Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

R+R Medicinals 2500mg Organic Full Spectrum Tincture - Fresh Mint

Infused, Hemp Infused

Date Issued:

01/22/2022

Serving Size:

0.5 milliliters

Total THC 68.850 mg/unit
Total CBD 2697.390 mg/unit
Sum Cannabinoids 2997.210 mg/unit
Total Cannabinoids 2997.210 mg/unit
Total Terpenoids 0.4569%
Top 3 Terpenoids
  1. β-Caryophyllene 0.1213%
  2. Guaiol 0.0654%
  3. α-Bisabolol 0.0654%

Sample Information

Sample Details

Sample ID:220117R010

Batch Number:0015

Cultivator / Manufacturer

Show Details

Distributor / Tested For

Show Details

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Cannabinoid Analysis - Summary

Total THC: 68.850 mg/unit

Total CBD: 2697.390 mg/unit

Sum of Cannabinoids: 2997.210 mg/unit

Total Cannabinoids: 2997.210 mg/unit

Density:0.955 g/mL

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

Total Terpenoids: 0.4569%

 
 
 

1

β-Caryophyllene (0.1213%)

2

Guaiol (0.0654%)

3

α-Bisabolol (0.0654%)

Safety Analysis - Summary

Pesticides: Pass

Mycotoxins: Pass

Residual Solvents: Pass

Heavy Metals: Pass

Microbiology (PCR): Pass

Microbiology (Plating): Pass

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 68.850 mg/unit

(Δ9-THC+0.877*THCa)

Total CBD: 2697.390 mg/unit

(CBD+0.877*CBDa)

Total Cannabinoids: 2997.210 mg/unit

Total CBG: 99.180 mg/unit

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 73.710 mg/unit

Total CBC (CBC+0.877*CBCa)

Total CBDV: 28.260 mg/unit

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

01/19/2022

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/mL)
Measurement
Uncertainty
(mg/mL)
Result
(mg/mL)
Result
(%)
Cannabidiol (CBD) 0.004 / 0.011 ±4.3068 89.913 9.4150
Cannabigerol (CBG) 0.002 / 0.006 ±0.2056 3.306 0.3462
Cannabichromene (CBC) 0.003 / 0.010 ±0.1017 2.457 0.2573
Δ9 Tetrahydrocannabinol (Δ9THC) 0.002 / 0.014 ±0.1618 2.295 0.2403
Cannabidivarin (CBDV) 0.002 / 0.012 ±0.0494 0.942 0.0986
Cannabinol (CBN) 0.001 / 0.007 ±0.0297 0.805 0.0843
Cannabicyclol (CBL) 0.003 / 0.010 ±0.0089 0.189 0.0198
Cannabichromenic Acid (CBCa) 0.001 / 0.015 N/A ND ND
Cannabidiolic Acid (CBDa) 0.001 / 0.026 N/A ND ND
Cannabigerolic Acid (CBGa) 0.002 / 0.007 N/A ND ND
Tetrahydrocannabivarin (THCV) 0.002 / 0.012 N/A ND ND
Tetrahydrocannabinolic Acid (THCa) 0.001 / 0.005 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.001 / 0.018 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.002 / 0.019 N/A ND ND
∆8 Tetrahydrocannabinol (Δ8THC) 0.01 / 0.02 N/A ND ND
SUM OF CANNABINOIDS 99.907 mg/mL 10.4615%
Unit Mass:

30 milliliters

/

Serving Size:

0.5 milliliters

Swipe left on table to see additional columns

Δ9-THC per Unit 68.850 mg/unit
Δ9-THC per Serving 1.148 mg/serving
Total THC per Unit 68.850 mg/unit
Total THC Per Serving 1.148 mg/serving
CBD per Unit 2697.390 mg/unit
CBD per Serving 44.956 mg/serving
Total CBD per Unit 2697.390 mg/unit
Total CBD per Serving 44.956 mg/serving
Sum of Cannabinoids per Unit 2997.210 mg/unit
Sum of Cannabinoids per Serving 49.954 mg/serving
Total Cannabinoids per Unit 2997.210 mg/unit
Total Cannabinoids per Serving 49.955 mg/serving
Density Test Result

0.955 g/mL Tested 01/19/2022 Method: QSP 7870 - Sample Preparation

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

Summary

Total Terpenoids (mg/g): 4.569 mg/g

Total Terpenoids (%): 0.4569%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume.

  1. β-Caryophyllene 0.1213%

    A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB2 receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

  2. Guaiol 0.0654%

    A sesquiterpene alcohol with a fragrance that can be described as floral, piney, herbal and woody. Found in guaiacum, cypress pine, ginseng, melaleuca, goatweed, incense grass...etc.

