DOUGH BOY

Certificate of Analysis

HEMP QUALITY ASSURANCE TEST

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Sample Name:

DOUGH BOY

Flower, Inhalable

Total THC 0.6894%

Total CBD 15.7258%

Sum Cannabinoids 20.1197%

Total Cannabinoids 17.8337%

Total Terpenoids 1.7452%
PhytoFacts^®

Top 3 Terpenoids

Myrcene 0.9144%
α-Pinene 0.1827%
β-Caryophyllene 0.1563%

Sample Information

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Sample Details

Sample ID:200129N040

Batch Number:

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Cultivator / Manufacturer

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Distributor / Tested For

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PhytoFacts® Report

aroma

flavor

effect

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The PhytoFacts chemometric report provides additional cannabinoid and terpenoid details, including dominant terpenes, entourage effects, aroma, flavor, and more.

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Cannabinoid Analysis - Summary

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Total THC: 0.6894%

Total CBD: 15.7258%

Sum of Cannabinoids: 20.1197%

Total Cannabinoids: 17.8337%

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ⁹-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ⁹-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ⁸-THC + CBL + CBN

Total Cannabinoids = (Δ⁹-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ⁸-THC + CBL + CBN

Why are Sum of Cannabinoids and Total Cannabinoids calculated separately?

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

36 tested, Top 3 Highlighted

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Total Terpenoids: 1.7452%

Myrcene (0.9144%)

α-Pinene (0.1827%)

β-Caryophyllene (0.1563%)

Safety Analysis - Summary

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Pesticides: Pass

Microbiology (PCR): Pass

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Cannabinoid Analysis

Tested

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 0.6894%

(Δ⁹-THC+0.877*THCa)

Total CBD: 15.7258%

(CBD+0.877*CBDa)

Total Cannabinoids: 17.8337%

Total CBG: 0.5501%

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 0.791%

Total CBC (CBC+0.877*CBCa)

Total CBDV: 0.0774%

Total CBDV (CBDV+0.877*CBDVa)

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The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

01/31/2020

Result Views

Table Pie Chart

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Compound	LOD/LOQ (mg/g)	Result (mg/g)	Result (%)
Cannabidiolic Acid (CBDa)	0.052 / 0.156	165.733	16.5733
Cannabidiol (CBD)	0.059 / 0.180	11.910	1.1910
Cannabichromenic Acid (CBCa)	0.233 / 0.705	7.802	0.7802
Tetrahydrocannabinolic Acid (THCa)	0.052 / 0.156	5.987	0.5987
Cannabigerolic Acid (CBGa)	0.034 / 0.102	5.457	0.5457
Δ9 Tetrahydrocannabinol (Δ9THC)	0.052 / 0.158	1.643	0.1643
Cannabichromene (CBC)	0.048 / 0.146	1.068	0.1068
Cannabidivarinic Acid (CBDVa)	0.030 / 0.090	0.882	0.0882
Cannabigerol (CBG)	0.048 / 0.144	0.715	0.0715
Cannabicyclol (CBL)	0.114 / 0.346	ND	ND
Cannabinol (CBN)	0.052 / 0.157	ND	ND
Cannabidivarin (CBDV)	0.027 / 0.080	ND	ND
Tetrahydrocannabivarin (THCV)	0.045 / 0.137	ND	ND
Tetrahydrocannabivarinic Acid (THCVa)	0.088 / 0.267	ND	ND
∆8 Tetrahydrocannabinol (Δ8THC)	0.074 / 0.224	ND	ND
SUM OF CANNABINOIDS		201.197 mg/g	20.1197%

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpenoid Analysis

Tested

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

View PhytoFacts COA

See a visual representation of this sample's cannabinoid and terpenoid properties, including entourage effects, aroma, and flavor profile.

Summary

Total Terpenoids (mg/g): 17.452 mg/g

Total Terpenoids (%): 1.7452%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume. To see more detail for terpenoid content, view the PhytoFacts report.

Myrcene 0.9144%
A monoterpene with a fragrance that can be described as peppery, spicy, herbal, floral and woody. Although it has a pleasant odor, it is typically used by the perfume industry as precursor for developing other fragrances. Found in hops, houttuynia, bay, thyme, lemon grass, mango, verbena, cardamom, citrus...etc.

α-Pinene 0.1827%
One of two isomers of the monoterpene Pinene, the most abundant terpene in the natural world. It is responsible for the distinct aroma of many coniferous trees, particularly pines, from which it derives its name. It is a primary constituent of turpentine. Found in pines, rose gun, parsley, frankincense, guava, juniper, rosemary, nutmeg, blue gum, valerian...etc.

