Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

D9 Water Emulsion Full Panel (5/12/2025)

Concentrate, Product Inhalable

Date Issued:

05/24/2025

Total THC 11.329%
Total CBD Not Detected
Sum Cannabinoids 11.588%
Total Cannabinoids 11.588%

Sample Information

Sample Details

Sample ID:250519P001

Batch Number:WS.D9.051225

Cultivator / Manufacturer

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Distributor / Tested For

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Cannabinoid Analysis - Summary

Total THC: 11.329%

Total CBD: Not Detected

Sum of Cannabinoids: 11.588%

Total Cannabinoids: 11.588%

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Safety Analysis - Summary

Pesticides: Pass

Mycotoxins: Pass

Residual Solvents: Pass

Heavy Metals: Fail

Microbiology (PCR): Pass

Microbiology (Plating): ND

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 11.329%

9-THC+0.877*THCa)

Total CBD: Not Detected

(CBD+0.877*CBDa)

Total Cannabinoids: 11.588%

Total CBG: 0.259%

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: ND

Total CBC (CBC+0.877*CBCa)

Total CBDV: ND

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

05/20/2025

Result Views

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Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
Δ9 Tetrahydrocannabinol (Δ9THC) 0.06 / 0.26 ±3.036 113.29 11.329
Cannabigerol (CBG) 0.06 / 0.19 ±0.080 2.59 0.259
Cannabichromene (CBC) 0.2 / 0.5 N/A ND ND
Cannabidiol (CBD) 0.07 / 0.29 N/A ND ND
Cannabicyclol (CBL) 0.06 / 0.24 N/A ND ND
Cannabinol (CBN) 0.1 / 0.3 N/A ND ND
Cannabichromenic Acid (CBCa) 0.07 / 0.28 N/A ND ND
Cannabidivarin (CBDV) 0.04 / 0.15 N/A ND ND
Cannabidiolic Acid (CBDa) 0.02 / 0.19 N/A ND ND
Cannabigerolic Acid (CBGa) 0.1 / 0.2 N/A ND ND
Tetrahydrocannabivarin (THCV) 0.1 / 0.2 N/A ND ND
Tetrahydrocannabinolic Acid (THCa) 0.05 / 0.14 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.03 / 0.53 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.07 / 0.20 N/A ND ND
∆8 Tetrahydrocannabinol (Δ8THC) 0.1 / 0.4 N/A ND ND
SUM OF CANNABINOIDS 115.88 mg/g 11.588%
Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

‡Analytes part of our California Select Panel.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

