Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

GREEN GRUFF Gold EASE Veterinary - Jar | 60 Soft Chews

Infused, Hemp

Date Issued:

02/01/2024

Serving Size:

3 grams

Total THC 8.8020 mg/unit
Total CBD 563.760 mg/unit
Sum Cannabinoids 597.420 mg/unit
Total Cannabinoids 597.420 mg/unit
Total Terpenoids 0.0012%
Top 3 Terpenoids
  1. β-Caryophyllene 0.0012%
  2. Guaiol <LOQ
  3. Borneol <LOQ

Sample Information

Sample Details

Sample ID:240126L039

Batch Number:3255894

Cultivator / Manufacturer

Show Details

Distributor / Tested For

Show Details

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Cannabinoid Analysis - Summary

Calculated using Dry-Weight

Total THC: 8.8020 mg/unit

Total CBD: 563.760 mg/unit

Sum of Cannabinoids: 597.420 mg/unit

Total Cannabinoids: 597.420 mg/unit

Moisture:7.1%

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN + exo-THC + Δ8-THCV + Δ8-iso-THC + 9S-HHC + 9R-HHC + Δ10-THC + Δ9-THC Acetate

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN + exo-THC + Δ8-THCV + Δ8-iso-THC + 9S-HHC + 9R-HHC + Δ10-THC + Δ9-THC Acetate

Dry weight: The weight of a sample after it goes through the drying process.

Pursuant to section § 5724 of California Code of Regulations Title 16 Division 42. Department of Cannabis Control, the equation for moisture correction is:  Dry-weight percent cannabinoid = wet-weight percent cannabinoid / (1 − percent moisture / 100)

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

Total Terpenoids: 0.0012%

 
 
 

1

β-Caryophyllene (0.0012%)

2

Guaiol (<LOQ)

3

Borneol (<LOQ)

Safety Analysis - Summary

Pesticides: ND

Mycotoxins: ND

Residual Solvents: ND

Heavy Metals: Detected

Microbiology (PCR): Detected

Microbiology (Plating): Detected

Foreign Material: Pass

Water Activity: Detected

Additives: Detected

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD). Calculated using Dry-Weight.

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD or QSP 34181 - Semisynthetic Cannabinoids Analysis by HPLC

Summary

Total THC: 8.8020 mg/unit

9-THC+0.877*THCa)

Total CBD: 563.760 mg/unit

(CBD+0.877*CBDa)

Total Cannabinoids: 597.420 mg/unit

Total CBG: ND

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 20.160 mg/unit

Total CBC (CBC+0.877*CBCa)

Total CBDV: ND

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

01/29/2024

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
Cannabidiol (CBD) 0.004 / 0.011 ±0.1168 3.132 0.3132
Cannabichromene (CBC) 0.003 / 0.010 ±0.0036 0.112 0.0112
Δ9 Tetrahydrocannabinol (Δ9THC) 0.0006 / 0.0053 ±0.00268 0.0489 0.00489
Cannabinol (CBN) 0.001 / 0.007 ±0.0007 0.026 0.0026
Cannabidiolic Acid (CBDa) 0.001 / 0.026 N/A <LOQ <LOQ
Cannabigerol (CBG) 0.002 / 0.006 N/A ND ND
Cannabicyclol (CBL) 0.003 / 0.010 N/A ND ND
Cannabichromenic Acid (CBCa) 0.001 / 0.015 N/A ND ND
Cannabidivarin (CBDV) 0.002 / 0.012 N/A ND ND
Cannabigerolic Acid (CBGa) 0.002 / 0.007 N/A ND ND
Tetrahydrocannabivarin (THCV) 0.002 / 0.012 N/A ND ND
Tetrahydrocannabinolic Acid (THCa) 0.0003 / 0.0019 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.001 / 0.018 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.002 / 0.019 N/A ND ND
9R-Hexahydrocannabinol (9R-HHC) 0.027 / 0.089 N/A ND ND
9S-Hexahydrocannabinol (9S-HHC) 0.027 / 0.090 N/A ND ND
Exo-Tetrahydrocannabinol (Exo-THC) 0.028 / 0.093 N/A ND ND
∆8 Tetrahydrocannabinol (Δ8THC) 0.01 / 0.02 N/A ND ND
Δ10 Tetrahydrocannabinol (Δ10THC) 0.024 / 0.078 N/A ND ND
∆8 Tetrahydrocannabivarin (Δ8THCV) 0.012 / 0.039 N/A ND ND
∆8 Isotetrahydrocannabinol (Δ8-iso-THC) 0.025 / 0.084 N/A ND ND
Δ9 Tetrahydrocannabinol Acetate (Δ9THC Acetate) 0.023 / 0.077 N/A ND ND
SUM OF CANNABINOIDS 3.319 mg/g 0.3319%
Unit Mass:

