Certificate of Analysis
REGULATORY COMPLIANCE

Sample Name:

Bubble-Mac Burger

Concentrate, Product Inhalable

Date Issued:

04/14/2023

Overall Batch Result:

Pass

Sum Cannabinoids 77.66%
Total Cannabinoids 68.47%
Total THC 65.413%
Total CBD 0.289%
Total Terpenoids 3.4977%
PhytoFacts®
Top 3 Terpenoids
  1. β-Caryophyllene 1.1794%
  2. Limonene 0.5012%
  3. α-Humulene 0.3911%

Sample Information

Sample Details

Sample ID:230411N023

Batch Number:1A4060300034A31000000308

Cultivator / Manufacturer

Show Details

Distributor

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Sampling Method: QSP 1265 - Sampling of Cannabis and Product Batches

PhytoFacts® Report

aroma
flavor
effect

The PhytoFacts chemometric report provides additional cannabinoid and terpenoid details, including dominant terpenes, entourage effects, aroma, flavor, and more.

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Cannabinoid Analysis - Summary

Sum of Cannabinoids: 77.66%

Total Cannabinoids: 68.47%

Total THC: 65.413%

Total CBD: 0.289%

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa+Δ8-THC) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + CBL + CBN

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877)) + Δ8-THC
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

Total Terpenoids: 3.4977%

 
 
 

1

β-Caryophyllene (1.1794%)

2

Limonene (0.5012%)

3

α-Humulene (0.3911%)

Safety Analysis - Summary

Δ9-THC per Unit: Pass

Pesticides: Pass

Mycotoxins: Pass

Residual Solvents: Pass

Heavy Metals: Pass

Microbiology: Pass

Foreign Material: Pass

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total Cannabinoids: 68.47%

Total THC: 65.413%

9-THC+0.877*THCa+Δ8-THC)

Total CBD: 0.289%

(CBD+0.877*CBDa)

Total CBG: 1.52%

Total CBG (CBG+0.877*CBGa)

Total THCV: 0.403%

Total THCV (THCV+0.877*THCVa)

Total CBC: 0.847%

Total CBC (CBC+0.877*CBCa)

Total CBDV: ND

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

04/13/2023

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
Tetrahydrocannabinolic Acid (THCa) 0.05 / 0.14 ±14.276 713.79 71.379
Δ9 Tetrahydrocannabinol (Δ9THC) 0.06 / 0.26 ±0.754 28.14 2.814
Cannabigerolic Acid (CBGa) 0.1 / 0.2 ±0.64 15.8 1.58
Cannabichromenic Acid (CBCa) 0.07 / 0.28 ±0.368 9.66 0.966
Tetrahydrocannabivarinic Acid (THCVa) 0.07 / 0.20 ±0.170 4.59 0.459
Cannabidiolic Acid (CBDa) 0.02 / 0.19 ±0.075 3.30 0.330
Cannabigerol (CBG) 0.06 / 0.19 ±0.040 1.30 0.130
∆8 Tetrahydrocannabinol (Δ8THC) 0.1 / 0.4 N/A ND ND
Tetrahydrocannabivarin (THCV) 0.1 / 0.2 N/A ND ND
Cannabidiol (CBD) 0.07 / 0.29 N/A ND ND
Cannabidivarin (CBDV) 0.04 / 0.15 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.03 / 0.53 N/A ND ND
Cannabicyclol (CBL) 0.06 / 0.24 N/A ND ND
Cannabinol (CBN) 0.1 / 0.3 N/A ND ND
Cannabichromene (CBC) 0.2 / 0.5 N/A ND ND
SUM OF CANNABINOIDS 776.6 mg/g 77.66%
Unit Mass:

2 grams

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Δ9-THC per Unit 1100 per-package limit 56.28 mg/unit Pass
Total THC per Unit 1308.26 mg/unit
CBD per Unit ND
Total CBD per Unit 5.78 mg/unit
Sum of Cannabinoids per Unit 1553.2 mg/unit
Total Cannabinoids per Unit 1369.4 mg/unit
Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

View PhytoFacts COA

See a visual representation of this sample's cannabinoid and terpenoid properties, including entourage effects, aroma, and flavor profile.

Summary

Total Terpenoids (mg/g): 34.977 mg/g

Total Terpenoids (%): 3.4977%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume. To see more detail for terpenoid content, view the PhytoFacts report.

