Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

Distillate

Concentrate, Product Inhalable

Date Issued:

02/10/2020

Total THC 0.2436%
Total CBD 56.3682%
Sum Cannabinoids 57.4252%
Total Cannabinoids 57.4252%
Total Terpenoids 5.6028%
PhytoFacts®
Top 3 Terpenoids
  1. Terpinolene 3.0595%
  2. α-Bisabolol 0.9333%
  3. β-Caryophyllene 0.3924%

Sample Information

Sample Details

Sample ID:200207S005

Batch Number:

Cultivator / Manufacturer

Show Details

Distributor / Tested For

Show Details

PhytoFacts® Report

aroma
flavor
effect

The PhytoFacts chemometric report provides additional cannabinoid and terpenoid details, including dominant terpenes, entourage effects, aroma, flavor, and more.

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Cannabinoid Analysis - Summary

Total THC: 0.2436%

Total CBD: 56.3682%

Sum of Cannabinoids: 57.4252%

Total Cannabinoids: 57.4252%

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

36 tested, Top 3 Highlighted

Total Terpenoids: 5.6028%

 
 
 

1

Terpinolene (3.0595%)

2

α-Bisabolol (0.9333%)

3

β-Caryophyllene (0.3924%)

Safety Analysis - Summary

Pesticides: Pass

Residual Solvents: Pass

Heavy Metals: Pass

Vitamin E: ND

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 0.2436%

9-THC+0.877*THCa)

Total CBD: 56.3682%

(CBD+0.877*CBDa)

Total Cannabinoids: 57.4252%

Total CBG: 0.0823%

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 0.2888%

Total CBC (CBC+0.877*CBCa)

Total CBDV: 0.4423%

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

02/09/2020

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Result
(mg/g)
Result
(%)
Cannabidiol (CBD) 0.052 / 0.158 563.682 56.3682
Cannabidivarin (CBDV) 0.021 / 0.063 4.423 0.4423
Cannabichromene (CBC) 0.031 / 0.094 2.888 0.2888
Δ9 Tetrahydrocannabinol (Δ9THC) 0.052 / 0.158 2.436 0.2436
Cannabigerol (CBG) 0.030 / 0.092 0.823 0.0823
Cannabicyclol (CBL) 0.130 / 0.393 ND ND
Cannabinol (CBN) 0.052 / 0.157 ND ND
Cannabichromenic Acid (CBCa) 0.129 / 0.392 ND ND
Cannabidiolic Acid (CBDa) 0.052 / 0.156 ND ND
Cannabigerolic Acid (CBGa) 0.044 / 0.133 ND ND
Tetrahydrocannabivarin (THCV) 0.023 / 0.069 ND ND
Tetrahydrocannabinolic Acid (THCa) 0.052 / 0.156 ND ND
Cannabidivarinic Acid (CBDVa) 0.037 / 0.111 ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.091 / 0.276 ND ND
∆8 Tetrahydrocannabinol (Δ8THC) 0.053 / 0.162 ND ND
SUM OF CANNABINOIDS 574.252 mg/g 57.4252%
Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

View PhytoFacts COA

See a visual representation of this sample's cannabinoid and terpenoid properties, including entourage effects, aroma, and flavor profile.

Summary

Total Terpenoids (mg/g): 56.028 mg/g

Total Terpenoids (%): 5.6028%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume. To see more detail for terpenoid content, view the PhytoFacts report.

  1. Terpinolene 3.0595%

    Also known as δ-terpinene, it is of four isomers of the monoterpene Terpinene. It has a fragrance that can be described as fresh, woody, piney, herbal with a hint of lemon. Found in conifers, cumin, apple, rosemary, sage, tea tree, lilac, nutmeg...etc.

  2. α-Bisabolol 0.9333%

    A sesquiterpene alcohol with a fragrance that can be described as floral, peppery, sweet and clean. Found in chamomile, figwort, yarrow, skullcaps, lavender, ironwort, germander...etc.

  3. β-Caryophyllene 0.3924%

    A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB2 receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