180 grams

/

Serving Size:

3 grams

Swipe left on table to see additional columns

Δ9-THC per Unit 8.8020 mg/unit
Δ9-THC per Serving 0.1467 mg/serving
Total THC per Unit 8.8020 mg/unit
Total THC Per Serving 0.1467 mg/serving
CBD per Unit 563.760 mg/unit
CBD per Serving 9.396 mg/serving
Total CBD per Unit 563.760 mg/unit
Total CBD per Serving 9.396 mg/serving
Sum of Cannabinoids per Unit 597.420 mg/unit
Sum of Cannabinoids per Serving 9.957 mg/serving
Total Cannabinoids per Unit 597.420 mg/unit
Total Cannabinoids per Serving 9.957 mg/serving
Moisture Test Result

7.1% Tested 01/29/2024 Method: QSP 1224 - Loss on Drying (Moisture)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

Summary

Total Terpenoids (mg/g): 0.012 mg/g

Total Terpenoids (%): 0.0012%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume.

  1. β-Caryophyllene 0.0012%

    A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB2 receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

  2. Guaiol <LOQ

    A sesquiterpene alcohol with a fragrance that can be described as floral, piney, herbal and woody. Found in guaiacum, cypress pine, ginseng, melaleuca, goatweed, incense grass...etc.

  3. Borneol <LOQ

    A monoterpenoid alcohol with a fragrance that can be described as fresh, piney and woody. Found in forskohlii, rosemary, coriander, Scotch pine, black-jack, ginger, oregano, savory, feverfew, rose gum, Aztec marigold, pennyroyal, sakhalin fir...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

01/29/2024

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
β-Caryophyllene 0.004 / 0.012 ±0.0003 0.012 0.0012
Guaiol 0.009 / 0.030 N/A <LOQ <LOQ
Borneol 0.005 / 0.016 N/A <LOQ <LOQ
Nerol 0.003 / 0.011 N/A ND ND
Cedrol 0.008 / 0.027 N/A ND ND
Camphor 0.006 / 0.019 N/A ND ND
Fenchol 0.010 / 0.034 N/A ND ND
Menthol 0.008 / 0.025 N/A ND ND
Myrcene 0.008 / 0.025 N/A ND ND
Camphene 0.005 / 0.015 N/A ND ND
Fenchone 0.009 / 0.028 N/A ND ND
Geraniol 0.002 / 0.007 N/A ND ND
Limonene 0.005 / 0.016 N/A ND ND
Linalool 0.009 / 0.032 N/A ND ND
Pulegone 0.003 / 0.011 N/A ND ND
Sabinene 0.004 / 0.014 N/A ND ND
p-Cymene 0.005 / 0.016 N/A ND ND
Nerolidol 0.006 / 0.019 N/A ND ND
Terpineol 0.009 / 0.031 N/A ND ND
Valencene 0.009 / 0.030 N/A ND ND
Eucalyptol 0.006 / 0.018 N/A ND ND
Isoborneol 0.004 / 0.012 N/A ND ND
Isopulegol 0.005 / 0.016 N/A ND ND
Citronellol 0.003 / 0.010 N/A ND ND
Terpinolene 0.008 / 0.026 N/A ND ND
β-Pinene 0.004 / 0.014 N/A ND ND
α-Pinene 0.005 / 0.017 N/A ND ND
β-Ocimene 0.006 / 0.020 N/A ND ND
Δ3-Carene 0.005 / 0.018 N/A ND ND
α-Cedrene 0.005 / 0.016 N/A ND ND
α-Humulene 0.009 / 0.029 N/A ND ND
Geranyl Acetate 0.004 / 0.014 N/A ND ND
α-Bisabolol 0.008 / 0.026 N/A ND ND
α-Terpinene 0.005 / 0.017 N/A ND ND
γ-Terpinene 0.006 / 0.018 N/A ND ND
Sabinene Hydrate 0.006 / 0.022 N/A ND ND
α-Phellandrene 0.006 / 0.020 N/A ND ND
Caryophyllene Oxide 0.010 / 0.033 N/A ND ND
trans-β-Farnesene 0.008 / 0.025 N/A ND ND
TOTAL 0.012 mg/g 0.0012%
Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

01/29/2024

ND

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Compound LOD/LOQ
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Abamectin 0.032 / 0.097 N/A ND
Acephate 0.006 / 0.018 N/A ND
Acequinocyl 0.009 / 0.027 N/A ND
Acetamiprid 0.016 / 0.049 N/A ND
Aldicarb 0.030 / 0.090 N/A ND
Allethrin 0.030 / 0.092 N/A ND
Atrazine 0.006 / 0.019 N/A ND
Azadirachtin 0.082 / 0.248 N/A ND
Azoxystrobin 0.003 / 0.009 N/A ND
Benzovindiflupyr 0.003 / 0.009 N/A ND
Bifenazate 0.003 / 0.009 N/A ND
Bifenthrin 0.021 / 0.064 N/A ND
Boscalid 0.003 / 0.009 N/A ND
Buprofezin 0.006 / 0.019 N/A ND
Captan 0.045 / 0.135 N/A ND
Carbaryl 0.007 / 0.020 N/A ND
Carbofuran 0.003 / 0.008 N/A ND
Chlorantraniliprole 0.006 / 0.018 N/A ND
Chlordane* 0.010 / 0.032 N/A ND
Chlorfenapyr* 0.005 / 0.015 N/A ND
Chlormequat chloride 0.022 / 0.066 N/A ND
Chlorpyrifos 0.013 / 0.039 N/A ND
Clofentezine 0.003 / 0.009 N/A ND
Clothianidin 0.008 / 0.025 N/A ND
Coumaphos 0.003 / 0.010 N/A ND
Cyantraniliprole 0.003 / 0.010 N/A ND
Cyfluthrin 0.052 / 0.159 N/A ND
Cypermethrin 0.051 / 0.153 N/A ND
Cyprodinil 0.003 / 0.008 N/A ND
Daminozide 0.026 / 0.077 N/A ND
Deltamethrin 0.059 / 0.180 N/A ND
Diazinon 0.006 / 0.017 N/A ND
Dichlorvos (DDVP) 0.012 / 0.038 N/A ND
Dimethoate 0.003 / 0.009 N/A ND
Dimethomorph 0.016 / 0.050 N/A ND
Dinotefuran 0.010 / 0.030 N/A ND
Diuron 0.013 / 0.040 N/A ND
Dodemorph 0.012 / 0.035 N/A ND
Endosulfan sulfate 0.016 / 0.048 N/A ND
Endosulfan-α* 0.004 / 0.014 N/A ND
Endosulfan-β* 0.006 / 0.019 N/A ND
Ethoprophos 0.003 / 0.009 N/A ND
Etofenprox 0.014 / 0.042 N/A ND
Etoxazole 0.007 / 0.020 N/A ND
Etridiazole* 0.002 / 0.005 N/A ND
Fenhexamid 0.003 / 0.008 N/A ND
Fenoxycarb 0.003 / 0.010 N/A ND
Fenpyroximate 0.007 / 0.020 N/A ND
Fensulfothion 0.003 / 0.010 N/A ND
Fenthion 0.003 / 0.010 N/A ND
Fenvalerate 0.033 / 0.099 N/A ND
