Tone Down Spray

Certificate of Analysis

HEMP QUALITY ASSURANCE TEST

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Sample Name:

Tone Down Spray

Infused, Colorado Infused

Total THC Not Detected

Total CBD 0.0394%

Sum Cannabinoids 0.0394%

Total Cannabinoids 0.0394%

Total Terpenoids 0.0384%

Top 3 Terpenoids

Menthol 0.0295%
Borneol 0.0040%
trans-β-Farnesene 0.0028%

Sample Information

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Sample Details

Sample ID:240711K021

Batch Number:417 4C

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Cannabinoid Analysis - Summary

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Total THC: Not Detected

Total CBD: 0.0394%

Sum of Cannabinoids: 0.0394%

Total Cannabinoids: 0.0394%

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ⁹-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ⁹-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ⁸-THC + CBL + CBN

Total Cannabinoids = (Δ⁹-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ⁸-THC + CBL + CBN

Why are Sum of Cannabinoids and Total Cannabinoids calculated separately?

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

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Total Terpenoids: 0.0384%

Menthol (0.0295%)

Borneol (0.0040%)

trans-β-Farnesene (0.0028%)

Safety Analysis - Summary

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Pesticides: Pass

Heavy Metals: Pass

View Complete Test Results:

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Cannabinoid Analysis

Tested

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: Not Detected

(Δ⁹-THC+0.877*THCa)

Total CBD: 0.0394%

(CBD+0.877*CBDa)

Total Cannabinoids: 0.0394%

Total CBG: ND

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: ND

Total CBC (CBC+0.877*CBCa)

Total CBDV: ND

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

07/15/2024

Result Views

Table Pie Chart

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Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
Cannabidiol (CBD)	0.004 / 0.011	±0.0147	0.394	0.0394
Cannabichromene (CBC)	0.003 / 0.010	N/A	ND	ND
Cannabigerol (CBG)	0.002 / 0.006	N/A	ND	ND
Cannabicyclol (CBL)	0.003 / 0.010	N/A	ND	ND
Cannabinol (CBN)	0.001 / 0.007	N/A	ND	ND
Cannabichromenic Acid (CBCa)	0.001 / 0.015	N/A	ND	ND
Cannabidivarin (CBDV)	0.002 / 0.012	N/A	ND	ND
Cannabidiolic Acid (CBDa)	0.001 / 0.026	N/A	ND	ND
Cannabigerolic Acid (CBGa)	0.002 / 0.007	N/A	ND	ND
Tetrahydrocannabivarin (THCV)	0.002 / 0.012	N/A	ND	ND
Tetrahydrocannabinolic Acid (THCa)	0.001 / 0.005	N/A	ND	ND
Cannabidivarinic Acid (CBDVa)	0.001 / 0.018	N/A	ND	ND
Tetrahydrocannabivarinic Acid (THCVa)	0.002 / 0.019	N/A	ND	ND
∆8 Tetrahydrocannabinol (Δ8THC)	0.01 / 0.02	N/A	ND	ND
Δ9 Tetrahydrocannabinol (Δ9THC)	0.002 / 0.014	N/A	ND	ND
Total THC		N/A	ND	ND
SUM OF CANNABINOIDS			0.394 mg/g	0.0394%

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpenoid Analysis

Tested

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

Summary

Total Terpenoids (mg/g): 0.384 mg/g

Total Terpenoids (%): 0.0384%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume.

Menthol 0.0295%
A monoterpenoid alcohol with a fragrance that can be described as fresh, cool and herbal. It is responsible for the distinct odor of mint. It is frequently added to cigarettes and mouthwash as a flavorant. Found in mint, sunflower, micromeria, mountain mint, rose geranium, pennyroyal, tarragon, savory, basil, juniper, couch grass, rhubarb, acinos (basil thyme), ironwort, muña...etc.

Borneol 0.0040%
A monoterpenoid alcohol with a fragrance that can be described as fresh, piney and woody. Found in forskohlii, rosemary, coriander, Scotch pine, black-jack, ginger, oregano, savory, feverfew, rose gum, Aztec marigold, pennyroyal, sakhalin fir...etc.

trans-β-Farnesene 0.0028%
A sesquiterpene with a fragrance that can be described as green apple. Found in green apple skin, sandalwood, cedarwood, patchouli, hops, ginger, tumeric, potatos, gardenias, ylang-ylang, grapefruite, myrrh...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

