Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

Valentine 1

Concentrate, Product Inhalable

Date Issued:

04/07/2022

Total THC 1.456%
Total CBD 42.811%
Sum Cannabinoids 51.351%
Total Cannabinoids 47.001%
Total Terpenoids 10.0066%
PhytoFacts®
Top 3 Terpenoids
  1. β-Caryophyllene 2.5724%
  2. Myrcene 2.4380%
  3. α-Humulene 0.9428%

Sample Information

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Sample Details

Sample ID:210322W013

Batch Number:

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Cultivator / Manufacturer

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Distributor / Tested For

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PhytoFacts® Report

aroma
flavor
effect
View Online Download

The PhytoFacts chemometric report provides additional cannabinoid and terpenoid details, including dominant terpenes, entourage effects, aroma, flavor, and more.

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Cannabinoid Analysis - Summary

View Full Results

Total THC: 1.456%

Total CBD: 42.811%

Sum of Cannabinoids: 51.351%

Total Cannabinoids: 47.001%

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

View Full Results

Total Terpenoids: 10.0066%

 
 
 

1

β-Caryophyllene (2.5724%)

2

Myrcene (2.4380%)

3

α-Humulene (0.9428%)

Safety Analysis - Summary

View Full Results

Pesticides: Fail

Heavy Metals: Pass

View Complete Test Results:

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Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 1.456%

(Δ9-THC+0.877*THCa)

Total CBD: 42.811%

(CBD+0.877*CBDa)

Total Cannabinoids: 47.001%

Total CBG: 0.766%

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 1.678%

Total CBC (CBC+0.877*CBCa)

Total CBDV: 0.290%

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

03/24/2021

Result Views

Table Pie Chart

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g) 		Measurement
Uncertainty
(mg/g) 		Result
(mg/g) 		Result
(%)
Cannabidiolic Acid (CBDa) 0.02 / 0.19 ±9.520 326.02 32.602
Cannabidiol (CBD) 0.07 / 0.29 ±6.583 142.19 14.219
Cannabichromenic Acid (CBCa) 0.07 / 0.28 ±0.685 14.00 1.400
Δ9 Tetrahydrocannabinol (Δ9THC) 0.06 / 0.26 ±0.301 8.75 0.875
Tetrahydrocannabinolic Acid (THCa) 0.05 / 0.14 ±0.170 6.63 0.663
Cannabichromene (CBC) 0.2 / 0.5 ±0.13 4.5 0.45
Cannabigerolic Acid (CBGa) 0.1 / 0.2 ±0.23 4.5 0.45
Cannabigerol (CBG) 0.06 / 0.19 ±0.146 3.71 0.371
Cannabidivarinic Acid (CBDVa) 0.03 / 0.53 ±0.076 2.55 0.255
Cannabidivarin (CBDV) 0.04 / 0.15 ±0.029 0.66 0.066
Cannabicyclol (CBL) 0.06 / 0.24 N/A ND ND
Cannabinol (CBN) 0.1 / 0.3 N/A ND ND
Tetrahydrocannabivarin (THCV) 0.1 / 0.2 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.07 / 0.20 N/A ND ND
∆8 Tetrahydrocannabinol (Δ8THC) 0.1 / 0.4 N/A ND ND
SUM OF CANNABINOIDS 513.51 mg/g 51.351%
Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

View PhytoFacts COA

See a visual representation of this sample's cannabinoid and terpenoid properties, including entourage effects, aroma, and flavor profile.

Summary

Total Terpenoids (mg/g): 100.066 mg/g

Total Terpenoids (%): 10.0066%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume. To see more detail for terpenoid content, view the PhytoFacts report.

  1. β-Caryophyllene 2.5724%

    A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB2 receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

  2. Myrcene 2.4380%

    A monoterpene with a fragrance that can be described as peppery, spicy, herbal, floral and woody. Although it has a pleasant odor, it is typically used by the perfume industry as precursor for developing other fragrances. Found in hops, houttuynia, bay, thyme, lemon grass, mango, verbena, cardamom, citrus...etc.

  3. α-Humulene 0.9428%

    Also known as α-caryophyllene, it is an isomer of the sesquiterpene β-Caryophyllene which frequently occurs in nature with many aromatic plants across the globe. It has a fragrance that can be described as earthy or musky with spicy undertones. Found in hops, forskohlii, skullcaps, basil, nutmeg, cloves, sage, cotton, tamarind, black pepper, guava, Scotch pine...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