Fipronil 0.003 / 0.010 N/A ND
Flonicamid 0.007 / 0.022 N/A ND
Fludioxonil 0.003 / 0.010 N/A ND
Fluopyram 0.003 / 0.009 N/A ND
Hexythiazox 0.003 / 0.010 N/A ND
Imazalil 0.003 / 0.009 N/A ND
Imidacloprid 0.003 / 0.010 N/A ND
Iprodione 0.077 / 0.233 N/A ND
Kinoprene 0.077 / 0.233 N/A ND
Kresoxim-methyl 0.006 / 0.019 N/A ND
λ-Cyhalothrin 0.068 / 0.206 N/A ND
Malathion 0.003 / 0.009 N/A ND
Metalaxyl 0.003 / 0.010 N/A ND
Methiocarb 0.003 / 0.008 N/A ND
Methomyl 0.008 / 0.025 N/A ND
Methoprene 0.172 / 0.521 N/A ND
Mevinphos 0.008 / 0.024 N/A ND
MGK-264 0.015 / 0.047 N/A ND
Myclobutanil 0.003 / 0.009 N/A ND
Naled 0.021 / 0.064 N/A ND
Novaluron 0.002 / 0.005 N/A ND
Oxamyl 0.017 / 0.051 N/A ND
Paclobutrazol 0.003 / 0.010 N/A ND
Parathion-methyl 0.016 / 0.050 N/A ND
Pentachloronitrobenzene (Quintozene)* 0.004 / 0.012 N/A ND
Permethrin 0.056 / 0.168 N/A ND
Phenothrin 0.016 / 0.047 N/A ND
Phosmet 0.007 / 0.020 N/A ND
Piperonyl Butoxide 0.010 / 0.029 N/A ND
Pirimicarb 0.003 / 0.009 N/A ND
Prallethrin 0.015 / 0.046 N/A ND
Propiconazole 0.027 / 0.080 N/A ND
Propoxur 0.003 / 0.008 N/A ND
Pyraclostrobin 0.003 / 0.010 N/A ND
Pyrethrins 0.016 / 0.049 N/A ND
Pyridaben 0.005 / 0.017 N/A ND
Pyriproxyfen 0.003 / 0.009 N/A ND
Resmethrin 0.013 / 0.039 N/A ND
Spinetoram 0.003 / 0.010 N/A ND
Spinosad 0.003 / 0.010 N/A ND
Spirodiclofen 0.031 / 0.093 N/A ND
Spiromesifen 0.016 / 0.050 N/A ND
Spirotetramat 0.003 / 0.010 N/A ND
Spiroxamine 0.020 / 0.062 N/A ND
Tebuconazole 0.003 / 0.010 N/A ND
Tebufenozide 0.003 / 0.008 N/A ND
Teflubenzuron 0.007 / 0.022 N/A ND
Tetrachlorvinphos 0.003 / 0.008 N/A ND
Tetramethrin 0.021 / 0.063 N/A ND
Thiabendazole 0.006 / 0.020 N/A ND
Thiacloprid 0.003 / 0.009 N/A ND
Thiamethoxam 0.003 / 0.010 N/A ND
Thiophanate-methyl 0.013 / 0.040 N/A ND
Trifloxystrobin 0.003 / 0.009 N/A ND