05/20/2025

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Abamectin 0.032 / 0.097 0.1 N/A ND Pass
Acephate 0.006 / 0.018 0.1 N/A ND Pass
Acequinocyl 0.009 / 0.027 0.1 N/A ND Pass
Acetamiprid 0.016 / 0.049 0.1 N/A ND Pass
Aldicarb 0.030 / 0.090 ≥ LOD N/A ND Pass
Allethrin 0.030 / 0.092 N/A ND
Atrazine 0.006 / 0.019 N/A ND
Azadirachtin 0.082 / 0.248 N/A ND
Azoxystrobin 0.003 / 0.009 0.1 N/A ND Pass
Benzovindiflupyr 0.003 / 0.009 N/A ND
Bifenazate 0.003 / 0.009 0.1 N/A ND Pass
Bifenthrin 0.021 / 0.064 3 N/A <LOQ Pass
Boscalid 0.003 / 0.009 0.1 N/A ND Pass
Buprofezin 0.006 / 0.019 N/A <LOQ
Captan 0.045 / 0.135 0.7 N/A ND Pass
Carbaryl 0.007 / 0.020 0.5 N/A ND Pass
Carbofuran 0.003 / 0.008 ≥ LOD N/A ND Pass
Chlorantraniliprole 0.006 / 0.018 10 N/A ND Pass
Chlordane* 0.010 / 0.032 ≥ LOD N/A ND Pass
Chlorfenapyr* 0.005 / 0.015 ≥ LOD N/A ND Pass
Chlormequat chloride 0.022 / 0.066 N/A ND
Chlorpyrifos 0.013 / 0.039 ≥ LOD N/A ND Pass
Clofentezine 0.003 / 0.009 0.1 N/A ND Pass
Clothianidin 0.008 / 0.025 N/A ND
Coumaphos 0.003 / 0.010 ≥ LOD N/A ND Pass
Cyantraniliprole 0.003 / 0.010 N/A ND
Cyfluthrin 0.052 / 0.159 2 N/A ND Pass
Cypermethrin 0.051 / 0.153 1 N/A ND Pass
Cyprodinil 0.003 / 0.008 N/A ND
Daminozide 0.026 / 0.077 ≥ LOD N/A ND Pass
Deltamethrin 0.059 / 0.180 N/A ND
Diazinon 0.006 / 0.017 0.1 N/A ND Pass
Dichlorvos (DDVP) 0.012 / 0.038 ≥ LOD N/A ND Pass
Dimethoate 0.003 / 0.009 ≥ LOD N/A ND Pass
Dimethomorph 0.016 / 0.050 2 N/A ND Pass
Dinotefuran 0.010 / 0.030 N/A ND
Diuron 0.013 / 0.040 N/A ND
Dodemorph 0.012 / 0.035 N/A ND
Endosulfan sulfate 0.016 / 0.048 N/A ND
Endosulfan-α* 0.004 / 0.014 N/A ND
Endosulfan-β* 0.006 / 0.019 N/A ND
Ethoprophos 0.003 / 0.009 ≥ LOD N/A ND Pass
Etofenprox 0.014 / 0.042 ≥ LOD N/A ND Pass
Etoxazole 0.007 / 0.020 0.1 N/A ND Pass
Etridiazole* 0.002 / 0.005 N/A ND
Fenhexamid 0.003 / 0.008 0.1 N/A ND Pass
Fenoxycarb 0.003 / 0.010 ≥ LOD N/A ND Pass
Fenpyroximate 0.007 / 0.020 0.1 N/A ND Pass
Fensulfothion 0.003 / 0.010 N/A ND
Fenthion 0.003 / 0.010 N/A ND
Fenvalerate 0.033 / 0.099 N/A ND
Fipronil 0.003 / 0.010 ≥ LOD N/A ND Pass
Flonicamid 0.007 / 0.022 0.1 N/A ND Pass
Fludioxonil 0.003 / 0.010 0.1 N/A ND Pass
Fluopyram 0.003 / 0.009 ±0.0003 0.011
Hexythiazox 0.003 / 0.010 0.1 N/A ND Pass
Imazalil 0.003 / 0.009 ≥ LOD N/A ND Pass
Imidacloprid 0.003 / 0.010 5 N/A ND Pass
Iprodione 0.077 / 0.233 N/A ND
Kinoprene 0.077 / 0.233 N/A ND
Kresoxim-methyl 0.006 / 0.019 0.1 N/A ND Pass
λ-Cyhalothrin 0.068 / 0.206 N/A ND
Malathion 0.003 / 0.009 0.5 N/A ND Pass
Metalaxyl 0.003 / 0.010 2 N/A ND Pass
Methiocarb 0.003 / 0.008 ≥ LOD N/A ND Pass
Methomyl 0.008 / 0.025 1 N/A ND Pass
Methoprene 0.172 / 0.521 N/A ND
Mevinphos 0.008 / 0.024 ≥ LOD N/A ND Pass
MGK-264 0.015 / 0.047 N/A ND
Myclobutanil 0.003 / 0.009 0.1 N/A ND Pass
Naled 0.021 / 0.064 0.1 N/A ND Pass
Novaluron 0.002 / 0.005 N/A ND
Oxamyl 0.017 / 0.051 0.5 N/A ND Pass
Paclobutrazol 0.003 / 0.010 ≥ LOD N/A ND Pass
Parathion-methyl 0.016 / 0.050 ≥ LOD N/A ND Pass
Pentachloronitrobenzene (Quintozene)* 0.004 / 0.012 0.1 N/A ND Pass
Permethrin 0.056 / 0.168 0.5 N/A ND Pass
Phenothrin 0.016 / 0.047 N/A ND
Phosmet 0.007 / 0.020 0.1 N/A ND Pass
Piperonyl Butoxide 0.010 / 0.029 3 N/A ND Pass
Pirimicarb 0.003 / 0.009 N/A ND
Prallethrin 0.015 / 0.046 0.1 N/A ND Pass
Propiconazole 0.027 / 0.080 0.1 N/A ND Pass
Propoxur 0.003 / 0.008 ≥ LOD N/A ND Pass
Pyraclostrobin 0.003 / 0.010 N/A ND
Pyrethrins 0.016 / 0.049 0.5 N/A ND Pass
Pyridaben 0.005 / 0.017 0.1 N/A ND Pass
Pyriproxyfen 0.003 / 0.009 N/A ND
Resmethrin 0.013 / 0.039 N/A ND
Spinetoram 0.003 / 0.010 0.1 N/A ND Pass
Spinosad 0.003 / 0.010 0.1 N/A ND Pass
Spirodiclofen 0.031 / 0.093 N/A ND
Spiromesifen 0.016 / 0.050 0.1 N/A ND Pass
Spirotetramat 0.003 / 0.010 0.1 N/A ND Pass
Spiroxamine 0.020 / 0.062 ≥ LOD N/A ND Pass
Tebuconazole 0.003 / 0.010 0.1 N/A ND Pass
Tebufenozide 0.003 / 0.008 N/A ND
Teflubenzuron 0.007 / 0.022 N/A ND
Tetrachlorvinphos 0.003 / 0.008 N/A ND
Tetramethrin 0.021 / 0.063 N/A ND
Thiabendazole 0.006 / 0.020 N/A ND
Thiacloprid 0.003 / 0.009 ≥ LOD N/A ND Pass
Thiamethoxam 0.003 / 0.010 5 N/A ND Pass
Thiophanate-methyl 0.013 / 0.040 N/A ND
Trifloxystrobin 0.003 / 0.009 0.1 N/A ND Pass