  1. β-Caryophyllene 1.1794%

    A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB2 receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

  2. Limonene 0.5012%

    A monoterpene with a fragrance that can be described as orangey, citrusy, sweet and tart. It is most commonly found in nature as D-Limonene and is a primary contributor to the distinct scent of orange peels, from which it is commonly derived. Found in numerous pines, red maple, silver maple, aspens, cottonwoods, hemlocks, sumac, cedar, junipers...etc.

  3. α-Humulene 0.3911%

    Also known as α-caryophyllene, it is an isomer of the sesquiterpene β-Caryophyllene which frequently occurs in nature with many aromatic plants across the globe. It has a fragrance that can be described as earthy or musky with spicy undertones. Found in hops, forskohlii, skullcaps, basil, nutmeg, cloves, sage, cotton, tamarind, black pepper, guava, Scotch pine...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

04/13/2023

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
β-Caryophyllene 0.004 / 0.012 ±0.3267 11.794 1.1794
Limonene 0.005 / 0.016 ±0.0556 5.012 0.5012
α-Humulene 0.009 / 0.029 ±0.0978 3.911 0.3911
Myrcene 0.008 / 0.025 ±0.0313 3.126 0.3126
trans-β-Farnesene 0.008 / 0.025 ±0.0522 1.890 0.1890
α-Bisabolol 0.008 / 0.026 ±0.0772 1.860 0.1860
Linalool 0.009 / 0.032 ±0.0396 1.338 0.1338
β-Pinene 0.004 / 0.014 ±0.0112 1.257 0.1257
α-Pinene 0.005 / 0.017 ±0.0063 0.945 0.0945
Guaiol 0.009 / 0.030 ±0.0326 0.889 0.0889
Fenchol 0.010 / 0.034 ±0.0191 0.633 0.0633
Terpineol 0.009 / 0.031 ±0.0289 0.605 0.0605
Nerolidol 0.006 / 0.019 ±0.0265 0.541 0.0541
Caryophyllene Oxide 0.010 / 0.033 ±0.0172 0.481 0.0481
Camphene 0.005 / 0.015 ±0.0019 0.206 0.0206
Borneol 0.005 / 0.016 ±0.0060 0.183 0.0183
β-Ocimene 0.006 / 0.020 ±0.0017 0.068 0.0068
Terpinolene 0.008 / 0.026 ±0.0010 0.065 0.0065
Fenchone 0.009 / 0.028 ±0.0012 0.053 0.0053
Eucalyptol 0.006 / 0.018 ±0.0009 0.045 0.0045
Sabinene Hydrate 0.006 / 0.022 ±0.0009 0.031 0.0031
Citronellol 0.003 / 0.010 ±0.0011 0.028 0.0028
Nerol 0.003 / 0.011 ±0.0006 0.016 0.0016
α-Terpinene 0.005 / 0.017 N/A <LOQ <LOQ
γ-Terpinene 0.006 / 0.018 N/A <LOQ <LOQ
Sabinene 0.004 / 0.014 N/A ND ND
α-Phellandrene 0.006 / 0.020 N/A ND ND
Δ3-Carene 0.005 / 0.018 N/A ND ND
p-Cymene 0.005 / 0.016 N/A ND ND
Isopulegol 0.005 / 0.016 N/A ND ND
Camphor 0.006 / 0.019 N/A ND ND
Isoborneol 0.004 / 0.012 N/A ND ND
Menthol 0.008 / 0.025 N/A ND ND
Pulegone 0.003 / 0.011 N/A ND ND
Geraniol 0.002 / 0.007 N/A ND ND
Geranyl Acetate 0.004 / 0.014 N/A ND ND
α-Cedrene 0.005 / 0.016 N/A ND ND
Valencene 0.009 / 0.030 N/A ND ND
Cedrol 0.008 / 0.027 N/A ND ND
TOTAL 34.977 mg/g 3.4977%
Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Category 1 Pesticide Test Results