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS

Mycotoxin Test Results

01/29/2024

ND

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Compound LOD/LOQ
(μg/kg)
Measurement
Uncertainty
(μg/kg)
Result
(μg/kg)
Aflatoxin B1 1.6 / 5.0 N/A ND
Aflatoxin B2 1.4 / 4.1 N/A ND
Aflatoxin G1 1.6 / 4.9 N/A ND
Aflatoxin G2 1.6 / 5.0 N/A ND
Ochratoxin A 1.6 / 5.0 N/A ND
Total Aflatoxin ± ND

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

01/29/2024

ND

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Compound LOD/LOQ
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Propane 0.234 / 0.781 N/A ND
2-Methylpropane (Isobutane) 0.052 / 0.173 N/A ND
n-Butane 0.019 / 0.063 N/A ND
Total Butanes ± ND
2-Methylbutane (Isopentane) 0.310 / 1.035 N/A ND
2,2-Dimethylpropane (Neopentane) 0.035 / 0.117 N/A ND
n-Pentane 0.310 / 1.033 N/A ND
Total Pentanes ± ND
2,2-Dimethylbutane (Neohexane) 9.831 / 32.77 N/A ND
2,3-Dimethylbutane / 2-Methylpentane (Isohexane) 0.381 / 1.271 N/A ND
3-Methylpentane 0.109 / 0.365 N/A ND
n-Hexane 0.110 / 0.366 N/A ND
Total Hexanes ± ND
Cyclohexane 0.357 / 1.190 N/A ND
2,2-Dimethylpentane (Neoheptane) 0.493 / 1.642 N/A ND
2,3-Dimethylpentane 1.009 / 3.365 N/A ND
2,4-Dimethylpentane 0.737 / 2.458 N/A ND
3,3-Dimethylpentane 0.198 / 0.660 N/A ND
2,2,3-Trimethylbutane (Triptane) 0.521 / 1.738 N/A ND
2-Methylhexane (Isoheptane) 0.610 / 2.034 N/A ND
3-Methylhexane 0.235 / 0.785 N/A ND
3-Ethylpentane 0.304 / 1.012 N/A ND
n-Heptane 13.12 / 43.72 N/A ND
Total Heptanes ± ND
Cycloheptane 0.597 / 1.989 N/A ND
Benzene 0.089 / 0.295 N/A ND
Toluene 0.115 / 0.382 N/A ND
Cumene 0.180 / 0.600 N/A ND
1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene) 0.451 / 1.502 N/A ND
1,2-Dimethylbenzene (o-Xylene) 0.387 / 1.289 N/A ND
Ethylbenzene 0.370 / 1.233 N/A ND
Total Xylenes ± ND
Methanol 53.92 / 163.4 N/A ND
Ethanol 8.984 / 27.23 N/A ND
1-Propanol 1.540 / 5.133 N/A ND
2-Propanol (Isopropyl Alcohol) 8.421 / 25.52 N/A ND
1-Butanol 0.475 / 1.582 N/A ND
2-Butanol 7.248 / 24.16 N/A ND
1-Pentanol 1.461 / 4.869 N/A ND
Acetone 10.59 / 32.08 N/A ND
2-Butanone 0.169 / 0.564 N/A ND
Tetrahydrofuran 0.622 / 2.075 N/A ND
Ethyl Ether 0.197 / 0.658 N/A ND
Ethylene Glycol 3.803 / 12.68 N/A ND
2-Ethoxyethanol 1.235 / 4.118 N/A ND
1,2-Dimethoxyethane 2.116 / 7.052 N/A ND
1,4-Dioxane 0.468 / 1.558 N/A ND
Ethylene Oxide 0.253 / 0.844 N/A ND
Ethyl Acetate 1.123 / 3.745 N/A ND
Isopropyl Acetate 0.347 / 1.158 N/A ND
Chloroform 0.251 / 0.838 N/A ND
Dichloromethane (Methylene Chloride) 2.651 / 8.838 N/A ND
Trichloroethylene 0.299 / 0.996 N/A ND
1,2-Dichloroethane 0.162 / 0.541 N/A ND
1,1-Dichloroethene 0.185 / 0.616 N/A ND
1,2-Dichloroethene 0.428 / 1.427 N/A ND
Sulfolane 47.66 / 158.9 N/A ND
Dimethyl Sulfoxide 6.168 / 20.56 N/A ND
Acetonitrile 1.595 / 4.833 N/A ND
Pyridine 0.407 / 1.355 N/A ND
N,N-Dimethylacetamide 0.127 / 0.422 N/A ND
N,N-Dimethylformamide 0.946 / 3.153 N/A ND

Total Butanes = n-Butane + 2-Methylpropane (Isobutane)

Total Pentanes = n-Pentane + 2-Methylbutane (Isopentane) + 2,2-Dimethylpropane (Neopentane)

Total Hexanes = n-Hexane + 2,2-Dimethylbutane (Neohexane) + 2,3-Dimethylbutane / 2-Methylpentane (Isohexane) + 3-Methylpentane

Total Heptanes = 2,2-Dimethylpentane (Neoheptane) + 2,3-Dimethylpentane + 2,4-Dimethylpentane + 3,3-Dimethylpentane + 2,2,3-Trimethylbutane (Triptane) + 2-Methylhexane (Isoheptane) + 3-Methylhexane + 3-Ethylpentane + n-Heptane

