Relief 1000mg

Certificate of Analysis

HEMP QUALITY ASSURANCE TEST

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Sample Name:

Relief 1000mg

Infused, Hemp Infused

Total THC 0.285 mg/unit

Total CBD 423.615 mg/unit

Sum Cannabinoids 428.460 mg/unit

Total Cannabinoids 428.460 mg/unit

Sample Information

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Sample Details

Sample ID:211119Q002

Batch Number:310821

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Cannabinoid Analysis - Summary

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Total THC: 0.285 mg/unit

Total CBD: 423.615 mg/unit

Sum of Cannabinoids: 428.460 mg/unit

Total Cannabinoids: 428.460 mg/unit

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ⁹-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ⁹-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ⁸-THC + CBL + CBN

Total Cannabinoids = (Δ⁹-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ⁸-THC + CBL + CBN

Why are Sum of Cannabinoids and Total Cannabinoids calculated separately?

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Safety Analysis - Summary

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Pesticides: Pass

Mycotoxins: Pass

Residual Solvents: Pass

Heavy Metals: Pass

Microbiology (PCR): Pass

Microbiology (Plating): Pass

View Complete Test Results:

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Cannabinoid Analysis

Tested

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 0.285 mg/unit

(Δ⁹-THC+0.877*THCa)

Total CBD: 423.615 mg/unit

(CBD+0.877*CBDa)

Total Cannabinoids: 428.460 mg/unit

Total CBG: ND

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 0.495 mg/unit

Total CBC (CBC+0.877*CBCa)

Total CBDV: 3.090 mg/unit

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

11/21/2021

Result Views

Table Pie Chart

Swipe left on table to see additional columns

Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
Cannabidiol (CBD)	0.004 / 0.011	±1.3527	28.241	2.8241
Cannabidivarin (CBDV)	0.002 / 0.012	±0.0108	0.206	0.0206
Cannabicyclol (CBL)	0.003 / 0.010	±0.0031	0.065	0.0065
Cannabichromene (CBC)	0.003 / 0.010	±0.0014	0.033	0.0033
Δ9 Tetrahydrocannabinol (Δ9THC)	0.002 / 0.014	±0.0013	0.019	0.0019
∆8 Tetrahydrocannabinol (Δ8THC)	0.01 / 0.02	N/A	ND	ND
Tetrahydrocannabinolic Acid (THCa)	0.001 / 0.005	N/A	ND	ND
Tetrahydrocannabivarin (THCV)	0.002 / 0.012	N/A	ND	ND
Tetrahydrocannabivarinic Acid (THCVa)	0.002 / 0.019	N/A	ND	ND
Cannabidiolic Acid (CBDa)	0.001 / 0.026	N/A	ND	ND
Cannabidivarinic Acid (CBDVa)	0.001 / 0.018	N/A	ND	ND
Cannabigerol (CBG)	0.002 / 0.006	N/A	ND	ND
Cannabigerolic Acid (CBGa)	0.002 / 0.007	N/A	ND	ND
Cannabinol (CBN)	0.001 / 0.007	N/A	ND	ND
Cannabichromenic Acid (CBCa)	0.001 / 0.015	N/A	ND	ND
SUM OF CANNABINOIDS			28.564 mg/g	2.8564%

Unit Mass:

15 grams

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Δ⁹-THC per Unit		0.285 mg/unit
Total THC per Unit		0.285 mg/unit
CBD per Unit		423.615 mg/unit
Total CBD per Unit		423.615 mg/unit
Sum of Cannabinoids per Unit		428.460 mg/unit
Total Cannabinoids per Unit		428.460 mg/unit