03/24/2021

Result Views

Table Bar Graph

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g) 		Measurement
Uncertainty
(mg/g) 		Result
(mg/g) 		Result
(%)
β-Caryophyllene 0.004 / 0.012 ±0.9158 25.724 2.5724
Myrcene 0.008 / 0.025 ±0.3145 24.380 2.4380
α-Humulene 0.009 / 0.029 ±0.3026 9.428 0.9428
α-Bisabolol 0.008 / 0.026 ±0.4675 8.755 0.8755
Guaiol 0.009 / 0.030 ±0.3267 6.921 0.6921
Limonene 0.005 / 0.016 ±0.0960 6.711 0.6711
α-Pinene 0.005 / 0.017 ±0.0429 4.990 0.4990
Linalool 0.009 / 0.032 ±0.0717 1.887 0.1887
β-Ocimene 0.011 / 0.038 ±0.0590 1.839 0.1839
Caryophyllene Oxide 0.010 / 0.033 ±0.0659 1.433 0.1433
Fenchol 0.010 / 0.034 ±0.0541 1.398 0.1398
β-Pinene 0.004 / 0.014 ±0.0160 1.390 0.1390
Terpineol 0.016 / 0.055 ±0.0818 1.332 0.1332
trans-β-Farnesene 0.008 / 0.025 ±0.0419 1.181 0.1181
Nerolidol 0.009 / 0.028 ±0.0428 0.681 0.0681
Borneol 0.005 / 0.016 ±0.0253 0.602 0.0602
Terpinolene 0.008 / 0.026 ±0.0090 0.438 0.0438
Camphene 0.005 / 0.015 ±0.0040 0.349 0.0349
Fenchone 0.009 / 0.028 ±0.0044 0.152 0.0152
Eucalyptol 0.006 / 0.018 ±0.0031 0.124 0.0124
Citronellol 0.003 / 0.010 ±0.0052 0.107 0.0107
γ-Terpinene 0.006 / 0.018 ±0.0017 0.098 0.0098
α-Phellandrene 0.006 / 0.020 ±0.0008 0.060 0.0060
α-Terpinene 0.005 / 0.017 ±0.0008 0.053 0.0053
p-Cymene 0.005 / 0.016 ±0.0009 0.033 0.0033
Sabinene Hydrate 0.006 / 0.022 N/A <LOQ <LOQ
Nerol 0.003 / 0.011 N/A ND ND
Cedrol 0.008 / 0.027 N/A ND ND
Camphor 0.006 / 0.019 N/A ND ND
Menthol 0.008 / 0.025 N/A ND ND
Geraniol 0.002 / 0.007 N/A ND ND
Pulegone 0.003 / 0.011 N/A ND ND
Sabinene 0.004 / 0.014 N/A ND ND
Valencene 0.009 / 0.030 N/A ND ND
Isoborneol 0.004 / 0.012 N/A ND ND
Isopulegol 0.005 / 0.016 N/A ND ND
Δ3-Carene 0.005 / 0.018 N/A ND ND
α-Cedrene 0.005 / 0.016 N/A ND ND
Geranyl Acetate 0.004 / 0.014 N/A ND ND
TOTAL 100.066 mg/g 10.0066%
Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