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS

Mycotoxin Test Results

05/20/2025

PASS

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Compound LOD/LOQ
(μg/kg)
Action Limit
(μg/kg)
Measurement
Uncertainty
(μg/kg)
Result
(μg/kg)
Result
Aflatoxin B1 1.6 / 5.0 N/A ND
Aflatoxin B2 1.4 / 4.1 N/A ND
Aflatoxin G1 1.6 / 4.9 N/A ND
Aflatoxin G2 1.6 / 5.0 N/A ND
Ochratoxin A 1.6 / 5.0 20 N/A ND Pass
Total Aflatoxin 20 ± ND Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

05/22/2025

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Propane 0.234 / 0.781 5000 N/A ND Pass
2-Methylpropane (Isobutane) 0.052 / 0.173 N/A ND
n-Butane 0.019 / 0.063 5000 N/A ND Pass
Total Butanes ± ND
2-Methylbutane (Isopentane) 0.310 / 1.035 N/A ND
2,2-Dimethylpropane (Neopentane) 0.035 / 0.117 N/A ND
n-Pentane 0.310 / 1.033 5000 N/A ND Pass
Total Pentanes ± ND
2,2-Dimethylbutane (Neohexane) 9.831 / 32.77 N/A ND
2,3-Dimethylbutane / 2-Methylpentane (Isohexane) 0.381 / 1.271 N/A ND
3-Methylpentane 0.109 / 0.365 N/A ND
n-Hexane 0.110 / 0.366 290 N/A ND Pass
Total Hexanes ± ND
Cyclohexane 0.357 / 1.190 N/A ND
2,2-Dimethylpentane (Neoheptane) 0.493 / 1.642 N/A ND
2,3-Dimethylpentane 1.009 / 3.365 N/A ND
2,4-Dimethylpentane 0.737 / 2.458 N/A ND
3,3-Dimethylpentane 0.198 / 0.660 N/A ND
2,2,3-Trimethylbutane (Triptane) 0.521 / 1.738 N/A ND
2-Methylhexane (Isoheptane) 0.610 / 2.034 N/A ND
3-Methylhexane 0.235 / 0.785 N/A ND
3-Ethylpentane 0.304 / 1.012 N/A ND
n-Heptane 13.12 / 43.72 5000 N/A ND Pass
Total Heptanes ± ND
Cycloheptane 0.597 / 1.989 N/A ND
Benzene 0.089 / 0.295 1 N/A ND Pass
Toluene 0.115 / 0.382 890 N/A ND Pass
Cumene 0.180 / 0.600 N/A ND
1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene) 0.451 / 1.502 N/A ND
1,2-Dimethylbenzene (o-Xylene) 0.387 / 1.289 N/A ND
Ethylbenzene 0.370 / 1.233 N/A ND
Total Xylenes 2170 ± ND Pass
Methanol 53.92 / 163.4 3000 N/A ND Pass
Ethanol 8.984 / 27.23 5000 N/A ND Pass
1-Propanol 1.540 / 5.133 N/A ND
2-Propanol (Isopropyl Alcohol) 8.421 / 25.52 5000 ±1.284 89.14 Pass
1-Butanol 0.475 / 1.582 N/A ND
2-Butanol 7.248 / 24.16 N/A ND
1-Pentanol 1.461 / 4.869 N/A ND
Acetone 10.59 / 32.08 5000 N/A <LOQ Pass
2-Butanone 0.169 / 0.564 N/A ND
Tetrahydrofuran 0.622 / 2.075 N/A ND
Ethyl Ether 0.197 / 0.658 5000 N/A ND Pass
Ethylene Glycol 3.803 / 12.68 N/A ND
2-Ethoxyethanol 1.235 / 4.118 N/A ND
1,2-Dimethoxyethane 2.116 / 7.052 N/A ND
1,4-Dioxane 0.468 / 1.558 N/A ND
Ethylene Oxide 0.253 / 0.844 1 N/A ND Pass
Ethyl Acetate 1.123 / 3.745 5000 N/A ND Pass
Isopropyl Acetate 0.347 / 1.158 N/A ND
Chloroform 0.251 / 0.838 1 N/A ND Pass
Dichloromethane (Methylene Chloride) 2.651 / 8.838 1 N/A ND Pass
Trichloroethylene 0.299 / 0.996 1 N/A ND Pass
1,2-Dichloroethane 0.162 / 0.541 1 N/A ND Pass
1,1-Dichloroethene 0.185 / 0.616 N/A ND
1,2-Dichloroethene 0.428 / 1.427 N/A ND
Sulfolane 47.66 / 158.9 N/A ND
Dimethyl Sulfoxide 6.168 / 20.56 N/A ND
Acetonitrile 1.595 / 4.833 410 N/A ND Pass
Pyridine 0.407 / 1.355 N/A ND
N,N-Dimethylacetamide 0.127 / 0.422 N/A ND
N,N-Dimethylformamide 0.946 / 3.153 N/A ND