  3. α-Bisabolol 0.0654%

    A sesquiterpene alcohol with a fragrance that can be described as floral, peppery, sweet and clean. Found in chamomile, figwort, yarrow, skullcaps, lavender, ironwort, germander...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

01/19/2022

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
β-Caryophyllene 0.004 / 0.012 ±0.0432 1.213 0.1213
Guaiol 0.009 / 0.030 ±0.0309 0.654 0.0654
α-Bisabolol 0.008 / 0.026 ±0.0349 0.654 0.0654
Menthol 0.008 / 0.025 ±0.0258 0.645 0.0645
α-Humulene 0.009 / 0.029 ±0.0124 0.386 0.0386
Caryophyllene Oxide 0.010 / 0.033 ±0.0098 0.214 0.0214
trans-β-Farnesene 0.008 / 0.025 ±0.0074 0.208 0.0208
Eucalyptol 0.006 / 0.018 ±0.0028 0.111 0.0111
Nerolidol 0.009 / 0.028 ±0.0067 0.106 0.0106
Limonene 0.005 / 0.016 ±0.0013 0.094 0.0094
Terpineol 0.016 / 0.055 ±0.0045 0.074 0.0074
Myrcene 0.008 / 0.025 ±0.0007 0.055 0.0055
Fenchol 0.010 / 0.034 ±0.0019 0.048 0.0048
Pulegone 0.003 / 0.011 ±0.0013 0.033 0.0033
β-Pinene 0.004 / 0.014 ±0.0003 0.030 0.0030
Sabinene 0.004 / 0.014 ±0.0003 0.023 0.0023
α-Pinene 0.005 / 0.017 ±0.0002 0.021 0.0021
p-Cymene 0.005 / 0.016 N/A <LOQ <LOQ
Citronellol 0.003 / 0.010 N/A <LOQ <LOQ
β-Ocimene 0.011 / 0.038 N/A <LOQ <LOQ
Sabinene Hydrate 0.006 / 0.022 N/A <LOQ <LOQ
Nerol 0.003 / 0.011 N/A ND ND
Cedrol 0.008 / 0.027 N/A ND ND
Borneol 0.005 / 0.016 N/A ND ND
Camphor 0.006 / 0.019 N/A ND ND
Camphene 0.005 / 0.015 N/A ND ND
Fenchone 0.009 / 0.028 N/A ND ND
Geraniol 0.002 / 0.007 N/A ND ND
Linalool 0.009 / 0.032 N/A ND ND
Valencene 0.009 / 0.030 N/A ND ND
Isoborneol 0.004 / 0.012 N/A ND ND
Isopulegol 0.005 / 0.016 N/A ND ND
Terpinolene 0.008 / 0.026 N/A ND ND
Δ3-Carene 0.005 / 0.018 N/A ND ND
α-Cedrene 0.005 / 0.016 N/A ND ND
Geranyl Acetate 0.004 / 0.014 N/A ND ND
α-Terpinene 0.005 / 0.017 N/A ND ND
γ-Terpinene 0.006 / 0.018 N/A ND ND
α-Phellandrene 0.006 / 0.020 N/A ND ND
TOTAL 4.569 mg/g 0.4569%
Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

