Certificate of Analysis
REGULATORY COMPLIANCE

Sample Name:

Dark Chocolate Sativa

Infused, Solid Edible

Date Issued:

12/02/2022

Overall Batch Result:

Pass

Serving Size:

5 grams

Sum Cannabinoids 112.400 mg/unit
Total Cannabinoids 112.400 mg/unit
Total THC 105.750 mg/unit
Total CBD 1.400 mg/unit

Sample Information

Sample Details

Sample ID:221129K010

Batch Number:22315-1

Cultivator / Manufacturer

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Distributor

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Sampling Method: QSP 1265 - Sampling of Cannabis and Product Batches

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Cannabinoid Analysis - Summary

Sum of Cannabinoids: 112.400 mg/unit

Total Cannabinoids: 112.400 mg/unit

Total THC: 105.750 mg/unit

Total CBD: 1.400 mg/unit

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa+Δ8-THC) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + CBL + CBN

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877)) + Δ8-THC
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Safety Analysis - Summary

Δ9-THC per Unit: Pass

Δ9-THC per Serving: Pass

Pesticides: Pass

Mycotoxins: Pass

Residual Solvents: Pass

Heavy Metals: Pass

Microbiology: Pass

Foreign Material: Pass

Water Activity: Pass

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total Cannabinoids: 112.400 mg/unit

Total THC: 105.750 mg/unit

9-THC+0.877*THCa+Δ8-THC)

Total CBD: 1.400 mg/unit

(CBD+0.877*CBDa)

Total CBG: 3.600 mg/unit

Total CBG (CBG+0.877*CBGa)

Total THCV: <LOQ

Total THCV (THCV+0.877*THCVa)

Total CBC: ND

Total CBC (CBC+0.877*CBCa)

Total CBDV: ND

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

12/01/2022

Result Views

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Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
Δ9 Tetrahydrocannabinol (Δ9THC) 0.002 / 0.014 ±0.1161 2.115 0.2115
Cannabigerol (CBG) 0.002 / 0.006 ±0.0035 0.072 0.0072
Cannabinol (CBN) 0.001 / 0.007 ±0.0009 0.033 0.0033
Cannabidiol (CBD) 0.004 / 0.011 ±0.0010 0.028 0.0028
Tetrahydrocannabivarin (THCV) 0.002 / 0.012 N/A <LOQ <LOQ
∆8 Tetrahydrocannabinol (Δ8THC) 0.01 / 0.02 N/A ND ND
Tetrahydrocannabinolic Acid (THCa) 0.001 / 0.005 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.002 / 0.019 N/A ND ND
Cannabidiolic Acid (CBDa) 0.001 / 0.026 N/A ND ND
Cannabidivarin (CBDV) 0.002 / 0.012 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.001 / 0.018 N/A ND ND
Cannabigerolic Acid (CBGa) 0.002 / 0.007 N/A ND ND
Cannabicyclol (CBL) 0.003 / 0.010 N/A ND ND
Cannabichromene (CBC) 0.003 / 0.010 N/A ND ND
Cannabichromenic Acid (CBCa) 0.001 / 0.015 N/A ND ND
SUM OF CANNABINOIDS 2.248 mg/g 0.2248%
Unit Mass:

50 grams

/

Serving Size:

5 grams

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Δ9-THC per Unit 110 per-package limit 105.750 mg/unit Pass
Δ9-THC per Serving 11 per-serving limit 10.575 mg/serving Pass
Total THC per Unit 105.750 mg/unit
Total THC Per Serving 10.575 mg/serving
CBD per Unit 1.400 mg/unit
CBD per Serving 0.140 mg/serving
Total CBD per Unit 1.400 mg/unit
Total CBD per Serving 0.140 mg/serving
Sum of Cannabinoids per Unit 112.400 mg/unit
Sum of Cannabinoids per Serving 11.240 mg/serving
Total Cannabinoids per Unit 112.400 mg/unit
Total Cannabinoids per Serving 11.240 mg/serving
Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Category 1 Pesticide Test Results