04/14/2023

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Aldicarb 0.03 / 0.08 ≥ LOD N/A ND Pass
Carbofuran 0.02 / 0.05 ≥ LOD N/A ND Pass
Chlordane* 0.03 / 0.08 ≥ LOD N/A ND Pass
Chlorfenapyr* 0.03 / 0.10 ≥ LOD N/A ND Pass
Chlorpyrifos 0.02 / 0.06 ≥ LOD N/A ND Pass
Coumaphos 0.02 / 0.07 ≥ LOD N/A ND Pass
Daminozide 0.02 / 0.07 ≥ LOD N/A ND Pass
Dichlorvos (DDVP) 0.03 / 0.09 ≥ LOD N/A ND Pass
Dimethoate 0.03 / 0.08 ≥ LOD N/A ND Pass
Ethoprophos 0.03 / 0.10 ≥ LOD N/A ND Pass
Etofenprox 0.02 / 0.06 ≥ LOD N/A ND Pass
Fenoxycarb 0.03 / 0.08 ≥ LOD N/A ND Pass
Fipronil 0.03 / 0.08 ≥ LOD N/A ND Pass
Imazalil 0.02 / 0.06 ≥ LOD N/A ND Pass
Methiocarb 0.02 / 0.07 ≥ LOD N/A ND Pass
Parathion-methyl 0.03 / 0.10 ≥ LOD N/A ND Pass
Mevinphos 0.03 / 0.09 ≥ LOD N/A ND Pass
Paclobutrazol 0.02 / 0.05 ≥ LOD N/A ND Pass
Propoxur 0.03 / 0.09 ≥ LOD N/A ND Pass
Spiroxamine 0.03 / 0.08 ≥ LOD N/A ND Pass
Thiacloprid 0.03 / 0.10 ≥ LOD N/A ND Pass
Category 2 Pesticide Test Results

04/14/2023

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Abamectin 0.03 / 0.10 0.1 N/A ND Pass
Acephate 0.02 / 0.07 0.1 N/A ND Pass
Acequinocyl 0.02 / 0.07 0.1 N/A ND Pass
Acetamiprid 0.02 / 0.05 0.1 N/A ND Pass
Azoxystrobin 0.02 / 0.07 0.1 N/A ND Pass
Bifenazate 0.01 / 0.04 0.1 N/A ND Pass
Bifenthrin 0.02 / 0.05 3 N/A ND Pass
Boscalid 0.03 / 0.09 0.1 N/A ND Pass
Captan 0.19 / 0.57 0.7 N/A ND Pass
Carbaryl 0.02 / 0.06 0.5 N/A ND Pass
Chlorantraniliprole 0.04 / 0.12 10 N/A ND Pass
Clofentezine 0.03 / 0.09 0.1 N/A ND Pass
Cyfluthrin 0.12 / 0.38 2 N/A ND Pass
Cypermethrin 0.11 / 0.32 1 N/A ND Pass
Diazinon 0.02 / 0.05 0.1 N/A ND Pass
Dimethomorph 0.03 / 0.09 2 N/A ND Pass
Etoxazole 0.02 / 0.06 0.1 N/A ND Pass
Fenhexamid 0.03 / 0.09 0.1 N/A ND Pass
Fenpyroximate 0.02 / 0.06 0.1 N/A ND Pass
Flonicamid 0.03 / 0.10 0.1 N/A ND Pass
Fludioxonil 0.03 / 0.10 0.1 N/A ND Pass
Hexythiazox 0.02 / 0.07 0.1 N/A ND Pass
Imidacloprid 0.04 / 0.11 5 N/A ND Pass
Kresoxim-methyl 0.02 / 0.07 0.1 N/A ND Pass
Malathion 0.03 / 0.09 0.5 N/A ND Pass
Metalaxyl 0.02 / 0.07 2 N/A ND Pass
Methomyl 0.03 / 0.10 1 N/A ND Pass
Myclobutanil 0.03 / 0.09 0.1 N/A ND Pass
Naled 0.02 / 0.07 0.1 N/A ND Pass
Oxamyl 0.04 / 0.11 0.5 N/A ND Pass
Pentachloronitrobenzene* 0.03 / 0.09 0.1 N/A ND Pass
Permethrin 0.04 / 0.12 0.5 N/A ND Pass
Phosmet 0.03 / 0.10 0.1 N/A ND Pass
Piperonyl Butoxide 0.02 / 0.07 3 N/A ND Pass
Prallethrin 0.03 / 0.08 0.1 N/A ND Pass
Propiconazole 0.02 / 0.07 0.1 N/A ND Pass
Pyrethrins 0.04 / 0.12 0.5 N/A ND Pass
Pyridaben 0.02 / 0.07 0.1 N/A ND Pass
Spinetoram 0.02 / 0.07 0.1 N/A ND Pass
Spinosad 0.02 / 0.07 0.1 N/A ND Pass
Spiromesifen 0.02 / 0.05 0.1 N/A ND Pass
Spirotetramat 0.02 / 0.06 0.1 N/A ND Pass
Tebuconazole 0.02 / 0.07 0.1 N/A ND Pass
Thiamethoxam 0.03 / 0.10 5 N/A ND Pass
Trifloxystrobin 0.03 / 0.08 0.1 N/A ND Pass

