Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

Hemp D9 Distillate (May 5, 2025)

Concentrate, Product Inhalable

Date Issued:

05/14/2025

Sample Information

Sample Details

Sample ID:250509Q008

Batch Number:DIST.HD9.050525

Cultivator / Manufacturer

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Distributor / Tested For

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Safety Analysis - Summary

Residual Solvents: Pass

Microbiology (PCR): Pass

Microbiology (Plating): ND

View Complete Test Results:

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

05/12/2025

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Propane 0.234 / 0.781 5000 N/A ND Pass
2-Methylpropane (Isobutane) 0.052 / 0.173 N/A ND
n-Butane 0.019 / 0.063 5000 N/A ND Pass
Total Butanes ± ND
2-Methylbutane (Isopentane) 0.310 / 1.035 N/A ND
2,2-Dimethylpropane (Neopentane) 0.035 / 0.117 N/A ND
n-Pentane 0.310 / 1.033 5000 N/A ND Pass
Total Pentanes ± ND
2,2-Dimethylbutane (Neohexane) 9.831 / 32.77 N/A ND
2,3-Dimethylbutane / 2-Methylpentane (Isohexane) 0.381 / 1.271 N/A ND
3-Methylpentane 0.109 / 0.365 N/A ND
n-Hexane 0.110 / 0.366 290 N/A ND Pass
Total Hexanes ± ND
Cyclohexane 0.357 / 1.190 N/A ND
2,2-Dimethylpentane (Neoheptane) 0.493 / 1.642 N/A ND
2,3-Dimethylpentane 1.009 / 3.365 N/A ND
2,4-Dimethylpentane 0.737 / 2.458 N/A ND
3,3-Dimethylpentane 0.198 / 0.660 N/A ND
2,2,3-Trimethylbutane (Triptane) 0.521 / 1.738 N/A ND
2-Methylhexane (Isoheptane) 0.610 / 2.034 N/A ND
3-Methylhexane 0.235 / 0.785 N/A ND
3-Ethylpentane 0.304 / 1.012 N/A ND
n-Heptane 13.12 / 43.72 5000 N/A ND Pass
Total Heptanes ± ND
Cycloheptane 0.597 / 1.989 N/A ND
Benzene 0.089 / 0.295 1 N/A ND Pass
Toluene 0.115 / 0.382 890 N/A ND Pass
Cumene 0.180 / 0.600 N/A ND
1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene) 0.451 / 1.502 N/A ND
1,2-Dimethylbenzene (o-Xylene) 0.387 / 1.289 N/A ND
Ethylbenzene 0.370 / 1.233 N/A ND
Total Xylenes 2170 ± ND Pass
Methanol 53.92 / 163.4 3000 N/A ND Pass
Ethanol 8.984 / 27.23 5000 N/A ND Pass
1-Propanol 1.540 / 5.133 N/A ND
2-Propanol (Isopropyl Alcohol) 8.421 / 25.52 5000 N/A ND Pass
1-Butanol 0.475 / 1.582 N/A ND
2-Butanol 7.248 / 24.16 N/A ND
1-Pentanol 1.461 / 4.869 N/A ND
Acetone 10.59 / 32.08 5000 N/A ND Pass
2-Butanone 0.169 / 0.564 N/A ND
Tetrahydrofuran 0.622 / 2.075 N/A ND
Ethyl Ether 0.197 / 0.658 5000 N/A ND Pass
Ethylene Glycol 3.803 / 12.68 N/A ND
2-Ethoxyethanol 1.235 / 4.118 N/A ND
1,2-Dimethoxyethane 2.116 / 7.052 N/A ND
1,4-Dioxane 0.468 / 1.558 N/A ND
Ethylene Oxide 0.253 / 0.844 1 N/A ND Pass
Ethyl Acetate 1.123 / 3.745 5000 N/A ND Pass
Isopropyl Acetate 0.347 / 1.158 N/A ND
Chloroform 0.251 / 0.838 1 N/A ND Pass
Dichloromethane (Methylene Chloride) 2.651 / 8.838 1 N/A ND Pass
Trichloroethylene 0.299 / 0.996 1 N/A ND Pass
1,2-Dichloroethane 0.162 / 0.541 1 N/A ND Pass
1,1-Dichloroethene 0.185 / 0.616 N/A ND
1,2-Dichloroethene 0.428 / 1.427 N/A ND
Sulfolane 47.66 / 158.9 N/A ND
Dimethyl Sulfoxide 6.168 / 20.56 N/A ND
Acetonitrile 1.595 / 4.833 410 N/A ND Pass
Pyridine 0.407 / 1.355 N/A ND
N,N-Dimethylacetamide 0.127 / 0.422 N/A ND
N,N-Dimethylformamide 0.946 / 3.153 N/A ND

Total Butanes = n-Butane + 2-Methylpropane (Isobutane)

Total Pentanes = n-Pentane + 2-Methylbutane (Isopentane) + 2,2-Dimethylpropane (Neopentane)

Total Hexanes = n-Hexane + 2,2-Dimethylbutane (Neohexane) + 2,3-Dimethylbutane / 2-Methylpentane (Isohexane) + 3-Methylpentane

Total Heptanes = 2,2-Dimethylpentane (Neoheptane) + 2,3-Dimethylpentane + 2,4-Dimethylpentane + 3,3-Dimethylpentane + 2,2,3-Trimethylbutane (Triptane) + 2-Methylhexane (Isoheptane) + 3-Methylhexane + 3-Ethylpentane + n-Heptane

Total Xylenes = 1,2-Dimethylbenzene (o-Xylene) + 1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene) + Ethylbenzene

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants. And Analysis conducted by 3MTM PetrifilmTM and plate counts of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants

Microbiology Test Results (PCR)

05/14/2025

PASS

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Compound Action Limit Result
(cfu/g)
Result
Yersinia spp. ND
Salmonella spp. Not Detected in 1g ND Pass
Candida albicans ND
Aspergillus niger Not Detected in 1g ND Pass
Aspergillus flavus Not Detected in 1g ND Pass
Campylobacter spp. ND
Aspergillus terreus Not Detected in 1g ND Pass
Aspergillus fumigatus Not Detected in 1g ND Pass
Staphylococcus aureus ND
Listeria monocytogenes ND
Pseudomonas aeruginosa ND
Bile-Tolerant Gram-Negative Bacteria ND
Shiga toxin-producing Escherichia coli Not Detected in 1g ND Pass
Microbiology Test Results (PLATING)

05/14/2025

ND

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Compound Action Limit
(cfu/g)
Result
(cfu/g)
Result
Coliforms ND
Escherichia coli ND
Total Yeast and Mold ND
Total Aerobic Bacteria ND
Total Enterobacteriaceae ND

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