Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

R&R 5mg Calming Dog Chews - THC-Free - Broad Spectrum

Infused, Hemp Infused

Date Issued:

07/03/2024

Total THC Not Detected
Total CBD 5.727 mg/unit
Sum Cannabinoids 6.004 mg/unit
Total Cannabinoids 5.991 mg/unit
Total Terpenoids 0.0024%
Top 3 Terpenoids
  1. Camphor 0.0024%

Sample Information

Sample Details

Sample ID:240625N001

Batch Number:6100C

Cultivator / Manufacturer

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Distributor / Tested For

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Cannabinoid Analysis - Summary

Total THC: Not Detected

Total CBD: 5.727 mg/unit

Sum of Cannabinoids: 6.004 mg/unit

Total Cannabinoids: 5.991 mg/unit

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

Total Terpenoids: 0.0024%

 

1

Camphor (0.0024%)

Safety Analysis - Summary

Pesticides: Pass

Mycotoxins: Pass

Residual Solvents: Pass

Heavy Metals: Pass

Microbiology (PCR): Pass

Microbiology (Plating): Pass

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: Not Detected

(Δ9-THC+0.877*THCa)

Total CBD: 5.727 mg/unit

(CBD+0.877*CBDa)

Total Cannabinoids: 5.991 mg/unit

Total CBG: 0.068 mg/unit

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: ND

Total CBC (CBC+0.877*CBCa)

Total CBDV: 0.046 mg/unit

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

06/28/2024

Result Views

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Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
Cannabidiol (CBD) 0.004 / 0.011 ±0.0956 2.563 0.2563
Cannabinol (CBN) 0.001 / 0.007 ±0.0020 0.068 0.0068
Cannabidiolic Acid (CBDa) 0.001 / 0.026 ±0.0013 0.046 0.0046
Cannabigerol (CBG) 0.002 / 0.006 ±0.0015 0.031 0.0031
Cannabidivarin (CBDV) 0.002 / 0.012 ±0.0009 0.021 0.0021
Cannabichromene (CBC) 0.003 / 0.010 N/A ND ND
Cannabicyclol (CBL) 0.003 / 0.010 N/A ND ND
Cannabichromenic Acid (CBCa) 0.001 / 0.015 N/A ND ND
Cannabigerolic Acid (CBGa) 0.002 / 0.007 N/A ND ND
Tetrahydrocannabivarin (THCV) 0.002 / 0.012 N/A ND ND
Tetrahydrocannabinolic Acid (THCa) 0.001 / 0.005 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.001 / 0.018 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.002 / 0.019 N/A ND ND
∆8 Tetrahydrocannabinol (Δ8THC) 0.01 / 0.02 N/A ND ND
Δ9 Tetrahydrocannabinol (Δ9THC) 0.002 / 0.014 N/A ND ND
SUM OF CANNABINOIDS 2.729 mg/g 0.2729%
Unit Mass:

2.2 grams

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Δ9-THC per Unit ND
Total THC per Unit ND
CBD per Unit 5.639 mg/unit
Total CBD per Unit 5.727 mg/unit
Sum of Cannabinoids per Unit 6.004 mg/unit
Total Cannabinoids per Unit 5.991 mg/unit
Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

Summary

Total Terpenoids (mg/g): 0.024 mg/g

Total Terpenoids (%): 0.0024%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume.

  1. Camphor 0.0024%

    A monoterpenoid ketone with a pungent fragrance that is as reminiscent of mothballs. It is commonly derived from Cinnamomum camphora, from which it lends its lame. It is a constituent of turpentine and has been used by certain cultures as an embalming fluid due to its antimicrobial effects. Found in camphor laurel, rosemary, East African camphorwood, goldenasters, coriander, feverfew, tarragon, nutmeg, sweet wormwood, yerba buena, mountain mint, hyssop, forskohlii, tansy, thyme, turmeric...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

06/27/2024

Result Views

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Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
Camphor 0.006 / 0.019 ±0.0007 0.024 0.0024
Nerol 0.003 / 0.011 N/A ND ND
Cedrol 0.008 / 0.027 N/A ND ND
Guaiol 0.009 / 0.030 N/A ND ND
Borneol 0.005 / 0.016 N/A ND ND
Fenchol 0.010 / 0.034 N/A ND ND
Menthol 0.008 / 0.025 N/A ND ND
Myrcene 0.008 / 0.025 N/A ND ND
Camphene 0.005 / 0.015 N/A ND ND
Fenchone 0.009 / 0.028 N/A ND ND
Geraniol 0.002 / 0.007 N/A ND ND
Limonene 0.005 / 0.016 N/A ND ND
Linalool 0.009 / 0.032 N/A ND ND
Pulegone 0.003 / 0.011 N/A ND ND
Sabinene 0.004 / 0.014 N/A ND ND
p-Cymene 0.005 / 0.016 N/A ND ND
Nerolidol 0.006 / 0.019 N/A ND ND
Terpineol 0.009 / 0.031 N/A ND ND
Valencene 0.009 / 0.030 N/A ND ND
Eucalyptol 0.006 / 0.018 N/A ND ND
Isoborneol 0.004 / 0.012 N/A ND ND
Isopulegol 0.005 / 0.016 N/A ND ND
Citronellol 0.003 / 0.010 N/A ND ND
Terpinolene 0.008 / 0.026 N/A ND ND
β-Pinene 0.004 / 0.014 N/A ND ND
α-Pinene 0.005 / 0.017 N/A ND ND
β-Ocimene 0.006 / 0.020 N/A ND ND
Δ3-Carene 0.005 / 0.018 N/A ND ND
α-Cedrene 0.005 / 0.016 N/A ND ND
α-Humulene 0.009 / 0.029 N/A ND ND
Geranyl Acetate 0.004 / 0.014 N/A ND ND
α-Bisabolol 0.008 / 0.026 N/A ND ND
α-Terpinene 0.005 / 0.017 N/A ND ND
γ-Terpinene 0.006 / 0.018 N/A ND ND
Sabinene Hydrate 0.006 / 0.022 N/A ND ND
α-Phellandrene 0.006 / 0.020 N/A ND ND
β-Caryophyllene 0.004 / 0.012 N/A ND ND
Caryophyllene Oxide 0.010 / 0.033 N/A ND ND
trans-β-Farnesene 0.008 / 0.025 N/A ND ND
TOTAL 0.024 mg/g 0.0024%
Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

