

HEMP QUALITY ASSURANCE TEST

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Sample Name:

Nightly Drops

Infused, Non-Inhalable

Total THC 30.450 mg/unit

Total CBD 793.500 mg/unit

Sum Cannabinoids 859.170 mg/unit

Total Cannabinoids 859.170 mg/unit

Total Terpenoids 0.153%

Top 3 Terpenoids

α-Bisabolol 0.054%
β-Caryophyllene 0.030%
Myrcene 0.018%

Sample Information

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Sample Details

Sample ID:201209U003

Batch Number:T-32320-B4

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Cannabinoid Analysis - Summary

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Total THC: 30.450 mg/unit

Total CBD: 793.500 mg/unit

Sum of Cannabinoids: 859.170 mg/unit

Total Cannabinoids: 859.170 mg/unit

Density:0.9498 g/mL

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ⁹-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ⁹-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ⁸-THC + CBL + CBN

Total Cannabinoids = (Δ⁹-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ⁸-THC + CBL + CBN

Why are Sum of Cannabinoids and Total Cannabinoids calculated separately?

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

36 tested, Top 3 Highlighted

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Total Terpenoids: 0.153%

α-Bisabolol (0.054%)

β-Caryophyllene (0.030%)

Myrcene (0.018%)

Safety Analysis - Summary

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Δ⁹-THC per Unit: Pass

Pesticides: Pass

Residual Solvents: Pass

Heavy Metals: Pass

View Complete Test Results:

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Cannabinoid Analysis

Tested

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 30.450 mg/unit

(Δ⁹-THC+0.877*THCa)

Total CBD: 793.500 mg/unit

(CBD+0.877*CBDa)

Total Cannabinoids: 859.170 mg/unit

Total CBG: 9.780 mg/unit

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 21.780 mg/unit

Total CBC (CBC+0.877*CBCa)

Total CBDV: 1.650 mg/unit

Total CBDV (CBDV+0.877*CBDVa)

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The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

12/11/2020

Result Views

Table Pie Chart

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Compound	LOD/LOQ (mg/mL)	Measurement Uncertainty (mg/mL)	Result (mg/mL)	Result (%)
Cannabidiol (CBD)	0.004 / 0.011	±1.2670	26.450	2.7848
Δ9 Tetrahydrocannabinol (Δ9THC)	0.002 / 0.005	±0.0716	1.015	0.1069
Cannabichromene (CBC)	0.003 / 0.010	±0.0301	0.726	0.0764
Cannabigerol (CBG)	0.002 / 0.005	±0.0203	0.326	0.0343
Cannabidivarin (CBDV)	0.002 / 0.007	±0.0029	0.055	0.0058
Cannabicyclol (CBL)	0.003 / 0.008	±0.0020	0.042	0.0044
Cannabinol (CBN)	0.001 / 0.004	±0.0009	0.025	0.0026
∆8 Tetrahydrocannabinol (Δ8THC)	0.01 / 0.02	N/A	ND	ND
Tetrahydrocannabinolic Acid (THCa)	0.001 / 0.002	N/A	ND	ND
Tetrahydrocannabivarin (THCV)	0.002 / 0.008	N/A	ND	ND
Tetrahydrocannabivarinic Acid (THCVa)	0.002 / 0.005	N/A	ND	ND
Cannabidiolic Acid (CBDa)	0.001 / 0.003	N/A	ND	ND
Cannabidivarinic Acid (CBDVa)	0.001 / 0.003	N/A	ND	ND
Cannabigerolic Acid (CBGa)	0.002 / 0.006	N/A	ND	ND
Cannabichromenic Acid (CBCa)	0.001 / 0.004	N/A	ND	ND
SUM OF CANNABINOIDS			28.639 mg/mL	3.0153%

Unit Mass:

30 milliliters

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Δ⁹-THC per Unit	1100 per-package limit	30.450 mg/unit	Pass
Total THC per Unit		30.450 mg/unit
CBD per Unit		793.500 mg/unit
Total CBD per Unit		793.500 mg/unit
Sum of Cannabinoids per Unit		859.170 mg/unit
Total Cannabinoids per Unit		859.170 mg/unit

Density Test Result

0.9498 g/mL Tested 12/11/2020 Method: QSP 7870 - Sample Preparation

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpenoid Analysis

Tested

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

Summary

Total Terpenoids (mg/g): 1.53 mg/g

Total Terpenoids (%): 0.153%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume.

