Distillate

Certificate of Analysis

HEMP QUALITY ASSURANCE TEST

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Sample Name:

Distillate

Concentrate, Product Inhalable

Total THC 0.2436%

Total CBD 56.3682%

Sum Cannabinoids 57.4252%

Total Cannabinoids 57.4252%

Total Terpenoids 5.6028%

Top 3 Terpenoids

Terpinolene 3.0595%
α-Bisabolol 0.9333%
β-Caryophyllene 0.3924%

Sample Information

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Sample Details

Sample ID:200207S005

Batch Number:

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Cannabinoid Analysis - Summary

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Total THC: 0.2436%

Total CBD: 56.3682%

Sum of Cannabinoids: 57.4252%

Total Cannabinoids: 57.4252%

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ⁹-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ⁹-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ⁸-THC + CBL + CBN

Total Cannabinoids = (Δ⁹-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ⁸-THC + CBL + CBN

Why are Sum of Cannabinoids and Total Cannabinoids calculated separately?

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

36 tested, Top 3 Highlighted

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Total Terpenoids: 5.6028%

Terpinolene (3.0595%)

α-Bisabolol (0.9333%)

β-Caryophyllene (0.3924%)

Safety Analysis - Summary

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Pesticides: Pass

Residual Solvents: Pass

Heavy Metals: Pass

Vitamin E: ND

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Cannabinoid Analysis

Tested

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 0.2436%

(Δ⁹-THC+0.877*THCa)

Total CBD: 56.3682%

(CBD+0.877*CBDa)

Total Cannabinoids: 57.4252%

Total CBG: 0.0823%

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 0.2888%

Total CBC (CBC+0.877*CBCa)

Total CBDV: 0.4423%

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

02/09/2020

Result Views

Table Pie Chart

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Compound	LOD/LOQ (mg/g)	Result (mg/g)	Result (%)
Cannabidiol (CBD)	0.052 / 0.158	563.682	56.3682
Cannabidivarin (CBDV)	0.021 / 0.063	4.423	0.4423
Cannabichromene (CBC)	0.031 / 0.094	2.888	0.2888
Δ9 Tetrahydrocannabinol (Δ9THC)	0.052 / 0.158	2.436	0.2436
Cannabigerol (CBG)	0.030 / 0.092	0.823	0.0823
∆8 Tetrahydrocannabinol (Δ8THC)	0.053 / 0.162	ND	ND
Tetrahydrocannabinolic Acid (THCa)	0.052 / 0.156	ND	ND
Tetrahydrocannabivarin (THCV)	0.023 / 0.069	ND	ND
Tetrahydrocannabivarinic Acid (THCVa)	0.091 / 0.276	ND	ND
Cannabidiolic Acid (CBDa)	0.052 / 0.156	ND	ND
Cannabidivarinic Acid (CBDVa)	0.037 / 0.111	ND	ND
Cannabigerolic Acid (CBGa)	0.044 / 0.133	ND	ND
Cannabicyclol (CBL)	0.130 / 0.393	ND	ND
Cannabinol (CBN)	0.052 / 0.157	ND	ND
Cannabichromenic Acid (CBCa)	0.129 / 0.392	ND	ND
SUM OF CANNABINOIDS		574.252 mg/g	57.4252%

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpenoid Analysis

Tested

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

Summary

Total Terpenoids (mg/g): 56.028 mg/g

Total Terpenoids (%): 5.6028%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume.

Terpinolene 3.0595%
Also known as δ-terpinene, it is of four isomers of the monoterpene Terpinene. It has a fragrance that can be described as fresh, woody, piney, herbal with a hint of lemon. Found in conifers, cumin, apple, rosemary, sage, tea tree, lilac, nutmeg...etc.

α-Bisabolol 0.9333%
A sesquiterpene alcohol with a fragrance that can be described as floral, peppery, sweet and clean. Found in chamomile, figwort, yarrow, skullcaps, lavender, ironwort, germander...etc.

β-Caryophyllene 0.3924%
A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB² receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

02/10/2020

Result Views

Table Bar Graph

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Compound	LOD/LOQ (mg/g)	Result (mg/g)	Result (%)
Terpinolene	0.045 / 0.135	30.595	3.0595
α-Bisabolol	0.034 / 0.102	9.333	0.9333
β-Caryophyllene	0.036 / 0.108	3.924	0.3924
Guaiol	0.044 / 0.132	2.555	0.2555
α-Humulene	0.025 / 0.076	2.225	0.2225
Linalool	0.038 / 0.116	1.846	0.1846
Myrcene	0.054 / 0.164	1.456	0.1456
Limonene	0.026 / 0.078	0.993	0.0993
Fenchone	0.061 / 0.184	0.933	0.0933
Terpineol	0.045 / 0.136	0.632	0.0632
Caryophyllene Oxide	0.055 / 0.167	0.608	0.0608
α-Pinene	0.044 / 0.135	0.558	0.0558
β-Pinene	0.054 / 0.162	0.196	0.0196
Valencene	0.015 / 0.046	0.174	0.0174
α-Phellandrene	0.073 / 0.222	<LOQ	<LOQ
Eucalyptol	0.042 / 0.126	<LOQ	<LOQ
γ-Terpinene	0.06 / 0.181	<LOQ	<LOQ
Borneol	0.097 / 0.293	<LOQ	<LOQ
Pulegone	0.045 / 0.135	<LOQ	<LOQ
Camphene	0.053 / 0.16	ND	ND
Sabinene	0.054 / 0.165	ND	ND
Δ³-Carene	0.057 / 0.174	ND	ND
α-Terpinene	0.06 / 0.18	ND	ND
β-Ocimene	0.056 / 0.171	ND	ND
Sabinene Hydrate	0.036 / 0.108	ND	ND
Fenchol	0.045 / 0.138	ND	ND
Isopulegol	0.026 / 0.08	ND	ND
Camphor	0.108 / 0.327	ND	ND
Isoborneol	0.066 / 0.201	ND	ND
Menthol	0.044 / 0.135	ND	ND
Nerol	0.045 / 0.137	ND	ND
Geraniol	0.033 / 0.1	ND	ND
Geranyl Acetate	0.031 / 0.095	ND	ND
α-Cedrene	0.034 / 0.102	ND	ND
Nerolidol	0.07 / 0.212	ND	ND
Cedrol	0.057 / 0.173	ND	ND
TOTAL		56.028 mg/g	5.6028%