12/01/2022

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Aldicarb 0.03 / 0.08 ≥ LOD N/A ND Pass
Carbofuran 0.02 / 0.05 ≥ LOD N/A ND Pass
Chlordane* 0.03 / 0.08 ≥ LOD N/A ND Pass
Chlorfenapyr* 0.03 / 0.10 ≥ LOD N/A ND Pass
Chlorpyrifos 0.02 / 0.06 ≥ LOD N/A ND Pass
Coumaphos 0.02 / 0.07 ≥ LOD N/A ND Pass
Daminozide 0.02 / 0.07 ≥ LOD N/A ND Pass
Dichlorvos (DDVP) 0.03 / 0.09 ≥ LOD N/A ND Pass
Dimethoate 0.03 / 0.08 ≥ LOD N/A ND Pass
Ethoprophos 0.03 / 0.10 ≥ LOD N/A ND Pass
Etofenprox 0.02 / 0.06 ≥ LOD N/A ND Pass
Fenoxycarb 0.03 / 0.08 ≥ LOD N/A ND Pass
Fipronil 0.03 / 0.08 ≥ LOD N/A ND Pass
Imazalil 0.02 / 0.06 ≥ LOD N/A ND Pass
Methiocarb 0.02 / 0.07 ≥ LOD N/A ND Pass
Parathion-methyl 0.03 / 0.10 ≥ LOD N/A ND Pass
Mevinphos 0.03 / 0.09 ≥ LOD N/A ND Pass
Paclobutrazol 0.02 / 0.05 ≥ LOD N/A ND Pass
Propoxur 0.03 / 0.09 ≥ LOD N/A ND Pass
Spiroxamine 0.03 / 0.08 ≥ LOD N/A ND Pass
Thiacloprid 0.03 / 0.10 ≥ LOD N/A ND Pass
Category 2 Pesticide Test Results

12/01/2022

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Abamectin 0.03 / 0.10 0.3 N/A ND Pass
Acephate 0.02 / 0.07 5 N/A ND Pass
Acequinocyl 0.02 / 0.07 4 N/A ND Pass
Acetamiprid 0.02 / 0.05 5 N/A ND Pass
Azoxystrobin 0.02 / 0.07 40 N/A ND Pass
Bifenazate 0.01 / 0.04 5 N/A ND Pass
Bifenthrin 0.02 / 0.05 0.5 N/A ND Pass
Boscalid 0.03 / 0.09 10 N/A ND Pass
Captan 0.19 / 0.57 5 N/A ND Pass
Carbaryl 0.02 / 0.06 0.5 N/A ND Pass
Chlorantraniliprole 0.04 / 0.12 40 N/A ND Pass
Clofentezine 0.03 / 0.09 0.5 N/A ND Pass
Cyfluthrin 0.12 / 0.38 1 N/A ND Pass
Cypermethrin 0.11 / 0.32 1 N/A ND Pass
Diazinon 0.02 / 0.05 0.2 N/A ND Pass
Dimethomorph 0.03 / 0.09 20 N/A ND Pass
Etoxazole 0.02 / 0.06 1.5 N/A ND Pass
Fenhexamid 0.03 / 0.09 10 N/A ND Pass
Fenpyroximate 0.02 / 0.06 2 N/A ND Pass
Flonicamid 0.03 / 0.10 2 N/A ND Pass
Fludioxonil 0.03 / 0.10 30 N/A ND Pass
Hexythiazox 0.02 / 0.07 2 N/A ND Pass
Imidacloprid 0.04 / 0.11 3 N/A ND Pass
Kresoxim-methyl 0.02 / 0.07 1 N/A ND Pass
Malathion 0.03 / 0.09 5 N/A ND Pass
Metalaxyl 0.02 / 0.07 15 N/A ND Pass
Methomyl 0.03 / 0.10 0.1 N/A ND Pass
Myclobutanil 0.03 / 0.09 9 N/A ND Pass
Naled 0.02 / 0.07 0.5 N/A ND Pass
Oxamyl 0.04 / 0.11 0.2 N/A ND Pass
Pentachloronitrobenzene* 0.03 / 0.09 0.2 N/A ND Pass
Permethrin 0.04 / 0.12 20 N/A ND Pass
Phosmet 0.03 / 0.10 0.2 N/A ND Pass
Piperonyl Butoxide 0.02 / 0.07 8 N/A ND Pass
Prallethrin 0.03 / 0.08 0.4 N/A ND Pass
Propiconazole 0.02 / 0.07 20 N/A ND Pass
Pyrethrins 0.04 / 0.12 1 N/A ND Pass
Pyridaben 0.02 / 0.07 3 N/A ND Pass
Spinetoram 0.02 / 0.07 3 N/A ND Pass
Spinosad 0.02 / 0.07 3 N/A ND Pass
Spiromesifen 0.02 / 0.05 12 N/A ND Pass
Spirotetramat 0.02 / 0.06 13 N/A ND Pass
Tebuconazole 0.02 / 0.07 2 N/A ND Pass
Thiamethoxam 0.03 / 0.10 4.5 N/A ND Pass
Trifloxystrobin 0.03 / 0.08 30 N/A ND Pass