α-Bisabolol 0.054%
A sesquiterpene alcohol with a fragrance that can be described as floral, peppery, sweet and clean. Found in chamomile, figwort, yarrow, skullcaps, lavender, ironwort, germander...etc.

β-Caryophyllene 0.030%
A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB² receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

Myrcene 0.018%
A monoterpene with a fragrance that can be described as peppery, spicy, herbal, floral and woody. Although it has a pleasant odor, it is typically used by the perfume industry as precursor for developing other fragrances. Found in hops, houttuynia, bay, thyme, lemon grass, mango, verbena, cardamom, citrus...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

12/11/2020

Result Views

Table Bar Graph

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Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
α-Bisabolol	0.02 / 0.07	±0.024	0.54	0.054
β-Caryophyllene	0.02 / 0.07	±0.014	0.30	0.030
Myrcene	0.04 / 0.11	±0.015	0.18	0.018
α-Humulene	0.02 / 0.05	±0.005	0.15	0.015
Guaiol	0.03 / 0.09	±0.008	0.14	0.014
Linalool	0.03 / 0.08	±0.006	0.12	0.012
Limonene	0.02 / 0.05	±0.004	0.10	0.010
α-Pinene	0.03 / 0.09	N/A	ND	ND
Camphene	0.04 / 0.11	N/A	ND	ND
Sabinene	0.04 / 0.11	N/A	ND	ND
β-Pinene	0.04 / 0.11	N/A	ND	ND
α-Phellandrene	0.05 / 0.1	N/A	ND	ND
Δ³-Carene	0.04 / 0.1	N/A	ND	ND
α-Terpinene	0.04 / 0.1	N/A	ND	ND
Eucalyptol	0.03 / 0.08	N/A	ND	ND
β-Ocimene	0.03 / 0.09	N/A	ND	ND
γ-Terpinene	0.04 / 0.1	N/A	ND	ND
Sabinene Hydrate	0.02 / 0.07	N/A	ND	ND
Fenchone	0.04 / 0.12	N/A	ND	ND
Terpinolene	0.03 / 0.09	N/A	ND	ND
Fenchol	0.03 / 0.09	N/A	ND	ND
Isopulegol	0.02 / 0.05	N/A	ND	ND
Camphor	0.1 / 0.2	N/A	ND	ND
Isoborneol	0.04 / 0.1	N/A	ND	ND
Borneol	0.1 / 0.2	N/A	ND	ND
Menthol	0.03 / 0.09	N/A	ND	ND
Terpineol	0.02 / 0.07	N/A	ND	ND
Nerol	0.03 / 0.09	N/A	ND	ND
Pulegone	0.03 / 0.09	N/A	ND	ND
Geraniol	0.02 / 0.07	N/A	ND	ND
Geranyl Acetate	0.02 / 0.06	N/A	ND	ND
α-Cedrene	0.02 / 0.07	N/A	ND	ND
Valencene	0.01 / 0.03	N/A	ND	ND
Nerolidol	0.3 / 0.8	N/A	ND	ND
Caryophyllene Oxide	0.04 / 0.11	N/A	ND	ND
Cedrol	0.04 / 0.11	N/A	ND	ND
TOTAL			1.53 mg/g	0.153%