01/19/2022

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Abamectin 0.032 / 0.097 0.07 N/A ND Pass
Acephate 0.006 / 0.018 0.05 N/A ND Pass
Acequinocyl 0.009 / 0.027 0.03 N/A ND Pass
Acetamiprid 0.016 / 0.049 0.05 N/A ND Pass
Aldicarb 0.030 / 0.090 0.1 N/A ND Pass
Allethrin 0.030 / 0.092 0.1 N/A ND Pass
Atrazine 0.006 / 0.019 0.025 N/A ND Pass
Azadirachtin 0.082 / 0.248 0.5 N/A ND Pass
Azoxystrobin 0.003 / 0.009 0.01 N/A ND Pass
Benzovindiflupyr 0.003 / 0.009 0.01 N/A ND Pass
Bifenazate 0.003 / 0.009 0.01 N/A ND Pass
Bifenthrin 0.021 / 0.064 0.2 N/A ND Pass
Boscalid 0.003 / 0.009 0.01 N/A ND Pass
Buprofezin‡ 0.006 / 0.019 0.02 N/A ND Pass
Captan 0.045 / 0.135 3 N/A ND Pass
Carbaryl 0.007 / 0.020 0.025 N/A ND Pass
Carbofuran 0.003 / 0.008 0.01 N/A ND Pass
Chlorantraniliprole 0.006 / 0.018 0.02 N/A ND Pass
Chlordane* 0.005 / 0.107 0.1 N/A ND Pass
Chlorfenapyr* 0.005 / 0.015 0.1 N/A ND Pass
Chlormequat chloride 0.022 / 0.066 3 N/A ND Pass
Chlorpyrifos 0.013 / 0.039 0.04 N/A ND Pass
Clofentezine 0.003 / 0.009 0.01 N/A ND Pass
Clothianidin 0.008 / 0.025 0.025 N/A ND Pass
Coumaphos 0.003 / 0.010 0.01 N/A ND Pass
Cyantraniliprole 0.003 / 0.010 0.01 N/A ND Pass
Cyfluthrin 0.052 / 0.159 0.1 N/A ND Pass
Cypermethrin 0.051 / 0.153 0.3 N/A ND Pass
Cyprodinil‡ 0.026 / 0.080 0.01 N/A ND Pass
Daminozide 0.026 / 0.077 0.1 N/A ND Pass
Deltamethrin 0.059 / 0.180 0.5 N/A ND Pass
Diazinon 0.006 / 0.017 0.02 N/A ND Pass
Dichlorvos (DDVP) 0.012 / 0.038 0.1 N/A ND Pass
Dimethoate 0.003 / 0.009 0.1 N/A ND Pass
Dimethomorph 0.016 / 0.050 0.05 N/A ND Pass
Dinotefuran 0.010 / 0.030 0.05 N/A ND Pass
Diuron 0.013 / 0.040 0.125 N/A ND Pass
Dodemorph 0.012 / 0.035 0.05 N/A ND Pass
Endosulfan sulfate†‡ 0.016 / 0.048 0.05 N/A ND Pass
Endosulfan-α*†‡ 0.004 / 0.014 0.2 N/A ND Pass
Endosulfan-β*†‡ 0.006 / 0.019 0.05 N/A ND Pass
Ethoprophos 0.003 / 0.009 0.01 N/A ND Pass
Etofenprox 0.014 / 0.042 0.05 N/A ND Pass
Etoxazole 0.007 / 0.020 0.01 N/A ND Pass
Etridiazole* 0.002 / 0.005 0.03 N/A ND Pass
Fenhexamid 0.003 / 0.008 0.125 N/A ND Pass
Fenoxycarb 0.003 / 0.010 0.01 N/A ND Pass
Fenpyroximate 0.007 / 0.020 0.2 N/A ND Pass
Fensulfothion 0.003 / 0.010 0.01 N/A ND Pass
Fenthion 0.003 / 0.010 0.01 N/A ND Pass
Fenvalerate‡ 0.033 / 0.099 0.1 N/A ND Pass