Learn more

Pesticide Analysis

Pass

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

02/10/2020

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Result (μg/g)	Result
Abamectin	0.030 / 0.091	0.1	ND	Pass
Bifenazate	0.012 / 0.035	0.1	ND	Pass
Bifenthrin	0.013 / 0.038	3.0	ND	Pass
Boscalid	0.008 / 0.023	0.1	ND	Pass
Etoxazole	0.007 / 0.022	0.1	ND	Pass
Imidacloprid	0.017 / 0.050	5.0	ND	Pass
Myclobutanil	0.015 / 0.044	0.1	ND	Pass
Piperonyl Butoxide	0.007 / 0.020	3.0	ND	Pass
Pyrethrins	0.012 / 0.036	0.5	ND	Pass
Spinosad	0.010 / 0.031	0.1	ND	Pass
Spiromesifen	0.005 / 0.015	0.1	ND	Pass
Spirotetramat	0.014 / 0.042	0.1	ND	Pass

Residual Solvents Analysis

Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

02/09/2020

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Result (μg/g)	Result
1,2-Dichloroethane	0.111 / 0.336	1.0	ND	Pass
Benzene	0.043 / 0.132	1.0	ND	Pass
Chloroform	0.064 / 0.195	1.0	ND	Pass
Ethylene Oxide	0.136 / 0.413	1.0	ND	Pass
Dichloromethane (Methylene Chloride)	0.172 / 0.521	1.0	ND	Pass
Trichloroethylene	0.040 / 0.120	1.0	ND	Pass
Acetone	14.703 / 44.549	5000.0	44.943	Pass
Acetonitrile	2.727 / 8.262	410.0	ND	Pass
n-Butane	5.672 / 17.185	5000.0	ND	Pass
Ethanol	11.775 / 35.679	5000.0	<LOQ	Pass
Ethyl Acetate	16.227 / 49.169	5000.0	ND	Pass
Ethyl Ether	11.608 / 35.172	5000.0	ND	Pass
n-Heptane	12.982 / 39.336	5000.0	ND	Pass
n-Hexane	1.816 / 5.502	290.0	ND	Pass
2-Propanol (Isopropyl Alcohol)	15.358 / 46.536	5000.0	ND	Pass
Methanol	15.584 / 47.220	3000.0	ND	Pass
n-Pentane	12.355 / 37.434	5000.0	ND	Pass
Propane	1.359 / 4.117	5000.0	ND	Pass
Toluene	7.174 / 21.736	890.0	ND	Pass
Total Xylenes	34.438 / 104.347	2170.0	ND	Pass

Heavy Metals Analysis

Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

02/10/2020

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Result (μg/g)	Result
Arsenic	0.013 / 0.039	0.2	ND	Pass
Cadmium	0.012 / 0.035	0.2	ND	Pass
Lead	0.031 / 0.095	0.5	ND	Pass
Mercury	0.002 / 0.005	0.1	ND	Pass

Vitamin E Analysis

Not Detected

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 6793 - Analysis of Vitamin E by HPLC-DAD

Vitamin E Test Results

02/10/2020

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Compound	LOD/LOQ (mg/g)	Result (mg/g)	Result (%)
Tocopheryl Acetate	10 / 10	ND	ND
α-Tocopherol	10 / 10	ND	ND
ß-Tocopherol / γ-Tocopherol	10 / 10	ND	ND
δ-Tocopherol	10 / 10	ND	ND

* ß-Tocopherol / γ-Tocopherol reported as a sum

COA ID: 200207S005-001

For quality assurance purposes. Not a Regulatory Hemp Lab Test Report. These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

Sample Certification: California Code of Regulations Title 4 Division 19. Department of Cannabis Control Business and Professions Code. Reference: Sections 26100, 26104 and 26110, Business and Professions Code.

Decision Rule: Statements of conformity (e.g. Pass/Fail) to specifications are made in this report without taking measurement uncertainty into account. Where statements of conformity are made in this report, the following decision rules are applied: PASS - Results within limits/specifications, FAIL - Results exceed limits/specifications.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT)