Certificate of Analysis
REGULATORY COMPLIANCE

Sample Name:

Dollar Dose - Apple Lozenges

Infused, Solid Edible

Date Issued:

05/09/2023

Overall Batch Result:

Pass

Serving Size:

4.5 grams

Sum Cannabinoids 4.8812 mg/unit
Total Cannabinoids 4.8812 mg/unit
Total THC 4.6283 mg/unit
Total CBD ND

Sample Information

Sample Details

Sample ID:230505N009

Batch Number:DLD-APL-230428

Cultivator / Manufacturer

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Distributor

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Sampling Method: QSP 1265 - Sampling of Cannabis and Product Batches

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Cannabinoid Analysis - Summary

Sum of Cannabinoids: 4.8812 mg/unit

Total Cannabinoids: 4.8812 mg/unit

Total THC: 4.6283 mg/unit

Total CBD: ND

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa+Δ8-THC) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + CBL + CBN

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877)) + Δ8-THC
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Safety Analysis - Summary

Δ9-THC per Unit: Pass

Δ9-THC per Serving: Pass

Pesticides: Pass

Mycotoxins: Pass

Residual Solvents: Pass

Heavy Metals: Pass

Microbiology: Pass

Foreign Material: Pass

Water Activity: Pass

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

†Analytes not part of our ISO/IEC 17025 scope of accreditation.

Method: LA-SOP-101 Cannabinoid Analysis by HPLC-DAD

Summary

Total Cannabinoids: 4.8812 mg/unit

Total THC: 4.6283 mg/unit

(Δ9-THC+0.877*THCa+Δ8-THC)

Total CBD: ND

(CBD+0.877*CBDa)

Total CBG: 0.1503 mg/unit

Total CBG (CBG+0.877*CBGa)

Total THCV: 0.0257 mg/unit

Total THCV (THCV+0.877*THCVa)

Total CBC: 0.0770 mg/unit

Total CBC (CBC+0.877*CBCa)

Total CBDV: ND

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

05/08/2023

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
Δ9 Tetrahydrocannabinol (Δ9THC) 0.0014 / 0.0042 ±0.00617 1.0285 0.10285
Cannabigerol (CBG) 0.0009 / 0.0028 ±0.00013 0.0334 0.00334
Cannabichromene (CBC) 0.0008 / 0.0025 ±0.00006 0.0171 0.00171
Tetrahydrocannabivarin (THCV) 0.0006 / 0.0021 ±0.00002 0.0057 0.00057
Cannabidiol (CBD) 0.0010 / 0.0029 N/A ND ND
Cannabicyclol (CBL)† 0.0013 / 0.0045 N/A ND ND
Cannabinol (CBN) 0.0005 / 0.0021 N/A ND ND
Cannabichromenic Acid (CBCa) 0.0005 / 0.0021 N/A ND ND
Cannabidivarin (CBDV) 0.0015 / 0.0046 N/A ND ND
Cannabidiolic Acid (CBDa) 0.0006 / 0.0021 N/A ND ND
Cannabigerolic Acid (CBGa) 0.0007 / 0.0022 N/A ND ND
Tetrahydrocannabinolic Acid (THCa) 0.0004 / 0.0021 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.0005 / 0.0021 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.0008 / 0.0023 N/A ND ND
∆8 Tetrahydrocannabinol (Δ8THC) 0.0010 / 0.0029 N/A ND ND
SUM OF CANNABINOIDS 1.0847 mg/g 0.10847%
Unit Mass:

4.5 grams

/

Serving Size:

4.5 grams

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Δ9-THC per Unit 110 per-package limit 4.6283 mg/unit Pass
Δ9-THC per Serving 11 per-serving limit 4.6283 mg/serving Pass
Total THC per Unit 4.6283 mg/unit
Total THC Per Serving 4.6283 mg/serving
CBD per Unit ND
CBD per Serving ND
Total CBD per Unit ND
Total CBD per Serving ND
Sum of Cannabinoids per Unit 4.8812 mg/unit
Sum of Cannabinoids per Serving 4.8812 mg/serving
Total Cannabinoids per Unit 4.8812 mg/unit
Total Cannabinoids per Serving 4.8812 mg/serving
Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: LA-SOP-301 Pesticides & Mycotoxins Analysis by LC-MS or LA-SOP-302 Pesticides Analysis by GC-MS

Pesticide Test Results

05/09/2023

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Aldicarb 0.0260 / 0.0770 ≥ LOD N/A ND Pass
Carbofuran 0.0260 / 0.0800 ≥ LOD N/A ND Pass
Chlordane* 0.0300 / 0.0900 ≥ LOD N/A ND Pass
Chlorfenapyr* 0.0160 / 0.0490 ≥ LOD N/A ND Pass
Chlorpyrifos 0.0110 / 0.0330 ≥ LOD N/A ND Pass
Coumaphos 0.0290 / 0.0890 ≥ LOD N/A ND Pass
Daminozide 0.0260 / 0.0780 ≥ LOD N/A ND Pass
Dichlorvos (DDVP) 0.0070 / 0.0220 ≥ LOD N/A ND Pass
Dimethoate 0.0190 / 0.0580 ≥ LOD N/A ND Pass
Ethoprophos 0.0300 / 0.0920 ≥ LOD N/A ND Pass
Etofenprox 0.0290 / 0.0870 ≥ LOD N/A ND Pass
Fenoxycarb 0.0330 / 0.1000 ≥ LOD N/A ND Pass
Fipronil 0.0170 / 0.0530 ≥ LOD N/A ND Pass
Imazalil 0.0310 / 0.0950 ≥ LOD N/A ND Pass
Methiocarb 0.0090 / 0.0260 ≥ LOD N/A ND Pass
Mevinphos 0.0180 / 0.0550 ≥ LOD N/A ND Pass
Paclobutrazol 0.0320 / 0.0980 ≥ LOD N/A ND Pass
Parathion-methyl* 0.0240 / 0.0720 ≥ LOD N/A ND Pass
Propoxur 0.0220 / 0.0680 ≥ LOD N/A ND Pass
Spiroxamine 0.0330 / 0.0990 ≥ LOD N/A ND Pass
Thiacloprid 0.0220 / 0.0660 ≥ LOD N/A ND Pass
Abamectin 0.0330 / 0.0990 0.3 N/A ND Pass
Acephate 0.0270 / 0.0810 5 N/A ND Pass
Acequinocyl 0.0270 / 0.0820 4 N/A ND Pass
Acetamiprid 0.0240 / 0.0730 5 N/A ND Pass
Azoxystrobin 0.0160 / 0.0500 40 N/A ND Pass
Bifenazate 0.0240 / 0.0740 5 N/A ND Pass
Bifenthrin 0.1650 / 0.4990 0.5 N/A ND Pass
Boscalid 0.0260 / 0.0800 10 N/A ND Pass
Captan* 0.0970 / 0.2940 5 N/A ND Pass
Carbaryl 0.0370 / 0.1130 0.5 N/A ND Pass
Chlorantraniliprole 0.0530 / 0.1620 40 N/A ND Pass
Clofentezine 0.0290 / 0.0870 0.5 N/A ND Pass
Cyfluthrin 0.1940 / 0.5870 1 N/A ND Pass
Cypermethrin 0.0490 / 0.1480 1 N/A ND Pass
Diazinon 0.0220 / 0.0670 0.2 N/A ND Pass
Dimethomorph 0.0700 / 0.2120 20 N/A ND Pass
Etoxazole 0.0240 / 0.0730 1.5 N/A ND Pass
Fenhexamid 0.0150 / 0.0460 10 N/A ND Pass
Fenpyroximate 0.0080 / 0.0250 2 N/A ND Pass
Flonicamid 0.0120 / 0.0370 2 N/A ND Pass
Fludioxonil 0.0300 / 0.0910 30 N/A ND Pass
Hexythiazox 0.0150 / 0.0460 2 N/A ND Pass
Imidacloprid 0.0400 / 0.1220 3 N/A ND Pass
Kresoxim-methyl 0.0290 / 0.0890 1 N/A ND Pass
Malathion 0.1370 / 0.4160 5 N/A ND Pass
Metalaxyl 0.0600 / 0.1820 15 N/A ND Pass
Methomyl 0.0130 / 0.0390 0.1 N/A ND Pass
Myclobutanil 0.0320 / 0.0980 9 N/A ND Pass
Naled 0.0160 / 0.0480 0.5 N/A ND Pass
Oxamyl 0.0380 / 0.1160 0.2 N/A ND Pass
Pentachloronitrobenzene (Quintozene)* 0.0270 / 0.0820 0.2 N/A ND Pass
Permethrin 0.0300 / 0.0900 20 N/A ND Pass
Phosmet 0.0300 / 0.0920 0.2 N/A ND Pass
Piperonyl Butoxide 0.0400 / 0.1210 8 N/A ND Pass
Prallethrin 0.0260 / 0.0790 0.4 N/A ND Pass
Propiconazole 0.0310 / 0.0940 20 N/A ND Pass
Pyrethrins 0.0590 / 0.1790 1 N/A ND Pass
Pyridaben 0.0240 / 0.0740 3 N/A ND Pass
Spinetoram 0.0210 / 0.0630 3 N/A ND Pass
Spinosad 0.0290 / 0.0880 3 N/A ND Pass
Spiromesifen 0.0320 / 0.0970 12 N/A ND Pass
Spirotetramat 0.0110 / 0.0330 13 N/A ND Pass
Tebuconazole 0.0200 / 0.0610 2 N/A ND Pass
Thiamethoxam 0.0360 / 0.1080 4.5 N/A ND Pass
Trifloxystrobin 0.0320 / 0.0970 30 N/A ND Pass

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: LA-SOP-301 Pesticides & Mycotoxins Analysis by LC-MS

Mycotoxin Test Results

05/09/2023

PASS

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Compound LOD/LOQ
(μg/kg)
Action Limit
(μg/kg)
Measurement
Uncertainty
(μg/kg)
Result
(μg/kg)
Result
Aflatoxin B1 1.6000 / 4.8600 N/A ND
Aflatoxin B2 1.0800 / 3.2800 N/A ND
Aflatoxin G1 1.0300 / 3.1400 N/A ND
Aflatoxin G2 2.0200 / 6.1300 N/A ND
Ochratoxin A 5.9800 / 18.1100 20 N/A ND Pass
Total Aflatoxin 20 ± ND Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: LA-SOP-202 Solvent Analysis by GC-MS

Category 1 Residual Solvents Test Results

05/09/2023

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Benzene 0.09 / 1.00 1 N/A ND Pass
Chloroform 0.21 / 1.00 1 N/A ND Pass
Ethylene Oxide 0.30 / 1.00 1 N/A ND Pass
Trichloroethylene 0.06 / 1.00 1 N/A ND Pass
1,2-Dichloroethane 0.08 / 1.00 1 N/A ND Pass
Dichloromethane (Methylene Chloride) 0.11 / 1.00 1 N/A ND Pass
Category 2 Residual Solvents Test Results

05/09/2023

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Acetone 9.19 / 50.00 5000 N/A ND Pass
Ethanol 14.96 / 50.00 5000 N/A <LOQ Pass
Propane 42.44 / 141.57 5000 N/A ND Pass
Toluene 23.99 / 80.03 890 N/A ND Pass
Methanol 149.00 / 497.01 3000 N/A ND Pass
n-Butane 35.32 / 117.80 5000 N/A ND Pass
n-Hexane 33.99 / 113.37 290 N/A ND Pass
n-Heptane 42.11 / 140.48 5000 N/A ND Pass
n-Pentane 28.08 / 93.67 5000 N/A ND Pass
Ethyl Ether 16.00 / 53.36 5000 N/A ND Pass
Acetonitrile 17.49 / 58.35 410 N/A ND Pass
Ethyl Acetate 12.80 / 50.00 5000 N/A ND Pass
Total Xylenes 65.49 / 218.45 2170 N/A ND Pass
2-Propanol (Isopropyl Alcohol) 19.79 / 66.02 5000 N/A ND Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: LA-SOP-502 Heavy Metals Analysis by ICP-MS

Heavy Metals Test Results

05/08/2023

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Arsenic 0.006 / 0.05 1.5 N/A <LOQ Pass
Cadmium 0.003 / 0.05 0.5 N/A ND Pass
Lead 0.010 / 0.05 0.5 N/A ND Pass
Mercury 0.003 / 0.05 3 N/A <LOQ Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants.

Method: LA-SOP-401 Microbial Data Analysis by qPCR

Microbiology Test Results

05/08/2023

PASS

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Compound Action Limit Result Result
Salmonella spp. Not Detected in 1g ND Pass
Shiga toxin-producing Escherichia coli Not Detected in 1g ND Pass

Visual analysis includes, but is not limited to, sand, soil, cinders, dirt, mold, hair, insect fragments, and mammalian excreta.

Method: LA-SOP-600 Foreign Material

Foreign Material Test Results

05/06/2023

PASS

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Compound Action Limit Result Result
Hair Count > 1 per 3 grams 0.0 Pass
Insect Fragment Count > 1 per 3 grams 0.0 Pass
Mammalian Excreta Count > 1 per 3 grams 0.0 Pass
Total Sample Area Covered by Mold >25% None Pass
Total Sample Area Covered by Sand, Soil, Cinders, or Dirt >25% None Pass
Total Sample Area Covered by an Imbedded Foreign Material >25% None Pass

Method: LA-SOP-102 Water Activity Analysis

Water Activity Test Results

05/08/2023

PASS

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Compound LOD/LOQ
(Aw)
Action Limit
(Aw)
Measurement
Uncertainty
(Aw)
Result
(Aw)
Result
Water Activity 0.030 / 0.250 0.85 ±0.0142 0.303 Pass

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