β-Caryophyllene 0.1563%
A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB² receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

02/03/2020

Result Views

Table Bar Graph

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Compound	LOD/LOQ (mg/g)	Result (mg/g)	Result (%)
Myrcene	0.03 / 0.092	9.144	0.9144
α-Pinene	0.028 / 0.084	1.827	0.1827
β-Caryophyllene	0.029 / 0.087	1.563	0.1563
Guaiol	0.035 / 0.106	1.135	0.1135
α-Humulene	0.017 / 0.051	0.831	0.0831
Limonene	0.04 / 0.12	0.74	0.074
β-Pinene	0.016 / 0.048	0.640	0.0640
α-Bisabolol	0.057 / 0.172	0.418	0.0418
Linalool	0.043 / 0.13	0.34	0.034
β-Ocimene	0.053 / 0.16	0.31	0.031
Terpineol	0.029 / 0.087	0.201	0.0201
Nerolidol	0.05 / 0.15	0.16	0.016
Caryophyllene Oxide	0.011 / 0.034	0.143	0.0143
Fenchol	0.051 / 0.153	<LOQ	<LOQ
Camphene	0.038 / 0.116	<LOQ	<LOQ
Valencene	0.018 / 0.055	<LOQ	<LOQ
Nerol	0.042 / 0.128	ND	ND
Cedrol	0.022 / 0.066	ND	ND
Borneol	0.063 / 0.19	ND	ND
Camphor	0.08 / 0.242	ND	ND
Menthol	0.043 / 0.129	ND	ND
Fenchone	0.06 / 0.181	ND	ND
Geraniol	0.037 / 0.112	ND	ND
Pulegone	0.016 / 0.047	ND	ND
Sabinene	0.024 / 0.073	ND	ND
Eucalyptol	0.051 / 0.155	ND	ND
Isoborneol	0.028 / 0.085	ND	ND
Isopulegol	0.026 / 0.08	ND	ND
Terpinolene	0.042 / 0.128	ND	ND
Δ³-Carene	0.028 / 0.085	ND	ND
α-Cedrene	0.012 / 0.035	ND	ND
Geranyl Acetate	0.025 / 0.076	ND	ND
α-Terpinene	0.051 / 0.155	ND	ND
γ-Terpinene	0.038 / 0.114	ND	ND
Sabinene Hydrate	0.046 / 0.138	ND	ND
α-Phellandrene	0.048 / 0.144	ND	ND
TOTAL		17.452 mg/g	1.7452%

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Pesticide Analysis

Pass

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

01/31/2020

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Result (μg/g)	Result
Abamectin	0.030 / 0.091	0.1	ND	Pass
Bifenazate	0.012 / 0.035	0.1	ND	Pass
Bifenthrin	0.013 / 0.038	3	ND	Pass
Boscalid	0.008 / 0.023	0.1	ND	Pass
Etoxazole	0.007 / 0.022	0.1	ND	Pass
Imidacloprid	0.017 / 0.050	5	ND	Pass
Myclobutanil	0.015 / 0.044	0.1	ND	Pass
Piperonyl Butoxide	0.007 / 0.020	3	ND	Pass
Pyrethrins	0.012 / 0.036	0.5	ND	Pass
Spinosad	0.010 / 0.031	0.1	ND	Pass
Spiromesifen	0.005 / 0.015	0.1	ND	Pass
Spirotetramat	0.014 / 0.042	0.1	ND	Pass

Microbiology Analysis

Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants

Microbiology Test Results (PCR)

01/31/2020

PASS

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Compound	Action Limit	Result	Result
Salmonella spp.	Not Detected in 1g	ND	Pass
Aspergillus niger	Not Detected in 1g	ND	Pass
Aspergillus flavus	Not Detected in 1g	ND	Pass
Aspergillus terreus	Not Detected in 1g	ND	Pass
Aspergillus fumigatus	Not Detected in 1g	ND	Pass
Shiga toxin-producing Escherichia coli	Not Detected in 1g	ND	Pass

COA ID: 200129N040-001

For quality assurance purposes. Not a Regulatory Hemp Lab Test Report. These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

Sample Certification: California Code of Regulations Title 4 Division 19. Department of Cannabis Control Business and Professions Code. Reference: Sections 26100, 26104 and 26110, Business and Professions Code.

Decision Rule: Statements of conformity (e.g. Pass/Fail) to specifications are made in this report without taking measurement uncertainty into account. Where statements of conformity are made in this report, the following decision rules are applied: PASS - Results within limits/specifications, FAIL - Results exceed limits/specifications.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT), μg/g = ppm, μg/kg = ppb