Fipronil 0.003 / 0.010 0.01 N/A ND Pass
Flonicamid 0.007 / 0.022 0.025 N/A ND Pass
Fludioxonil 0.003 / 0.010 0.01 N/A ND Pass
Fluopyram‡ 0.003 / 0.009 0.01 N/A ND Pass
Hexythiazox 0.003 / 0.010 0.01 N/A ND Pass
Imazalil 0.003 / 0.009 0.01 N/A ND Pass
Imidacloprid 0.003 / 0.010 0.01 N/A ND Pass
Iprodione 0.077 / 0.233 0.5 N/A ND Pass
Kinoprene 0.077 / 0.233 0.5 N/A ND Pass
Kresoxim-methyl 0.006 / 0.019 0.02 N/A ND Pass
Malathion 0.003 / 0.009 0.02 N/A ND Pass
Metalaxyl 0.003 / 0.010 0.02 N/A ND Pass
Methiocarb 0.003 / 0.008 0.02 N/A ND Pass
Methomyl 0.008 / 0.025 0.05 N/A ND Pass
Methoprene 0.172 / 0.521 2 N/A ND Pass
Mevinphos 0.008 / 0.024 0.025 N/A ND Pass
MGK-264 0.015 / 0.047 0.05 N/A ND Pass
Myclobutanil 0.003 / 0.009 0.01 N/A ND Pass
Naled 0.021 / 0.064 0.1 N/A ND Pass
Novaluron 0.002 / 0.005 0.025 N/A ND Pass
Oxamyl 0.017 / 0.051 0.5 N/A ND Pass
Paclobutrazol 0.003 / 0.010 0.01 N/A ND Pass
Parathion-methyl 0.016 / 0.050 0.05 N/A ND Pass
Pentachloronitrobenzene (Quintozene)* 0.004 / 0.012 0.02 N/A ND Pass
Permethrin 0.056 / 0.168 0.04 N/A ND Pass
Phenothrin 0.016 / 0.047 0.05 N/A ND Pass
Phosmet 0.007 / 0.020 0.02 N/A ND Pass
Piperonyl Butoxide 0.010 / 0.029 0.2 N/A ND Pass
Pirimicarb 0.015 / 0.046 0.01 N/A ND Pass
Prallethrin 0.003 / 0.009 0.05 N/A ND Pass
Propiconazole 0.027 / 0.080 0.1 N/A ND Pass
Propoxur 0.003 / 0.008 0.01 N/A ND Pass
Pyraclostrobin 0.003 / 0.010 0.01 N/A ND Pass
Pyrethrins 0.016 / 0.049 0.05 N/A ND Pass
Pyridaben 0.005 / 0.017 0.02 N/A ND Pass
Pyriproxyfen 0.003 / 0.009 0.01 N/A ND Pass
Resmethrin 0.013 / 0.039 0.05 N/A ND Pass
Spinetoram 0.004 / 0.014 0.01 N/A ND Pass
Spinosad 0.004 / 0.012 0.01 N/A ND Pass
Spirodiclofen 0.031 / 0.093 0.25 N/A ND Pass
Spiromesifen 0.016 / 0.050 0.03 N/A ND Pass
Spirotetramat 0.003 / 0.010 0.01 N/A ND Pass
Spiroxamine 0.020 / 0.062 0.1 N/A ND Pass
Tebuconazole 0.003 / 0.010 0.01 N/A ND Pass
Tebufenozide 0.003 / 0.008 0.01 N/A ND Pass
Teflubenzuron 0.007 / 0.022 0.025 N/A ND Pass
Tetrachlorvinphos 0.003 / 0.008 0.01 N/A ND Pass
Tetramethrin 0.021 / 0.063 0.1 N/A ND Pass
Thiabendazole 0.006 / 0.020 0.02 N/A ND Pass
Thiacloprid 0.003 / 0.009 0.01 N/A ND Pass
Thiamethoxam 0.003 / 0.010 0.01 N/A ND Pass
Thiophanate-methyl 0.013 / 0.040 0.05 N/A ND Pass
Trifloxystrobin 0.003 / 0.009 0.02 N/A ND Pass