Total Butanes = n-Butane + 2-Methylpropane (Isobutane)

Total Pentanes = n-Pentane + 2-Methylbutane (Isopentane) + 2,2-Dimethylpropane (Neopentane)

Total Hexanes = n-Hexane + 2,2-Dimethylbutane (Neohexane) + 2,3-Dimethylbutane / 2-Methylpentane (Isohexane) + 3-Methylpentane

Total Heptanes = 2,2-Dimethylpentane (Neoheptane) + 2,3-Dimethylpentane + 2,4-Dimethylpentane + 3,3-Dimethylpentane + 2,2,3-Trimethylbutane (Triptane) + 2-Methylhexane (Isoheptane) + 3-Methylhexane + 3-Ethylpentane + n-Heptane

Total Xylenes = 1,2-Dimethylbenzene (o-Xylene) + 1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene) + Ethylbenzene

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

05/21/2025

FAIL

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Arsenic 0.02 / 0.1 0.2 N/A <LOQ Pass
Cadmium 0.02 / 0.05 0.2 ±0.010 0.51 Fail
Lead 0.04 / 0.1 0.5 N/A ND Pass
Mercury 0.002 / 0.01 0.1 N/A ND Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants. And Analysis conducted by 3MTM PetrifilmTM and plate counts of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants

Microbiology Test Results (PCR)

05/24/2025

PASS

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Compound Action Limit Result
(cfu/g)
Result
Yersinia spp. ND
Salmonella spp. Not Detected in 1g ND Pass
Candida albicans ND
Aspergillus niger Not Detected in 1g ND Pass
Aspergillus flavus Not Detected in 1g ND Pass
Campylobacter spp. ND
Aspergillus terreus Not Detected in 1g ND Pass
Aspergillus fumigatus Not Detected in 1g ND Pass
Staphylococcus aureus ND
Listeria monocytogenes ND
Pseudomonas aeruginosa ND
Bile-Tolerant Gram-Negative Bacteria ND
Shiga toxin-producing Escherichia coli Not Detected in 1g ND Pass
Microbiology Test Results (PLATING)

05/24/2025

ND

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Compound Action Limit
(cfu/g)
Result
(cfu/g)
Result
Coliforms ND
Escherichia coli ND
Total Yeast and Mold ND
Total Aerobic Bacteria ND
Total Enterobacteriaceae ND

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