Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

Daily Drops

Infused, Non-Inhalable

Date Issued:

04/09/2020

Total THC 23.160 mg/unit
Total CBD 551.520 mg/unit
Sum Cannabinoids 598.860 mg/unit
Total Cannabinoids 598.710 mg/unit
Total Terpenoids 0.0552%
Top 3 Terpenoids
  1. β-Caryophyllene 0.0342%
  2. α-Bisabolol 0.0166%
  3. α-Humulene 0.0044%

Sample Information

Sample Details

Sample ID:200407L001

Batch Number:T-07220-B3

Cultivator / Manufacturer

Show Details

Distributor / Tested For

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Cannabinoid Analysis - Summary

Total THC: 23.160 mg/unit

Total CBD: 551.520 mg/unit

Sum of Cannabinoids: 598.860 mg/unit

Total Cannabinoids: 598.710 mg/unit

Density:0.949 g/mL

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

36 tested, Top 3 Highlighted

Total Terpenoids: 0.0552%

 
 
 

1

β-Caryophyllene (0.0342%)

2

α-Bisabolol (0.0166%)

3

α-Humulene (0.0044%)

Safety Analysis - Summary

Δ9-THC per Unit: Pass

Pesticides: Pass

Residual Solvents: Pass

Heavy Metals: Pass

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 23.160 mg/unit

9-THC+0.877*THCa)

Total CBD: 551.520 mg/unit

(CBD+0.877*CBDa)

Total Cannabinoids: 598.710 mg/unit

Total CBG: 6.390 mg/unit

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 14.460 mg/unit

Total CBC (CBC+0.877*CBCa)

Total CBDV: 1.170 mg/unit

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

04/08/2020

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/mL)
Measurement
Uncertainty
(mg/mL)
Result
(mg/mL)
Result
(%)
Cannabidiol (CBD) 0.0009 / 0.003 ±0.8790 18.351 1.9337
Δ9 Tetrahydrocannabinol (Δ9THC) 0.0009 / 0.003 ±0.0544 0.772 0.0813
Cannabichromene (CBC) 0.0011 / 0.003 ±0.0200 0.482 0.0508
Cannabigerol (CBG) 0.001 / 0.003 ±0.0132 0.213 0.0224
Cannabidivarin (CBDV) 0.0004 / 0.001 ±0.0020 0.039 0.0041
Cannabidiolic Acid (CBDa) 0.0009 / 0.003 ±0.0014 0.038 0.0040
Cannabicyclol (CBL) 0.0021 / 0.006 ±0.0017 0.035 0.0037
Cannabinol (CBN) 0.0009 / 0.003 ±0.0012 0.032 0.0034
∆8 Tetrahydrocannabinol (Δ8THC) 0.0009 / 0.003 N/A ND ND
Tetrahydrocannabinolic Acid (THCa) 0.0009 / 0.003 N/A ND ND
Tetrahydrocannabivarin (THCV) 0.0004 / 0.001 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.0013 / 0.004 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.0003 / 0.001 N/A ND ND
Cannabigerolic Acid (CBGa) 0.0008 / 0.002 N/A ND ND
Cannabichromenic Acid (CBCa) 0.0015 / 0.005 N/A ND ND
SUM OF CANNABINOIDS 19.962 mg/mL 2.1035%
Unit Mass:

30 milliliters

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Δ9-THC per Unit 1100 per-package limit 23.160 mg/unit Pass
Total THC per Unit 23.160 mg/unit
CBD per Unit 550.530 mg/unit
Total CBD per Unit 551.520 mg/unit
Sum of Cannabinoids per Unit 598.860 mg/unit
Total Cannabinoids per Unit 598.710 mg/unit
Density Test Result

0.949 g/mL Tested 04/08/2020 Method: QSP 7870 - Sample Preparation

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

Summary

Total Terpenoids (mg/g): 0.552 mg/g

Total Terpenoids (%): 0.0552%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume.

  1. β-Caryophyllene 0.0342%

    A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB2 receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

  2. α-Bisabolol 0.0166%

    A sesquiterpene alcohol with a fragrance that can be described as floral, peppery, sweet and clean. Found in chamomile, figwort, yarrow, skullcaps, lavender, ironwort, germander...etc.

  3. α-Humulene 0.0044%

    Also known as α-caryophyllene, it is an isomer of the sesquiterpene β-Caryophyllene which frequently occurs in nature with many aromatic plants across the globe. It has a fragrance that can be described as earthy or musky with spicy undertones. Found in hops, forskohlii, skullcaps, basil, nutmeg, cloves, sage, cotton, tamarind, black pepper, guava, Scotch pine...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