07/02/2024

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Abamectin 0.032 / 0.097 0.07 N/A ND Pass
Acephate 0.006 / 0.018 0.05 N/A ND Pass
Acequinocyl 0.009 / 0.027 0.03 N/A ND Pass
Acetamiprid 0.016 / 0.049 0.05 N/A ND Pass
Aldicarb 0.030 / 0.090 0.1 N/A ND Pass
Allethrin 0.030 / 0.092 0.1 N/A ND Pass
Atrazine 0.006 / 0.019 0.025 N/A ND Pass
Azadirachtin 0.082 / 0.248 0.5 N/A ND Pass
Azoxystrobin 0.003 / 0.009 0.01 N/A ND Pass
Benzovindiflupyr 0.003 / 0.009 0.01 N/A ND Pass
Bifenazate 0.003 / 0.009 0.01 N/A ND Pass
Bifenthrin 0.021 / 0.064 0.2 N/A ND Pass
Boscalid 0.003 / 0.009 0.01 N/A ND Pass
Buprofezin‡ 0.006 / 0.019 0.02 N/A ND Pass
Carbaryl 0.007 / 0.020 0.025 N/A ND Pass
Carbofuran 0.003 / 0.008 0.01 N/A ND Pass
Chlorantraniliprole 0.006 / 0.018 0.02 N/A ND Pass
Chlorfenapyr* 0.005 / 0.015 0.1 N/A ND Pass
Chlorpyrifos 0.013 / 0.039 0.04 N/A ND Pass
cis-Permethrin ± 0.00
Clofentezine 0.003 / 0.009 0.01 N/A ND Pass
Clothianidin 0.008 / 0.025 0.025 N/A ND Pass
Coumaphos 0.003 / 0.010 0.01 N/A ND Pass
Cyantraniliprole 0.003 / 0.010 0.01 N/A ND Pass
Cyfluthrin 0.052 / 0.159 0.1 N/A ND Pass
Cypermethrin 0.051 / 0.153 0.3 N/A ND Pass
Cyprodinil‡ 0.003 / 0.008 0.01 N/A ND Pass
Daminozide 0.026 / 0.077 0.1 N/A ND Pass
Deltamethrin 0.059 / 0.180 0.5 N/A ND Pass
Diazinon 0.006 / 0.017 0.02 N/A ND Pass
Dichlorvos (DDVP) 0.012 / 0.038 0.1 N/A ND Pass
Dimethoate 0.003 / 0.009 0.1 N/A ND Pass
Dimethomorph 0.016 / 0.050 0.05 N/A ND Pass
Dinotefuran 0.010 / 0.030 0.05 N/A ND Pass
Diuron 0.013 / 0.040 0.125 N/A ND Pass
Dodemorph 0.012 / 0.035 0.05 N/A ND Pass
Endosulfan sulfate†‡ 0.016 / 0.048 0.05 N/A ND Pass
Endosulfan-α*†‡ 0.004 / 0.014 0.2 N/A ND Pass
Endosulfan-β*†‡ 0.006 / 0.019 0.05 N/A ND Pass
Ethoprophos 0.003 / 0.009 0.01 N/A ND Pass
Etofenprox 0.014 / 0.042 0.05 N/A ND Pass
Etoxazole 0.007 / 0.020 0.01 N/A ND Pass
Etridiazole* 0.002 / 0.005 0.03 N/A ND Pass
Fenhexamid 0.003 / 0.008 0.125 N/A ND Pass
Fenoxycarb 0.003 / 0.010 0.01 N/A ND Pass
Fenpyroximate 0.007 / 0.020 0.2 N/A ND Pass
Fensulfothion 0.003 / 0.010 0.01 N/A ND Pass
Fenthion 0.003 / 0.010 0.01 N/A ND Pass
Fenvalerate‡ 0.033 / 0.099 0.1 N/A ND Pass
Fipronil 0.003 / 0.010 0.01 N/A ND Pass
Flonicamid 0.007 / 0.022 0.025 N/A ND Pass
Fludioxonil 0.003 / 0.010 0.01 N/A ND Pass
Fluopyram‡ 0.003 / 0.009 0.01 N/A ND Pass
Hexythiazox 0.003 / 0.010 0.01 N/A ND Pass
Imazalil 0.003 / 0.009 0.01 N/A ND Pass
Imidacloprid 0.003 / 0.010 0.01 N/A ND Pass
Iprodione 0.077 / 0.233 0.5 N/A ND Pass
Kinoprene 0.077 / 0.233 0.5 N/A ND Pass
Kresoxim-methyl 0.006 / 0.019 0.02 N/A ND Pass
λ-Cyhalothrin 0.068 / 0.206 0.25 N/A ND Pass
Malathion 0.003 / 0.009 0.02 N/A ND Pass
Metalaxyl 0.003 / 0.010 0.02 N/A ND Pass
Methiocarb 0.003 / 0.008 0.02 N/A ND Pass
Methomyl 0.008 / 0.025 0.05 N/A ND Pass
Methoprene 0.172 / 0.521 2 N/A ND Pass
Mevinphos 0.008 / 0.024 0.025 N/A ND Pass
MGK-264 0.015 / 0.047 0.05 N/A ND Pass
Myclobutanil 0.003 / 0.009 0.01 N/A ND Pass
Naled 0.021 / 0.064 0.1 N/A ND Pass
Novaluron 0.002 / 0.005 0.025 N/A ND Pass
Oxamyl 0.017 / 0.051 0.5 N/A ND Pass
Paclobutrazol 0.003 / 0.010 0.01 N/A ND Pass
Parathion-methyl 0.016 / 0.050 0.05 N/A ND Pass
Pentachloronitrobenzene (Quintozene)* 0.004 / 0.012 0.02 N/A ND Pass
Permethrin 0.056 / 0.168 0.04 N/A ND Pass
Phenothrin 0.016 / 0.047 0.05 N/A ND Pass
Phosmet 0.007 / 0.020 0.02 N/A ND Pass
Piperonyl Butoxide 0.010 / 0.029 0.2 N/A ND Pass
Pirimicarb 0.003 / 0.009 0.01 N/A ND Pass
Prallethrin 0.015 / 0.046 0.05 N/A ND Pass
Propiconazole 0.027 / 0.080 0.1 N/A ND Pass
Propoxur 0.003 / 0.008 0.01 N/A ND Pass
Pyraclostrobin 0.003 / 0.010 0.01 N/A ND Pass
Pyrethrins 0.016 / 0.049 0.05 N/A ND Pass
Pyridaben 0.005 / 0.017 0.02 N/A ND Pass
Pyriproxyfen 0.003 / 0.009 0.01 N/A ND Pass
Resmethrin 0.013 / 0.039 0.05 N/A ND Pass
Spinetoram 0.003 / 0.010 0.01 N/A ND Pass
Spinosad 0.003 / 0.010 0.01 N/A ND Pass
Spirodiclofen 0.031 / 0.093 0.25 N/A ND Pass
Spiromesifen 0.016 / 0.050 0.03 N/A ND Pass
Spirotetramat 0.003 / 0.010 0.01 N/A ND Pass
Spiroxamine 0.020 / 0.062 0.1 N/A ND Pass
Tebuconazole 0.003 / 0.010 0.01 N/A ND Pass
Tebufenozide 0.003 / 0.008 0.01 N/A ND Pass
Teflubenzuron 0.007 / 0.022 0.025 N/A ND Pass
Tetrachlorvinphos 0.003 / 0.008 0.01 N/A ND Pass
Tetramethrin 0.021 / 0.063 0.1 N/A ND Pass
Thiabendazole 0.006 / 0.020 0.02 N/A ND Pass
Thiacloprid 0.003 / 0.009 0.01 N/A ND Pass
Thiamethoxam 0.003 / 0.010 0.01 N/A ND Pass
Thiophanate-methyl 0.013 / 0.040 0.05 N/A ND Pass
trans-Permethrin ± 0.00
Trifloxystrobin 0.003 / 0.009 0.02 N/A ND Pass