03/24/2021

FAIL

Swipe left on table to see additional columns

Compound LOD/LOQ
(μg/g) 		Action Limit
(μg/g) 		Measurement
Uncertainty
(μg/g) 		Result
(μg/g) 		Result
Aldicarb 0.03 / 0.08 ≥ LOD N/A ND Pass
Carbofuran 0.02 / 0.05 ≥ LOD N/A ND Pass
Chlordane* 0.03 / 0.08 ≥ LOD N/A ND Pass
Chlorfenapyr* 0.03 / 0.10 ≥ LOD N/A ND Pass
Chlorpyrifos 0.02 / 0.06 ≥ LOD N/A ND Pass
Coumaphos 0.02 / 0.07 ≥ LOD N/A ND Pass
Daminozide 0.02 / 0.07 ≥ LOD N/A ND Pass
Dichlorvos (DDVP) 0.03 / 0.09 ≥ LOD N/A ND Pass
Dimethoate 0.03 / 0.08 ≥ LOD N/A ND Pass
Ethoprophos 0.03 / 0.10 ≥ LOD N/A ND Pass
Etofenprox 0.02 / 0.06 ≥ LOD N/A ND Pass
Fenoxycarb 0.03 / 0.08 ≥ LOD N/A ND Pass
Fipronil 0.03 / 0.08 ≥ LOD N/A ND Pass
Imazalil 0.02 / 0.06 ≥ LOD N/A ND Pass
Methiocarb 0.02 / 0.07 ≥ LOD N/A ND Pass
Mevinphos 0.03 / 0.09 ≥ LOD N/A ND Pass
Paclobutrazol 0.02 / 0.05 ≥ LOD N/A ND Pass
Parathion-methyl 0.03 / 0.10 ≥ LOD N/A ND Pass
Propoxur 0.03 / 0.09 ≥ LOD N/A ND Pass
Spiroxamine 0.03 / 0.08 ≥ LOD N/A ND Pass
Thiacloprid 0.03 / 0.10 ≥ LOD N/A ND Pass
Abamectin 0.03 / 0.10 0.1 N/A ND Pass
Acephate 0.02 / 0.07 0.1 N/A ND Pass
Acequinocyl 0.02 / 0.07 0.1 N/A ND Pass
Acetamiprid 0.02 / 0.05 0.1 N/A ND Pass
Azoxystrobin 0.02 / 0.07 0.1 ±0.008 0.20 Fail
Bifenazate 0.01 / 0.04 0.1 N/A <LOQ Pass
Bifenthrin 0.02 / 0.05 3 ±0.006 0.12 Pass
Boscalid 0.03 / 0.09 0.1 N/A ND Pass
Captan 0.19 / 0.57 0.7 N/A <LOQ Pass
Carbaryl 0.02 / 0.06 0.5 N/A ND Pass
Chlorantraniliprole 0.04 / 0.12 10 N/A ND Pass
Clofentezine 0.03 / 0.09 0.1 N/A ND Pass
Cyfluthrin 0.12 / 0.38 2 N/A ND Pass
Cypermethrin 0.11 / 0.32 1 N/A ND Pass
Diazinon 0.02 / 0.05 0.1 N/A ND Pass
Dimethomorph 0.03 / 0.09 2 N/A ND Pass
Etoxazole 0.02 / 0.06 0.1 N/A ND Pass
Fenhexamid 0.03 / 0.09 0.1 N/A ND Pass
Fenpyroximate 0.02 / 0.06 0.1 N/A ND Pass
Flonicamid 0.03 / 0.10 0.1 N/A ND Pass
Fludioxonil 0.03 / 0.10 0.1 N/A ND Pass
Hexythiazox 0.02 / 0.07 0.1 N/A ND Pass
Imidacloprid 0.04 / 0.11 5 N/A ND Pass
Kresoxim-methyl 0.02 / 0.07 0.1 N/A ND Pass
Malathion 0.03 / 0.09 0.5 N/A <LOQ Pass
Metalaxyl 0.02 / 0.07 2 N/A ND Pass
Methomyl 0.03 / 0.10 1 N/A ND Pass
Myclobutanil 0.03 / 0.09 0.1 N/A ND Pass
Naled 0.02 / 0.07 0.1 N/A ND Pass
Oxamyl 0.04 / 0.11 0.5 N/A ND Pass
Pentachloronitrobenzene (Quintozene)* 0.03 / 0.09 0.1 N/A ND Pass
Permethrin 0.04 / 0.12 0.5 ±0.009 0.14 Pass
Phosmet 0.03 / 0.10 0.1 N/A ND Pass
Piperonyl Butoxide 0.02 / 0.07 3 N/A ND Pass
Prallethrin 0.03 / 0.08 0.1 N/A ND Pass
Propiconazole 0.02 / 0.07 0.1 N/A <LOQ Pass
Pyrethrins 0.04 / 0.12 0.5 N/A ND Pass
Pyridaben 0.02 / 0.07 0.1 N/A ND Pass
Spinetoram 0.02 / 0.07 0.1 N/A ND Pass
Spinosad 0.02 / 0.07 0.1 N/A ND Pass
Spiromesifen 0.02 / 0.05 0.1 N/A ND Pass
Spirotetramat 0.02 / 0.06 0.1 N/A ND Pass
Tebuconazole 0.02 / 0.07 0.1 N/A ND Pass
Thiamethoxam 0.03 / 0.10 5 N/A ND Pass
Trifloxystrobin 0.03 / 0.08 0.1 N/A ND Pass

Hide Failed Pesticide Details

Fail

Azoxystrobin | Trade Names: Amistar, Abound, Heritage, Olympus, Ortiva, Priori Xtra, Bankit, Quadris, Azoxy 2SC...etc.; A commonly used systemic strobilurin fungicide. Although it has a low toxicity in mammals, it is moderately toxic to aquatic organisms, birds, earthoworms and honeybees.

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

03/23/2021

PASS

Swipe left on table to see additional columns

Compound LOD/LOQ
(μg/g) 		Action Limit
(μg/g) 		Measurement
Uncertainty
(μg/g) 		Result
(μg/g) 		Result
Arsenic 0.02 / 0.1 0.2 N/A ND Pass
Cadmium 0.02 / 0.05 0.2 N/A ND Pass
Lead 0.04 / 0.1 0.5 N/A ND Pass
Mercury 0.002 / 0.01 0.1 N/A ND Pass

Notes

COA Notes:

CoA Amended Update: Order Details-Name

COA ID: 210322W013-002

These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

Sample Certification: California Code of Regulations Title 4 Division 19. Department of Cannabis Control Business and Professions Code. Reference: Sections 26100, 26104 and 26110, Business and Professions Code.

Decision Rule: Statements of conformity (e.g. Pass/Fail) to specifications are made in this report without taking measurement uncertainty into account. Where statements of conformity are made in this report, the following decision rules are applied: PASS - Results within limits/specifications, FAIL - Results exceed limits/specifications.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT), μg/g = ppm, μg/kg = ppb

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