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS

Mycotoxin Test Results

01/19/2022

PASS

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Compound LOD/LOQ
(μg/kg)
Action Limit
(μg/kg)
Measurement
Uncertainty
(μg/kg)
Result
(μg/kg)
Result
Aflatoxin B1 1.6 / 5 5 N/A ND Pass
Aflatoxin B2 1.4 / 4.1 20 N/A ND Pass
Aflatoxin G1 1.6 / 4.9 20 N/A ND Pass
Aflatoxin G2 1.6 / 5 20 N/A ND Pass
Ochratoxin A 1.6 / 5 5 N/A ND Pass
Total Aflatoxin 20 ± ND Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

01/20/2022

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Propane 0.133 / 0.445 500 N/A ND Pass
2-Methylpropane (Isobutane) 0.04 / 0.133 5000 N/A ND Pass
n-Butane 0.042 / 0.141 2000 N/A ND Pass
Total Butanes 500 ± ND Pass
2-Methylbutane (Isopentane) 0.065 / 0.216 5000 N/A ND Pass
2,2-Dimethylpropane (Neopentane) 0.181 / 0.604 N/A ND
n-Pentane 0.181 / 0.604 1000 N/A ND Pass
Total Pentanes 500 ± ND Pass
2,2-Dimethylbutane (Neohexane) 0.147 / 0.488 290 N/A ND Pass
2,3-Dimethylbutane / 2-Methylpentane (Isohexane) 0.375 / 1.249 290 N/A ND Pass
3-Methylpentane 0.075 / 0.251 290 N/A ND Pass
n-Hexane 0.054 / 0.181 0 N/A ND Pass
Total Hexanes 290 ± ND Pass
Cyclohexane 0.091 / 0.302 500 N/A ND Pass
n-Heptane 0.153 / 0.511 500 N/A ND Pass
Benzene 0.066 / 0.221 0 N/A ND Pass
Toluene 0.074 / 0.246 0 N/A ND Pass
Cumene 0.31 / 1.033 70 N/A ND Pass
1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene) 0.213 / 0.71 2170 N/A ND Pass
1,2-Dimethylbenzene (o-Xylene) 0.239 / 0.797 2170 N/A ND Pass
Ethylbenzene 0.176 / 0.586 2170 N/A ND Pass
Total Xylenes 0.320 / 1.067 217 N/A ND Pass
Methanol 0.018 / 0.061 500 N/A ND Pass
Ethanol 0.129 / 0.429 1000 ±11.2358 148.622 Pass
1-Propanol 0.528 / 1.759 5000 N/A ND Pass
2-Propanol (Isopropyl Alcohol) 0.064 / 0.214 500 N/A ND Pass
1-Butanol 0.17 / 0.565 5000 N/A ND Pass
2-Butanol 0.535 / 1.784 5000 N/A ND Pass
1-Pentanol 0.379 / 1.262 N/A ND
Acetone 0.083 / 0.277 5000 ±0.4487 5.553 Pass
2-Butanone 0.193 / 0.642 5000 N/A ND Pass
Tetrahydrofuran 0.22 / 0.735 720 N/A ND Pass
Ethyl Ether 0.1 / 0.335 5000 N/A ND Pass
Ethylene Glycol 31.104 / 103.68 620 N/A ND Pass
2-Ethoxyethanol 1.08 / 3.599 160 N/A ND Pass
1,2-Dimethoxyethane 1.093 / 3.645 100 N/A ND Pass
1,4-Dioxane 0.379 / 1.265 380 N/A ND Pass
Ethylene Oxide 0.05 / 0.166 5 N/A ND Pass
Ethyl Acetate 0.29 / 0.967 1000 ±1.6424 27.603 Pass
Isopropyl Acetate 0.346 / 1.153 5000 N/A ND Pass
Chloroform 0.1 / 0.2 1 N/A ND Pass
Dichloromethane (Methylene Chloride) 0.114 / 0.381 600 N/A ND Pass
Trichloroethylene 0.1 / 0.3 80 N/A ND Pass
1,2-Dichloroethane 0.05 / 0.1 5 N/A ND Pass
Sulfolane 11.728 / 39.094 160 N/A ND Pass
Dimethyl Sulfoxide 1.679 / 5.596 5000 N/A ND Pass
Acetonitrile 0.049 / 0.164 410 N/A ND Pass
Pyridine 0.118 / 0.394 100 N/A ND Pass
N,N-Dimethylacetamide 0.2 / 0.668 1090 N/A ND Pass
N,N-Dimethylformamide 0.335 / 1.116 880 N/A ND Pass

Total Butanes = n-Butane + 2-Methylpropane (Isobutane)

Total Pentanes = n-Pentane + 2-Methylbutane (Isopentane) + 2,2-Dimethylpropane (Neopentane)

Total Hexanes = n-Hexane + 2,2-Dimethylbutane (Neohexane) + 2,3-Dimethylbutane / 2-Methylpentane (Isohexane) + 3-Methylpentane

Total Xylenes = 1,2-Dimethylbenzene (o-Xylene) + 1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene) + Ethylbenzene

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

01/19/2022

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Arsenic 0.02 / 0.1 0.42 N/A ND Pass
Cadmium 0.02 / 0.05 0.27 N/A ND Pass
Lead 0.04 / 0.1 0.5 N/A ND Pass
Mercury 0.002 / 0.01 0.4 N/A ND Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants. And Analysis conducted by 3MTM PetrifilmTM and plate counts of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants and QSP 6794 - Plating with 3MTM PetrifilmTM

Microbiology Test Results (PCR)

01/21/2022

PASS

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Compound Action Limit Result
(cfu/g)
Result
Yersinia spp. Not Detected in 1g ND Pass
Salmonella spp. Not Detected in 1g ND Pass
Candida albicans Not Detected in 1g ND Pass
Aspergillus niger Not Detected in 1g ND Pass
Aspergillus flavus Not Detected in 1g ND Pass
Campylobacter spp. Not Detected in 1g ND Pass
Aspergillus terreus Not Detected in 1g ND Pass
Aspergillus fumigatus Not Detected in 1g ND Pass
Staphylococcus aureus Not Detected in 1g ND Pass
Listeria monocytogenes Not Detected in 1g ND Pass
Pseudomonas aeruginosa Not Detected in 1g ND Pass
Bile-Tolerant Gram-Negative Bacteria 100 ND Pass
Shiga toxin-producing Escherichia coli Not Detected in 1g ND Pass
Microbiology Test Results (PLATING)

01/21/2022

PASS

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Compound Action Limit
(cfu/g)
Result
(cfu/g)
Result
Coliforms 100 ND Pass
Escherichia coli Not Detected in 1g ND Pass
Total Yeast and Mold 10 ND Pass
Total Aerobic Bacteria 100 ND Pass
Total Enterobacteriaceae 1000 ND Pass

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