Total Xylenes = 1,2-Dimethylbenzene (o-Xylene) + 1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene) + Ethylbenzene

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

01/29/2024

DETECTED

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Compound LOD/LOQ
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Arsenic 0.02 / 0.1 ±0.05 1.5
Boron 0.21 / 0.64 ±0.444 7.85
Cadmium 0.02 / 0.05 ±0.001 0.06
Chromium 0.12 / 0.35 ±0.014 0.51
Cobalt 0.10 / 0.30 N/A <LOQ
Copper 0.14 / 0.44 ±1.198 8.32
Lead 0.04 / 0.1 N/A <LOQ
Lithium 0.10 / 0.31 N/A ND
Manganese 0.13 / 0.40 ±1.042 31.20
Mercury 0.002 / 0.01 N/A <LOQ
Molybdenum 0.15 / 0.44 N/A <LOQ
Nickel 0.13 / 0.39 ±0.023 0.81
Selenium 0.5 / 1.5 N/A ND
Silver 0.15 / 0.47 N/A ND
Sulfur 78 / 235 ±73.4 2565
Titanium 0.12 / 0.38 ±0.058 1.63
Tungsten 0.10 / 0.32 N/A <LOQ
Zinc 0.8 / 2.5 ±6.25 47.6

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants. And Analysis conducted by 3MTM PetrifilmTM and plate counts of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants

Exclusions1: See Notes section at bottom.

Microbiology Test Results (PCR)

02/01/2024

DETECTED

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Compound Result
(cfu/g)
Yersinia spp. ND
Salmonella spp. ND
Candida albicans ND
Aspergillus niger ND
Aspergillus flavus ND
Campylobacter spp. ND
Aspergillus terreus ND
Aspergillus fumigatus ND
Staphylococcus aureus ND
Listeria monocytogenes ND
Pseudomonas aeruginosa Detected
Bile-Tolerant Gram-Negative Bacteria 26868.0
Shiga toxin-producing Escherichia coli ND
Microbiology Test Results (PLATING)

02/01/2024

DETECTED

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Compound Result
(cfu/g)
Coliforms ND
Escherichia coli ND
Total Yeast and Mold 10.0
Total Aerobic Bacteria 4100.0
Total Enterobacteriaceae ND

Visual analysis includes, but is not limited to, sand, soil, cinders, dirt, mold, hair, insect fragments, and mammalian excreta.

Method: QSP 1226 - Analysis of Foreign Material in Cannabis and Cannabis Products

Foreign Material Test Results

01/27/2024

PASS

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Compound Action Limit Result Result
Hair Count > 1 per 3 grams 0.0 Pass
Insect Fragment Count > 1 per 3 grams 0.0 Pass
Mammalian Excreta Count > 1 per 3 grams 0.0 Pass
Total Sample Area Covered by Mold >25% None Pass
Total Sample Area Covered by Sand, Soil, Cinders, or Dirt >25% None Pass
Total Sample Area Covered by an Imbedded Foreign Material >25% None Pass

Method: QSP 1227 - Analysis of Water Activity in Cannabis and Cannabis Products

Water Activity Test Results

01/26/2024

DETECTED

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Compound LOD/LOQ
(Aw)
Measurement
Uncertainty
(Aw)
Result
(Aw)
Water Activity 0.030 / 0.15 ±0.021 0.43

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 6793 - Analysis of Vitamin E by HPLC-DAD

Additives Test Results

01/30/2024

DETECTED

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Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
α-Tocopherol 0.069 / 0.209 ±0.0017 0.252 0.0252
δ-Tocopherol 0.061 / 0.183 ±0.0125 0.456 0.0456
Tocopheryl Acetate 0.047 / 0.143 N/A ND ND
ß-Tocopherol / γ-Tocopherol 0.093 / 0.281 ±0.0193 0.841 0.0841

* ß-Tocopherol / γ-Tocopherol reported as a sum

Notes

Deviations:

1. Analysis performed on matrix not included in ISO 17025 scope of accreditation.

Exclusions:

1. Action limit ignored/removed for total aerobic and total yeast and mold

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