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS

Mycotoxin Test Results

12/01/2022

PASS

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Compound LOD/LOQ
(μg/kg)
Action Limit
(μg/kg)
Measurement
Uncertainty
(μg/kg)
Result
(μg/kg)
Result
Aflatoxin B1 2.0 / 6.0 N/A ND
Aflatoxin B2 1.8 / 5.6 N/A ND
Aflatoxin G1 1.0 / 3.1 N/A ND
Aflatoxin G2 1.2 / 3.5 N/A ND
Total Aflatoxin 20 ± ND Pass
Ochratoxin A 6.3 / 19.2 20 N/A ND Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Category 1 Residual Solvents Test Results

12/01/2022

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
1,2-Dichloroethane 0.05 / 0.1 1 N/A ND Pass
Benzene 0.03 / 0.09 1 N/A ND Pass
Chloroform 0.1 / 0.2 1 N/A ND Pass
Ethylene Oxide 0.3 / 0.8 1 N/A ND Pass
Dichloromethane (Methylene Chloride) 0.3 / 0.9 1 N/A ND Pass
Trichloroethylene 0.1 / 0.3 1 N/A ND Pass
Category 2 Residual Solvents Test Results

12/01/2022

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Acetone 20 / 50 5000 N/A ND Pass
Acetonitrile 2 / 7 410 N/A ND Pass
n-Butane 10 / 50 5000 N/A ND Pass
Ethanol 20 / 50 5000 N/A ND Pass
Ethyl Acetate 20 / 60 5000 N/A ND Pass
Ethyl Ether 20 / 50 5000 N/A ND Pass
n-Heptane 20 / 60 5000 N/A ND Pass
n-Hexane 2 / 5 290 N/A ND Pass
2-Propanol (Isopropyl Alcohol) 10 / 40 5000 N/A ND Pass
Methanol 50 / 200 3000 N/A ND Pass
n-Pentane 20 / 50 5000 N/A ND Pass
Propane 10 / 20 5000 N/A ND Pass
Toluene 7 / 21 890 N/A ND Pass
Total Xylenes 50 / 160 2170 N/A ND Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

12/01/2022

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Arsenic 0.02 / 0.1 1.5 N/A ND Pass
Cadmium 0.02 / 0.05 0.5 ±0.002 0.08 Pass
Lead 0.04 / 0.1 0.5 N/A ND Pass
Mercury 0.002 / 0.01 3 N/A <LOQ Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants

Microbiology Test Results

12/02/2022

PASS

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Compound Action Limit Result Result
Salmonella spp. Not Detected in 1g ND Pass
Shiga toxin-producing Escherichia coli Not Detected in 1g ND Pass

Visual analysis includes, but is not limited to, sand, soil, cinders, dirt, mold, hair, insect fragments, and mammalian excreta.

Method: QSP 1226 - Analysis of Foreign Material in Cannabis and Cannabis Products

Foreign Material Test Results

12/01/2022

PASS

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Compound Action Limit Result Result
Total Sample Area Covered by Sand, Soil, Cinders, or Dirt >25% None Pass
Total Sample Area Covered by Mold >25% None Pass
Total Sample Area Covered by an Imbedded Foreign Material >25% None Pass
Insect Fragment Count > 1 per 3 grams 0.0 Pass
Hair Count > 1 per 3 grams 0.0 Pass
Mammalian Excreta Count > 1 per 3 grams 0.0 Pass

Method: QSP 1227 - Analysis of Water Activity in Cannabis and Cannabis Products

Water Activity Test Results

11/30/2022

PASS

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Compound LOD/LOQ
(Aw)
Action Limit
(Aw)
Measurement
Uncertainty
(Aw)
Result
(Aw)
Result
Water Activity 0.030 / 0.030 0.85 ±0.0111 0.227 Pass

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