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Pesticide Analysis

Pass

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

11/22/2021

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
Abamectin	0.032 / 0.097	0.07	N/A	ND	Pass
Acephate	0.006 / 0.018	0.05	N/A	ND	Pass
Acequinocyl	0.009 / 0.027	0.03	N/A	ND	Pass
Acetamiprid	0.016 / 0.049	0.05	N/A	ND	Pass
Aldicarb	0.030 / 0.090	0.1	N/A	ND	Pass
Allethrin	0.030 / 0.092	0.1	N/A	ND	Pass
Atrazine	0.006 / 0.019	0.025	N/A	ND	Pass
Azadirachtin	0.082 / 0.248	0.5	N/A	ND	Pass
Azoxystrobin	0.003 / 0.009	0.01	N/A	ND	Pass
Benzovindiflupyr	0.003 / 0.009	0.01	N/A	ND	Pass
Bifenazate	0.003 / 0.009	0.01	N/A	ND	Pass
Bifenthrin	0.021 / 0.064	0.2	N/A	ND	Pass
Boscalid	0.003 / 0.009	0.01	N/A	ND	Pass
Buprofezin	0.006 / 0.019	0.02	N/A	ND	Pass
Captan	0.045 / 0.135	3	N/A	ND	Pass
Carbaryl	0.007 / 0.020	0.025	N/A	ND	Pass
Carbofuran	0.003 / 0.008	0.01	N/A	ND	Pass
Chlorantraniliprole	0.006 / 0.018	0.02	N/A	ND	Pass
Chlordane*	0.005 / 0.107	0.1	N/A	ND	Pass
Chlorfenapyr*	0.005 / 0.015	0.1	N/A	ND	Pass
Chlormequat chloride	0.022 / 0.066	3	N/A	ND	Pass
Chlorpyrifos	0.013 / 0.039	0.04	N/A	ND	Pass
Clofentezine	0.003 / 0.009	0.01	N/A	ND	Pass
Clothianidin	0.008 / 0.025	0.025	N/A	ND	Pass
Coumaphos	0.003 / 0.010	0.01	N/A	ND	Pass
Cyantraniliprole	0.003 / 0.010	0.01	N/A	ND	Pass
Cyfluthrin	0.052 / 0.159	0.1	N/A	ND	Pass
Cypermethrin	0.051 / 0.153	0.3	N/A	ND	Pass
Cyprodinil	0.026 / 0.080	0.01	N/A	ND	Pass
Daminozide	0.026 / 0.077	0.1	N/A	ND	Pass
Deltamethrin	0.059 / 0.180	0.5	N/A	ND	Pass
Diazinon	0.006 / 0.017	0.02	N/A	ND	Pass
Dichlorvos (DDVP)	0.012 / 0.038	0.1	N/A	ND	Pass
Dimethoate	0.003 / 0.009	0.1	N/A	ND	Pass
Dimethomorph	0.016 / 0.050	0.05	N/A	ND	Pass
Dinotefuran	0.010 / 0.030	0.05	N/A	ND	Pass
Diuron	0.013 / 0.040	0.125	N/A	ND	Pass
Dodemorph	0.012 / 0.035	0.05	N/A	ND	Pass
Endosulfan sulfate	0.016 / 0.048	0.05	N/A	ND	Pass
Endosulfan-α*	0.004 / 0.014	0.2	N/A	ND	Pass
Endosulfan-β*	0.006 / 0.019	0.05	N/A	ND	Pass
Ethoprophos	0.003 / 0.009	0.01	N/A	ND	Pass
Etofenprox	0.014 / 0.042	0.05	N/A	ND	Pass
Etoxazole	0.007 / 0.020	0.01	N/A	ND	Pass
Etridiazole*	0.002 / 0.005	0.03	N/A	ND	Pass
Fenhexamid	0.003 / 0.008	0.125	N/A	ND	Pass
Fenoxycarb	0.003 / 0.010	0.01	N/A	ND	Pass
Fenpyroximate	0.007 / 0.020	0.2	N/A	ND	Pass
Fensulfothion	0.003 / 0.010	0.01	N/A	ND	Pass
Fenthion	0.003 / 0.010	0.01	N/A	ND	Pass
Fenvalerate	0.033 / 0.099	0.1	N/A	ND	Pass
Fipronil	0.003 / 0.010	0.01	N/A	ND	Pass
Flonicamid	0.007 / 0.022	0.025	N/A	ND	Pass
Fludioxonil	0.003 / 0.010	0.01	N/A	ND	Pass
Fluopyram	0.003 / 0.009	0.01	N/A	ND	Pass
Hexythiazox	0.003 / 0.010	0.01	N/A	ND	Pass
Imazalil	0.003 / 0.009	0.01	N/A	ND	Pass
Imidacloprid	0.003 / 0.010	0.01	N/A	ND	Pass
Iprodione	0.077 / 0.233	0.5	N/A	ND	Pass
Kinoprene	0.077 / 0.233	0.5	N/A	ND	Pass
Kresoxim-methyl	0.006 / 0.019	0.02	N/A	ND	Pass
Malathion	0.003 / 0.009	0.02	N/A	ND	Pass
Metalaxyl	0.003 / 0.010	0.02	N/A	ND	Pass
Methiocarb	0.003 / 0.008	0.02	N/A	ND	Pass
Methomyl	0.008 / 0.025	0.05	N/A	ND	Pass
Methoprene	0.172 / 0.521	2	N/A	ND	Pass
Mevinphos	0.008 / 0.024	0.025	N/A	ND	Pass
MGK-264	0.015 / 0.047	0.05	N/A	ND	Pass
Myclobutanil	0.003 / 0.009	0.01	N/A	ND	Pass
Naled	0.021 / 0.064	0.1	N/A	ND	Pass
Novaluron	0.002 / 0.005	0.025	N/A	ND	Pass
Oxamyl	0.017 / 0.051	0.5	N/A	ND	Pass
Paclobutrazol	0.003 / 0.010	0.01	N/A	ND	Pass
Parathion-methyl	0.016 / 0.050	0.05	N/A	ND	Pass
Pentachloronitrobenzene*	0.004 / 0.012	0.02	N/A	ND	Pass
Permethrin	0.056 / 0.168	0.04	N/A	ND	Pass
Phenothrin	0.016 / 0.047	0.05	N/A	ND	Pass
Phosmet	0.007 / 0.020	0.02	N/A	ND	Pass
Piperonyl Butoxide	0.010 / 0.029	0.2	N/A	ND	Pass
Pirimicarb	0.015 / 0.046	0.01	N/A	ND	Pass
Prallethrin	0.003 / 0.009	0.05	N/A	ND	Pass
Propiconazole	0.027 / 0.080	0.1	N/A	ND	Pass
Propoxur	0.003 / 0.008	0.01	N/A	ND	Pass
Pyraclostrobin	0.003 / 0.010	0.01	N/A	ND	Pass
Pyrethrins	0.016 / 0.049	0.05	N/A	ND	Pass
Pyridaben	0.005 / 0.017	0.02	N/A	ND	Pass
Pyriproxyfen	0.003 / 0.009	0.01	N/A	ND	Pass
Resmethrin	0.013 / 0.039	0.05	N/A	ND	Pass
Spinetoram	0.004 / 0.014	0.01	N/A	ND	Pass
Spinosad	0.004 / 0.012	0.01	N/A	ND	Pass
Spirodiclofen	0.031 / 0.093	0.25	N/A	ND	Pass
Spiromesifen	0.016 / 0.050	0.03	N/A	ND	Pass
Spirotetramat	0.003 / 0.010	0.01	N/A	ND	Pass
Spiroxamine	0.020 / 0.062	0.1	N/A	ND	Pass
Tebuconazole	0.003 / 0.010	0.01	N/A	ND	Pass
Tebufenozide	0.003 / 0.008	0.01	N/A	ND	Pass
Teflubenzuron	0.007 / 0.022	0.025	N/A	ND	Pass
Tetrachlorvinphos	0.003 / 0.008	0.01	N/A	ND	Pass
Tetramethrin	0.021 / 0.063	0.1	N/A	ND	Pass
Thiabendazole	0.006 / 0.020	0.02	N/A	ND	Pass
Thiacloprid	0.003 / 0.009	0.01	N/A	ND	Pass
Thiamethoxam	0.003 / 0.010	0.01	N/A	ND	Pass
Thiophanate-methyl	0.013 / 0.040	0.05	N/A	ND	Pass
Trifloxystrobin	0.003 / 0.009	0.02	N/A	ND	Pass

Mycotoxin Analysis

Pass

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS

Mycotoxin Test Results

11/22/2021

PASS

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Compound	LOD/LOQ (μg/kg)	Action Limit (μg/kg)	Measurement Uncertainty (μg/kg)	Result (μg/kg)	Result
Aflatoxin B1	1.6 / 5	5	N/A	ND	Pass
Aflatoxin B2	1.4 / 4.1	20	N/A	ND	Pass
Aflatoxin G1	1.6 / 4.9	20	N/A	ND	Pass
Aflatoxin G2	1.6 / 5	20	N/A	ND	Pass
Total Aflatoxin		20	±	ND	Pass
Ochratoxin A	1.6 / 5	5	N/A	ND	Pass

Residual Solvents Analysis

Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

11/25/2021

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
Propane	0.133 / 0.445	500	N/A	ND	Pass
2-Methylpropane (Isobutane)	0.04 / 0.133	5000	N/A	ND	Pass
n-Butane	0.042 / 0.141	2000	N/A	ND	Pass
Total Butanes		500	±	ND	Pass
2-Methylbutane (Isopentane)	0.065 / 0.216	5000	N/A	ND	Pass
2,2-Dimethylpropane (Neopentane)	0.181 / 0.604		N/A	ND
n-Pentane	0.181 / 0.604	1000	N/A	ND	Pass
Total Pentanes		500	±	ND	Pass
2,2-Dimethylbutane (Neohexane)	0.147 / 0.488	290	N/A	ND	Pass
2,3-Dimethylbutane / 2-Methylpentane (Isohexane)	0.375 / 1.249	290	N/A	ND	Pass
3-Methylpentane	0.075 / 0.251	290	N/A	ND	Pass
n-Hexane	0.054 / 0.181	0	N/A	ND	Pass
Total Hexanes		290	±	ND	Pass
Cyclohexane	0.091 / 0.302	500	N/A	ND	Pass
n-Heptane	0.153 / 0.511	500	N/A	ND	Pass
Benzene	0.066 / 0.221	0	N/A	ND	Pass
Toluene	0.074 / 0.246	0	N/A	ND	Pass
Cumene	0.31 / 1.033	70	N/A	<LOQ	Pass
1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene)	0.213 / 0.71	2170	N/A	ND	Pass
1,2-Dimethylbenzene (o-Xylene)	0.239 / 0.797	2170	N/A	ND	Pass
Ethylbenzene	0.176 / 0.586	2170	N/A	ND	Pass
Total Xylenes	0.320 / 1.067	217	N/A	ND	Pass
Methanol	0.018 / 0.061	500	±0.0449	0.570	Pass
Ethanol	0.129 / 0.429	1000	±0.2694	3.564	Pass
1-Propanol	0.528 / 1.759	5000	N/A	ND	Pass
2-Propanol (Isopropyl Alcohol)	0.064 / 0.214	500	N/A	ND	Pass
1-Butanol	0.17 / 0.565	5000	N/A	ND	Pass
2-Butanol	0.535 / 1.784	5000	N/A	ND	Pass
1-Pentanol	0.379 / 1.262		N/A	ND
Acetone	0.083 / 0.277	5000	N/A	ND	Pass
2-Butanone	0.193 / 0.642	5000	N/A	ND	Pass
Tetrahydrofuran	0.22 / 0.735	720	N/A	ND	Pass
Ethyl Ether	0.1 / 0.335	5000	N/A	ND	Pass
Ethylene Glycol	31.104 / 103.68	620	N/A	ND	Pass
2-Ethoxyethanol	1.08 / 3.599	160	N/A	ND	Pass
1,2-Dimethoxyethane	1.093 / 3.645	100	N/A	ND	Pass
1,4-Dioxane	0.379 / 1.265	380	N/A	ND	Pass
Ethylene Oxide	0.05 / 0.166	5	N/A	ND	Pass
Ethyl Acetate	0.29 / 0.967	1000	N/A	ND	Pass
Isopropyl Acetate	0.346 / 1.153	5000	N/A	ND	Pass
Chloroform	0.1 / 0.2	1	N/A	ND	Pass
Dichloromethane (Methylene Chloride)	0.114 / 0.381	600	N/A	ND	Pass
Trichloroethylene	0.1 / 0.3	80	N/A	ND	Pass
1,2-Dichloroethane	0.05 / 0.1	5	N/A	ND	Pass
Sulfolane	11.728 / 39.094	160	N/A	ND	Pass
Dimethyl Sulfoxide	1.679 / 5.596	5000	N/A	ND	Pass
Acetonitrile	0.049 / 0.164	410	N/A	<LOQ	Pass
Pyridine	0.118 / 0.394	100	N/A	ND	Pass
N,N-Dimethylacetamide	0.2 / 0.668	1090	N/A	ND	Pass
N,N-Dimethylformamide	0.335 / 1.116	880	N/A	ND	Pass

Total Butanes = n-Butane + 2-Methylpropane (Isobutane)

Total Pentanes = n-Pentane + 2-Methylbutane (Isopentane)

Total Hexanes = n-Hexane + 2,2-Dimethylbutane (Neohexane) + 2,3-Dimethylbutane / 2-Methylpentane (Isohexane) + 3-Methylpentane

Total Xylenes = 1,2-Dimethylbenzene (o-Xylene) + 1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene) + Ethylbenzene

Heavy Metals Analysis

Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

11/23/2021

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
Arsenic	0.02 / 0.1	0.42	N/A	<LOQ	Pass
Cadmium	0.02 / 0.05	0.27	N/A	ND	Pass
Lead	0.04 / 0.1	0.5	N/A	ND	Pass
Mercury	0.002 / 0.01	0.4	N/A	ND	Pass

Microbiology Analysis

Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants. And Analysis conducted by 3M^TM Petrifilm^TM and plate counts of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants and QSP 6794 - Plating with 3M^TM Petrifilm^TM

Microbiology Test Results (PCR)

11/24/2021

PASS

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Compound	Action Limit	Result (cfu/g)	Result
Bile-Tolerant Gram-Negative Bacteria	100	ND	Pass
Campylobacter spp.	Not Detected in 1g	ND	Pass
Candida albicans	Not Detected in 1g	ND	Pass
Shiga toxin-producing Escherichia coli	Not Detected in 1g	ND	Pass
Salmonella spp.	Not Detected in 1g	ND	Pass
Aspergillus fumigatus	Not Detected in 1g	ND	Pass
Aspergillus flavus	Not Detected in 1g	ND	Pass
Aspergillus niger	Not Detected in 1g	ND	Pass
Aspergillus terreus	Not Detected in 1g	ND	Pass
Listeria monocytogenes	Not Detected in 1g	ND	Pass
Pseudomonas aeruginosa	Not Detected in 1g	ND	Pass
Staphylococcus aureus	Not Detected in 1g	ND	Pass
Yersinia spp.	Not Detected in 1g	ND	Pass

Microbiology Test Results (PLATING)

11/24/2021

PASS

Swipe left on table to see additional columns

Compound	Action Limit (cfu/g)	Result (cfu/g)	Result
Total Yeast and Mold	10	ND	Pass
Total Enterobacteriaceae	1000	ND	Pass
Escherichia coli	Not Detected in 1g	ND	Pass
Coliforms	100	ND	Pass
Total Aerobic Bacteria	100	ND	Pass

Notes

COA Notes:

COA amended, update to order detail information.

COA ID: 211119Q002-002

For quality assurance purposes. Not a Regulatory Hemp Lab Test Report. These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

Sample Certification: Action Limits used in this report are a compilation of guidance from state regulatory agencies in all states except Alaska. Action limits for required tests are the lower of any conflicting state regulations.

Decision Rule: Statements of conformity (e.g. Pass/Fail) to specifications are made in this report without taking measurement uncertainty into account. Where statements of conformity are made in this report, the following decision rules are applied: PASS - Results within limits/specifications, FAIL - Results exceed limits/specifications.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT), too numerous to count >250 cfu/plate (TNTC), colony-forming unit (cfu)