04/08/2020

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
β-Caryophyllene 0.018 / 0.054 ±0.0162 0.342 0.0342
α-Bisabolol 0.017 / 0.051 ±0.0074 0.166 0.0166
α-Humulene 0.013 / 0.038 ±0.0014 0.044 0.0044
Valencene 0.008 / 0.023 N/A <LOQ <LOQ
Guaiol 0.022 / 0.066 N/A <LOQ <LOQ
α-Pinene 0.022 / 0.067 N/A ND ND
Camphene 0.027 / 0.08 N/A ND ND
Sabinene 0.027 / 0.082 N/A ND ND
β-Pinene 0.027 / 0.081 N/A ND ND
Myrcene 0.027 / 0.082 N/A ND ND
α-Phellandrene 0.037 / 0.111 N/A ND ND
Δ3-Carene 0.029 / 0.087 N/A ND ND
α-Terpinene 0.03 / 0.09 N/A ND ND
Limonene 0.013 / 0.039 N/A ND ND
Eucalyptol 0.021 / 0.063 N/A ND ND
β-Ocimene 0.028 / 0.085 N/A ND ND
γ-Terpinene 0.03 / 0.09 N/A ND ND
Sabinene Hydrate 0.018 / 0.054 N/A ND ND
Fenchone 0.03 / 0.092 N/A ND ND
Terpinolene 0.022 / 0.067 N/A ND ND
Linalool 0.019 / 0.058 N/A ND ND
Fenchol 0.023 / 0.069 N/A ND ND
Isopulegol 0.013 / 0.04 N/A ND ND
Camphor 0.054 / 0.163 N/A ND ND
Isoborneol 0.033 / 0.101 N/A ND ND
Borneol 0.048 / 0.146 N/A ND ND
Menthol 0.022 / 0.067 N/A ND ND
Terpineol 0.022 / 0.068 N/A ND ND
Nerol 0.023 / 0.068 N/A ND ND
Pulegone 0.022 / 0.068 N/A ND ND
Geraniol 0.017 / 0.05 N/A ND ND
Geranyl Acetate 0.016 / 0.048 N/A ND ND
α-Cedrene 0.017 / 0.051 N/A ND ND
Nerolidol 0.035 / 0.106 N/A ND ND
Caryophyllene Oxide 0.028 / 0.084 N/A ND ND
Cedrol 0.029 / 0.086 N/A ND ND
TOTAL 0.552 mg/g 0.0552%
Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

04/09/2020

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Abamectin 0.030 / 0.091 0.3 N/A ND Pass
Azoxystrobin 0.015 / 0.047 40 N/A ND Pass
Bifenazate 0.012 / 0.035 5 N/A ND Pass
Bifenthrin 0.013 / 0.038 0.5 N/A ND Pass
Boscalid 0.008 / 0.023 10 N/A ND Pass
Chlorpyrifos 0.029 / 0.089 ≥ LOD N/A ND Pass
Cypermethrin 0.030 / 0.091 1 N/A ND Pass
Etoxazole 0.007 / 0.022 1.5 N/A ND Pass
Hexythiazox 0.009 / 0.027 2 N/A ND Pass
Imidacloprid 0.017 / 0.050 3 N/A ND Pass
Malathion 0.006 / 0.019 5 N/A ND Pass
Myclobutanil 0.015 / 0.044 9 N/A ND Pass
Permethrin 0.027 / 0.082 20 N/A ND Pass
Piperonyl Butoxide 0.007 / 0.020 8 N/A ND Pass
Propiconazole 0.004 / 0.013 20 N/A ND Pass
Spiromesifen 0.005 / 0.015 12 N/A ND Pass
Tebuconazole 0.006 / 0.018 2 N/A ND Pass
Trifloxystrobin 0.007 / 0.020 30 N/A ND Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

04/08/2020

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
1,2-Dichloroethane 0.111 / 0.336 1 N/A ND Pass
Benzene 0.043 / 0.132 1 N/A ND Pass
Chloroform 0.064 / 0.195 1 N/A ND Pass
Ethylene Oxide 0.136 / 0.413 1 N/A ND Pass
Dichloromethane (Methylene Chloride) 0.172 / 0.521 1 N/A ND Pass
Trichloroethylene 0.040 / 0.120 1 N/A ND Pass
Acetone 14.703 / 44.549 5000 N/A ND Pass
Acetonitrile 2.727 / 8.262 410 N/A ND Pass
n-Butane 5.672 / 17.185 5000 N/A ND Pass
Ethanol 11.775 / 35.679 5000 N/A <LOQ Pass
Ethyl Acetate 16.227 / 49.169 5000 N/A ND Pass
Ethyl Ether 11.608 / 35.172 5000 N/A ND Pass
n-Heptane 12.982 / 39.336 5000 N/A ND Pass
n-Hexane 1.816 / 5.502 290 N/A ND Pass
2-Propanol (Isopropyl Alcohol) 15.358 / 46.536 5000 N/A ND Pass
Methanol 15.584 / 47.220 3000 N/A ND Pass
n-Pentane 12.355 / 37.434 5000 N/A ND Pass
Propane 1.359 / 4.117 5000 N/A ND Pass
Toluene 7.174 / 21.736 890 N/A ND Pass
Total Xylenes 34.438 / 104.347 2170 N/A ND Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

04/08/2020

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Arsenic 0.013 / 0.039 1.5 N/A ND Pass
Cadmium 0.012 / 0.035 0.5 N/A ND Pass
Lead 0.031 / 0.095 0.5 N/A <LOQ Pass
Mercury 0.002 / 0.005 3 N/A ND Pass

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