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS

Mycotoxin Test Results

04/14/2023

PASS

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Compound LOD/LOQ
(μg/kg)
Action Limit
(μg/kg)
Measurement
Uncertainty
(μg/kg)
Result
(μg/kg)
Result
Aflatoxin B1 2.0 / 6.0 N/A ND
Aflatoxin B2 1.8 / 5.6 N/A ND
Aflatoxin G1 1.0 / 3.1 N/A ND
Aflatoxin G2 1.2 / 3.5 N/A ND
Total Aflatoxin 20 ± ND Pass
Ochratoxin A 6.3 / 19.2 20 N/A ND Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Category 1 Residual Solvents Test Results

04/13/2023

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
1,2-Dichloroethane 0.05 / 0.1 1 N/A ND Pass
Benzene 0.03 / 0.09 1 N/A ND Pass
Chloroform 0.1 / 0.2 1 N/A ND Pass
Ethylene Oxide 0.3 / 0.8 1 N/A ND Pass
Dichloromethane (Methylene Chloride) 0.3 / 0.9 1 N/A ND Pass
Trichloroethylene 0.1 / 0.3 1 N/A ND Pass
Category 2 Residual Solvents Test Results

04/13/2023

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Acetone 20 / 50 5000 N/A <LOQ Pass
Acetonitrile 2 / 7 410 N/A ND Pass
n-Butane 10 / 50 5000 N/A ND Pass
Ethanol 20 / 50 5000 N/A ND Pass
Ethyl Acetate 20 / 60 5000 N/A ND Pass
Ethyl Ether 20 / 50 5000 N/A ND Pass
n-Heptane 20 / 60 5000 N/A ND Pass
n-Hexane 2 / 5 290 N/A <LOQ Pass
2-Propanol (Isopropyl Alcohol) 10 / 40 5000 ±2.3 100 Pass
Methanol 50 / 200 3000 N/A ND Pass
n-Pentane 20 / 50 5000 N/A ND Pass
Propane 10 / 20 5000 N/A ND Pass
Toluene 7 / 21 890 N/A ND Pass
Total Xylenes 50 / 160 2170 N/A ND Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

04/13/2023

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Arsenic 0.02 / 0.1 0.2 N/A <LOQ Pass
Cadmium 0.02 / 0.05 0.2 N/A ND Pass
Lead 0.04 / 0.1 0.5 N/A <LOQ Pass
Mercury 0.002 / 0.01 0.1 N/A <LOQ Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants

Microbiology Test Results

04/13/2023

PASS

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Compound Action Limit Result Result
Aspergillus flavus Not Detected in 1g ND Pass
Aspergillus fumigatus Not Detected in 1g ND Pass
Aspergillus niger Not Detected in 1g ND Pass
Aspergillus terreus Not Detected in 1g ND Pass
Salmonella spp. Not Detected in 1g ND Pass
Shiga toxin-producing Escherichia coli Not Detected in 1g ND Pass

Visual analysis includes, but is not limited to, sand, soil, cinders, dirt, mold, hair, insect fragments, and mammalian excreta.

Method: QSP 1226 - Analysis of Foreign Material in Cannabis and Cannabis Products

Foreign Material Test Results

04/12/2023

PASS

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Compound Action Limit Result Result
Total Sample Area Covered by Sand, Soil, Cinders, or Dirt >25% None Pass
Total Sample Area Covered by Mold >25% None Pass
Total Sample Area Covered by an Imbedded Foreign Material >25% None Pass
Insect Fragment Count > 1 per 3 grams 0.0 Pass
Hair Count > 1 per 3 grams 0.0 Pass
Mammalian Excreta Count > 1 per 3 grams 0.0 Pass

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