Learn more

Pesticide Analysis

Pass

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

12/10/2020

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
Abamectin	0.03 / 0.10	0.3	N/A	ND	Pass
Azoxystrobin	0.01 / 0.04	40	N/A	ND	Pass
Bifenazate	0.01 / 0.02	5	N/A	ND	Pass
Bifenthrin	0.01 / 0.02	0.5	N/A	ND	Pass
Boscalid	0.02 / 0.06	10	N/A	ND	Pass
Chlorpyrifos	0.02 / 0.06	≥ LOD	N/A	ND	Pass
Cypermethrin	0.1 / 0.3	1	N/A	ND	Pass
Etoxazole	0.010 / 0.028	1.5	N/A	ND	Pass
Hexythiazox	0.01 / 0.04	2	N/A	ND	Pass
Imidacloprid	0.01 / 0.04	3	N/A	ND	Pass
Malathion	0.02 / 0.05	5	N/A	ND	Pass
Myclobutanil	0.03 / 0.1	9	N/A	ND	Pass
Permethrin	0.03 / 0.09	20	N/A	ND	Pass
Piperonyl Butoxide	0.003 / 0.009	8	N/A	<LOQ	Pass
Propiconazole	0.01 / 0.03	20	N/A	ND	Pass
Spiromesifen	0.02 / 0.05	12	N/A	ND	Pass
Tebuconazole	0.02 / 0.07	2	N/A	ND	Pass
Trifloxystrobin	0.01 / 0.03	30	N/A	ND	Pass

Residual Solvents Analysis

Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

12/11/2020

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
1,2-Dichloroethane	0.05 / 0.1	1	N/A	ND	Pass
Benzene	0.03 / 0.09	1	N/A	ND	Pass
Chloroform	0.1 / 0.2	1	N/A	ND	Pass
Ethylene Oxide	0.1 / 0.4	1	N/A	ND	Pass
Dichloromethane (Methylene Chloride)	0.3 / 0.9	1	N/A	ND	Pass
Trichloroethylene	0.1 / 0.3	1	N/A	ND	Pass
Acetone	20 / 50	5000	N/A	ND	Pass
Acetonitrile	2 / 7	410	N/A	ND	Pass
n-Butane	10 / 50	5000	N/A	ND	Pass
Ethanol	20 / 50	5000	±2.7	71	Pass
Ethyl Acetate	20 / 60	5000	N/A	ND	Pass
Ethyl Ether	20 / 50	5000	N/A	ND	Pass
n-Heptane	20 / 60	5000	N/A	ND	Pass
n-Hexane	2 / 5	290	N/A	ND	Pass
2-Propanol (Isopropyl Alcohol)	10 / 40	5000	N/A	ND	Pass
Methanol	50 / 200	3000	N/A	ND	Pass
n-Pentane	20 / 50	5000	N/A	ND	Pass
Propane	10 / 20	5000	N/A	ND	Pass
Toluene	7 / 21	890	N/A	ND	Pass
Total Xylenes	50 / 160	2170	N/A	ND	Pass

Heavy Metals Analysis

Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

12/11/2020

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
Arsenic	0.02 / 0.1	1.5	N/A	ND	Pass
Cadmium	0.02 / 0.05	0.5	N/A	ND	Pass
Lead	0.04 / 0.1	0.5	N/A	ND	Pass
Mercury	0.002 / 0.01	3	N/A	ND	Pass

COA ID: 201209U003-001

For quality assurance purposes. Not a Regulatory Hemp Lab Test Report. These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

Sample Certification: California Code of Regulations Title 4 Division 19. Department of Cannabis Control Business and Professions Code. Reference: Sections 26100, 26104 and 26110, Business and Professions Code.

Decision Rule: Statements of conformity (e.g. Pass/Fail) to specifications are made in this report without taking measurement uncertainty into account. Where statements of conformity are made in this report, the following decision rules are applied: PASS - Results within limits/specifications, FAIL - Results exceed limits/specifications.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT)