DIST-GDFS-0823A

Certificate of Analysis

HEMP QUALITY ASSURANCE TEST

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Sample Name:

DIST-GDFS-0823A

Concentrate, Hemp

Total THC 3.577%

Total CBD 76.11%

Sum Cannabinoids 87.96%

Total Cannabinoids 87.96%

Sample Information

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Sample Details

Sample ID:230905P008

Batch Number:DIST-GDFS-0823A

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Cultivator / Manufacturer

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Cannabinoid Analysis - Summary

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Total THC: 3.577%

Total CBD: 76.11%

Sum of Cannabinoids: 87.96%

Total Cannabinoids: 87.96%

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ⁹-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ⁹-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ⁸-THC + CBL + CBN

Total Cannabinoids = (Δ⁹-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ⁸-THC + CBL + CBN

Why are Sum of Cannabinoids and Total Cannabinoids calculated separately?

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Safety Analysis - Summary

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Pesticides: Detected

Residual Solvents: ND

Heavy Metals: ND

Microbiology (PCR): ND

Microbiology (Plating): ND

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Cannabinoid Analysis

Tested

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 3.577%

(Δ⁹-THC+0.877*THCa)

Total CBD: 76.11%

(CBD+0.877*CBDa)

Total Cannabinoids: 87.96%

Total CBG: 4.741%

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 2.82%

Total CBC (CBC+0.877*CBCa)

Total CBDV: 0.357%

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

09/08/2023

Result Views

Table Pie Chart

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Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
Cannabidiol (CBD)	0.07 / 0.29	±27.400	761.10	76.110
Cannabigerol (CBG)	0.06 / 0.19	±1.455	47.41	4.741
Δ9 Tetrahydrocannabinol (Δ9THC)	0.06 / 0.26	±0.959	35.77	3.577
Cannabichromene (CBC)	0.2 / 0.5	±0.65	28.2	2.82
Cannabidivarin (CBDV)	0.04 / 0.15	±0.121	3.57	0.357
Cannabinol (CBN)	0.1 / 0.3	±0.18	3.5	0.35
Cannabicyclol (CBL)	0.06 / 0.24	N/A	ND	ND
Cannabichromenic Acid (CBCa)	0.07 / 0.28	N/A	ND	ND
Cannabidiolic Acid (CBDa)	0.02 / 0.19	N/A	ND	ND
Cannabigerolic Acid (CBGa)	0.1 / 0.2	N/A	ND	ND
Tetrahydrocannabivarin (THCV)	0.1 / 0.2	N/A	ND	ND
Tetrahydrocannabinolic Acid (THCa)	0.05 / 0.14	N/A	ND	ND
Cannabidivarinic Acid (CBDVa)	0.03 / 0.53	N/A	ND	ND
Tetrahydrocannabivarinic Acid (THCVa)	0.07 / 0.20	N/A	ND	ND
∆8 Tetrahydrocannabinol (Δ8THC)	0.1 / 0.4	N/A	ND	ND
SUM OF CANNABINOIDS			879.6 mg/g	87.96%

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Pesticide Analysis

Detected

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

09/07/2023

DETECTED

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Compound	LOD/LOQ (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)
Abamectin	0.03 / 0.10	N/A	ND
Azoxystrobin	0.02 / 0.07	N/A	ND
Bifenazate	0.01 / 0.04	N/A	ND
Bifenthrin	0.02 / 0.05	±0.008	0.19
Boscalid	0.03 / 0.09	N/A	ND
Chlorpyrifos	0.02 / 0.06	N/A	ND
Cypermethrin	0.11 / 0.32	N/A	ND
Etoxazole	0.02 / 0.06	N/A	ND
Hexythiazox	0.02 / 0.07	N/A	ND
Imidacloprid	0.04 / 0.11	N/A	ND
Malathion	0.03 / 0.09	N/A	ND
Myclobutanil	0.03 / 0.09	N/A	ND
Permethrin	0.04 / 0.12	N/A	ND
Piperonyl Butoxide	0.02 / 0.07	N/A	ND
Propiconazole	0.02 / 0.07	N/A	ND
Spiromesifen	0.02 / 0.05	N/A	ND
Tebuconazole	0.02 / 0.07	N/A	ND
Trifloxystrobin	0.03 / 0.08	N/A	ND

Residual Solvents Analysis

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

09/07/2023

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Compound	LOD/LOQ (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)
1,2-Dichloroethane	0.05 / 0.1	N/A	ND
Benzene	0.03 / 0.09	N/A	ND
Chloroform	0.1 / 0.2	N/A	ND
Dichloromethane (Methylene Chloride)	0.3 / 0.9	N/A	ND
Ethylene Oxide	0.3 / 0.8	N/A	ND
Trichloroethylene	0.1 / 0.3	N/A	ND
2-Propanol (Isopropyl Alcohol)	10 / 40	N/A	ND
Acetone	20 / 50	N/A	ND
Acetonitrile	2 / 7	N/A	ND
Ethanol	20 / 50	N/A	ND
Ethyl Acetate	20 / 60	N/A	ND
Ethyl Ether	20 / 50	N/A	ND
Methanol	50 / 200	N/A	ND
n-Butane	10 / 50	N/A	ND
n-Heptane	20 / 60	N/A	ND
n-Hexane	2 / 5	N/A	ND
n-Pentane	20 / 50	N/A	ND
Propane	10 / 20	N/A	ND
Toluene	7 / 21	N/A	ND
Total Xylenes	50 / 160	N/A	ND

Heavy Metals Analysis

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

09/09/2023

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Compound	LOD/LOQ (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)
Arsenic	0.02 / 0.1	N/A	ND
Cadmium	0.02 / 0.05	N/A	ND
Lead	0.04 / 0.1	N/A	ND
Mercury	0.002 / 0.01	N/A	ND

Microbiology Analysis

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants. And Analysis conducted by 3M^TM Petrifilm^TM and plate counts of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants and QSP 6794 - Plating with 3M^TM Petrifilm^TM

Microbiology Test Results (PCR)

09/09/2023

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Compound	Result (cfu/g)
Salmonella spp.	ND
Staphylococcus aureus	ND
Bile-Tolerant Gram-Negative Bacteria	ND
Shiga toxin-producing Escherichia coli	ND

Microbiology Test Results (PLATING)

09/09/2023

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Compound	Result (cfu/g)
Total Yeast and Mold	ND
Total Aerobic Bacteria	ND

COA ID: 230905P008-001

For quality assurance purposes. Not a Regulatory Hemp Lab Test Report. These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT), too numerous to count >250 cfu/plate (TNTC), colony-forming unit (cfu)