02/10/2020

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Result
(mg/g)
Result
(%)
Terpinolene 0.045 / 0.135 30.595 3.0595
α-Bisabolol 0.034 / 0.102 9.333 0.9333
β-Caryophyllene 0.036 / 0.108 3.924 0.3924
Guaiol 0.044 / 0.132 2.555 0.2555
α-Humulene 0.025 / 0.076 2.225 0.2225
Linalool 0.038 / 0.116 1.846 0.1846
Myrcene 0.054 / 0.164 1.456 0.1456
Limonene 0.026 / 0.078 0.993 0.0993
Fenchone 0.061 / 0.184 0.933 0.0933
Terpineol 0.045 / 0.136 0.632 0.0632
Caryophyllene Oxide 0.055 / 0.167 0.608 0.0608
α-Pinene 0.044 / 0.135 0.558 0.0558
β-Pinene 0.054 / 0.162 0.196 0.0196
Valencene 0.015 / 0.046 0.174 0.0174
Borneol 0.097 / 0.293 <LOQ <LOQ
Pulegone 0.045 / 0.135 <LOQ <LOQ
Eucalyptol 0.042 / 0.126 <LOQ <LOQ
γ-Terpinene 0.06 / 0.181 <LOQ <LOQ
α-Phellandrene 0.073 / 0.222 <LOQ <LOQ
Nerol 0.045 / 0.137 ND ND
Cedrol 0.057 / 0.173 ND ND
Camphor 0.108 / 0.327 ND ND
Fenchol 0.045 / 0.138 ND ND
Menthol 0.044 / 0.135 ND ND
Camphene 0.053 / 0.16 ND ND
Geraniol 0.033 / 0.1 ND ND
Sabinene 0.054 / 0.165 ND ND
Nerolidol 0.07 / 0.212 ND ND
Isoborneol 0.066 / 0.201 ND ND
Isopulegol 0.026 / 0.08 ND ND
β-Ocimene 0.056 / 0.171 ND ND
Δ3-Carene 0.057 / 0.174 ND ND
α-Cedrene 0.034 / 0.102 ND ND
Geranyl Acetate 0.031 / 0.095 ND ND
α-Terpinene 0.06 / 0.18 ND ND
Sabinene Hydrate 0.036 / 0.108 ND ND
TOTAL 56.028 mg/g 5.6028%
Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

02/10/2020

PASS

Swipe left on table to see additional columns

Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Result
(μg/g)
Result
Abamectin 0.030 / 0.091 0.1 ND Pass
Bifenazate 0.012 / 0.035 0.1 ND Pass
Bifenthrin 0.013 / 0.038 3 ND Pass
Boscalid 0.008 / 0.023 0.1 ND Pass
Etoxazole 0.007 / 0.022 0.1 ND Pass
Imidacloprid 0.017 / 0.050 5 ND Pass
Myclobutanil 0.015 / 0.044 0.1 ND Pass
Piperonyl Butoxide 0.007 / 0.020 3 ND Pass
Pyrethrins 0.012 / 0.036 0.5 ND Pass
Spinosad 0.010 / 0.031 0.1 ND Pass
Spiromesifen 0.005 / 0.015 0.1 ND Pass
Spirotetramat 0.014 / 0.042 0.1 ND Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

02/09/2020

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Result
(μg/g)
Result
1,2-Dichloroethane 0.111 / 0.336 1 ND Pass
Benzene 0.043 / 0.132 1 ND Pass
Chloroform 0.064 / 0.195 1 ND Pass
Dichloromethane (Methylene Chloride) 0.172 / 0.521 1 ND Pass
Ethylene Oxide 0.136 / 0.413 1 ND Pass
Trichloroethylene 0.040 / 0.120 1 ND Pass
2-Propanol (Isopropyl Alcohol) 15.358 / 46.536 5000 ND Pass
Acetone 14.703 / 44.549 5000 44.943 Pass
Acetonitrile 2.727 / 8.262 410 ND Pass
Ethanol 11.775 / 35.679 5000 <LOQ Pass
Ethyl Acetate 16.227 / 49.169 5000 ND Pass
Ethyl Ether 11.608 / 35.172 5000 ND Pass
Methanol 15.584 / 47.220 3000 ND Pass
n-Butane 5.672 / 17.185 5000 ND Pass
n-Heptane 12.982 / 39.336 5000 ND Pass
n-Hexane 1.816 / 5.502 290 ND Pass
n-Pentane 12.355 / 37.434 5000 ND Pass
Propane 1.359 / 4.117 5000 ND Pass
Toluene 7.174 / 21.736 890 ND Pass
Total Xylenes 34.438 / 104.347 2170 ND Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

02/10/2020

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Result
(μg/g)
Result
Arsenic 0.013 / 0.039 0.2 ND Pass
Cadmium 0.012 / 0.035 0.2 ND Pass
Lead 0.031 / 0.095 0.5 ND Pass
Mercury 0.002 / 0.005 0.1 ND Pass

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 6793 - Analysis of Vitamin E by HPLC-DAD

Vitamin E Test Results

02/10/2020

ND

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Compound LOD/LOQ
(mg/g)
Result
(mg/g)
Result
(%)
α-Tocopherol 10 / 10 ND ND
δ-Tocopherol 10 / 10 ND ND
Tocopheryl Acetate 10 / 10 ND ND
ß-Tocopherol / γ-Tocopherol 10 / 10 ND ND

* ß-Tocopherol / γ-Tocopherol reported as a sum

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