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS

Mycotoxin Test Results

07/02/2024

PASS

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Compound LOD/LOQ
(μg/kg)
Action Limit
(μg/kg)
Measurement
Uncertainty
(μg/kg)
Result
(μg/kg)
Result
Aflatoxin B1 1.6 / 5.0 5 N/A ND Pass
Aflatoxin B2 1.4 / 4.1 20 N/A ND Pass
Aflatoxin G1 1.6 / 4.9 20 N/A ND Pass
Aflatoxin G2 1.6 / 5.0 20 N/A ND Pass
Ochratoxin A 1.6 / 5.0 5 N/A ND Pass
Total Aflatoxin 20 ± ND Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

06/28/2024

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Propane 0.234 / 0.781 500 N/A ND Pass
2-Methylpropane (Isobutane) 0.052 / 0.173 5000 N/A ND Pass
n-Butane 0.019 / 0.063 2000 N/A ND Pass
Total Butanes 500 ± ND Pass
n-Pentane 0.310 / 1.033 1000 N/A ND Pass
n-Hexane 0.110 / 0.366 0 N/A ND Pass
2,2-Dimethylpentane (Neoheptane) 0.493 / 1.642 N/A ND
2,3-Dimethylpentane 1.009 / 3.365 N/A ND
2,4-Dimethylpentane 0.737 / 2.458 N/A ND
3,3-Dimethylpentane 0.198 / 0.660 N/A ND
2,2,3-Trimethylbutane (Triptane) 0.521 / 1.738 N/A ND
2-Methylhexane (Isoheptane) 0.610 / 2.034 N/A ND
3-Methylhexane 0.235 / 0.785 N/A ND
3-Ethylpentane 0.304 / 1.012 N/A ND
n-Heptane 13.12 / 43.72 500 N/A ND Pass
Total Heptanes 1000 ± ND Pass
Benzene 0.089 / 0.295 0 N/A ND Pass
Toluene 0.115 / 0.382 0 N/A ND Pass
1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene) 0.451 / 1.502 2170 N/A ND Pass
1,2-Dimethylbenzene (o-Xylene) 0.387 / 1.289 2170 N/A ND Pass
Total Xylenes 217 ± ND Pass
Methanol 53.92 / 163.4 500 N/A ND Pass
Ethanol 8.984 / 27.23 1000 N/A ND Pass
2-Propanol (Isopropyl Alcohol) 8.421 / 25.52 500 N/A <LOQ Pass
Acetone 10.59 / 32.08 5000 N/A <LOQ Pass
Ethyl Acetate 1.123 / 3.745 1000 N/A ND Pass

Total Butanes = n-Butane + 2-Methylpropane (Isobutane)

Total Heptanes = 2,2-Dimethylpentane (Neoheptane) + 2,3-Dimethylpentane + 2,4-Dimethylpentane + 3,3-Dimethylpentane + 2,2,3-Trimethylbutane (Triptane) + 2-Methylhexane (Isoheptane) + 3-Methylhexane + 3-Ethylpentane + n-Heptane

Total Xylenes = 1,2-Dimethylbenzene (o-Xylene) + 1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene)

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

06/27/2024

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Arsenic 0.02 / 0.1 0.42 N/A ND Pass
Cadmium 0.02 / 0.05 0.27 N/A ND Pass
Lead 0.04 / 0.1 0.5 N/A ND Pass
Mercury 0.002 / 0.01 0.4 N/A ND Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants. And Analysis conducted by 3MTM PetrifilmTM and plate counts of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants and QSP 6794 - Plating with 3MTM PetrifilmTM

Microbiology Test Results (PCR)

06/29/2024

PASS

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Compound Action Limit Result Result
Salmonella spp. Not Detected in 25g ND Pass
Shiga toxin-producing Escherichia coli Not Detected in 25g ND Pass
Microbiology Test Results (PLATING)

06/29/2024

PASS

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Compound Action Limit
(cfu/g)
Result
(cfu/g)
Result
Coliforms 100 ND Pass
Total Yeast and Mold 10 ND Pass
Total Aerobic Bacteria 100 ND Pass

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