07/15/2024

Result Views

Table Bar Graph

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Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
Menthol	0.008 / 0.025	±0.0092	0.295	0.0295
Borneol	0.005 / 0.016	±0.0013	0.040	0.0040
trans-β-Farnesene	0.008 / 0.025	±0.0008	0.028	0.0028
Isopulegol	0.005 / 0.016	±0.0007	0.021	0.0021
Camphor	0.006 / 0.019	N/A	<LOQ	<LOQ
Myrcene	0.008 / 0.025	N/A	<LOQ	<LOQ
Limonene	0.005 / 0.016	N/A	<LOQ	<LOQ
α-Humulene	0.009 / 0.029	N/A	<LOQ	<LOQ
β-Caryophyllene	0.004 / 0.012	N/A	<LOQ	<LOQ
Nerol	0.003 / 0.011	N/A	ND	ND
Cedrol	0.008 / 0.027	N/A	ND	ND
Guaiol	0.009 / 0.030	N/A	ND	ND
Fenchol	0.010 / 0.034	N/A	ND	ND
Camphene	0.005 / 0.015	N/A	ND	ND
Fenchone	0.009 / 0.028	N/A	ND	ND
Geraniol	0.002 / 0.007	N/A	ND	ND
Linalool	0.009 / 0.032	N/A	ND	ND
Pulegone	0.003 / 0.011	N/A	ND	ND
Sabinene	0.004 / 0.014	N/A	ND	ND
p-Cymene	0.005 / 0.016	N/A	ND	ND
Nerolidol	0.006 / 0.019	N/A	ND	ND
Terpineol	0.009 / 0.031	N/A	ND	ND
Valencene	0.009 / 0.030	N/A	ND	ND
Eucalyptol	0.006 / 0.018	N/A	ND	ND
Isoborneol	0.004 / 0.012	N/A	ND	ND
Citronellol	0.003 / 0.010	N/A	ND	ND
Terpinolene	0.008 / 0.026	N/A	ND	ND
β-Pinene	0.004 / 0.014	N/A	ND	ND
α-Pinene	0.005 / 0.017	N/A	ND	ND
β-Ocimene	0.006 / 0.020	N/A	ND	ND
Δ³-Carene	0.005 / 0.018	N/A	ND	ND
α-Cedrene	0.005 / 0.016	N/A	ND	ND
Geranyl Acetate	0.004 / 0.014	N/A	ND	ND
α-Bisabolol	0.008 / 0.026	N/A	ND	ND
α-Terpinene	0.005 / 0.017	N/A	ND	ND
γ-Terpinene	0.006 / 0.018	N/A	ND	ND
Sabinene Hydrate	0.006 / 0.022	N/A	ND	ND
α-Phellandrene	0.006 / 0.020	N/A	ND	ND
Caryophyllene Oxide	0.010 / 0.033	N/A	ND	ND
TOTAL			0.384 mg/g	0.0384%

Learn more

Pesticide Analysis

Pass

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Exclusions¹: See Notes section at bottom.

Exclusions²: See Notes section at bottom.

Pesticide Test Results

07/15/2024

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
Aldicarb	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Carbofuran	0.02 / 0.05	≥ LOD	N/A	ND	Pass
Chlordane*	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Chlorfenapyr*	0.03 / 0.10	≥ LOD	N/A	ND	Pass
Chlorpyrifos	0.02 / 0.06	≥ LOD	N/A	ND	Pass
Coumaphos	0.02 / 0.07	≥ LOD	N/A	ND	Pass
Daminozide	0.02 / 0.07	≥ LOD	N/A	ND	Pass
Dichlorvos (DDVP)	0.03 / 0.09	≥ LOD	N/A	ND	Pass
Dimethoate	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Ethoprophos	0.03 / 0.10	≥ LOD	N/A	ND	Pass
Etofenprox	0.02 / 0.06	≥ LOD	N/A	ND	Pass
Fenoxycarb	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Fipronil	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Imazalil	0.02 / 0.06	≥ LOD	N/A	ND	Pass
Methiocarb	0.02 / 0.07	≥ LOD	N/A	ND	Pass
Mevinphos	0.03 / 0.09	≥ LOD	N/A	ND	Pass
Paclobutrazol	0.02 / 0.05	≥ LOD	N/A	ND	Pass
Parathion-methyl	0.03 / 0.10	≥ LOD	N/A	ND	Pass
Propoxur	0.03 / 0.09	≥ LOD	N/A	ND	Pass
Spiroxamine	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Thiacloprid	0.03 / 0.10	≥ LOD	N/A	ND	Pass
Abamectin	0.03 / 0.10	0.3	N/A	ND	Pass
Acephate	0.02 / 0.07	5	N/A	ND	Pass
Acequinocyl	0.02 / 0.07	4	N/A	ND	Pass
Acetamiprid	0.02 / 0.05	5	N/A	ND	Pass
Azoxystrobin	0.02 / 0.07	40	N/A	ND	Pass
Bifenazate	0.01 / 0.04	5	N/A	ND	Pass
Bifenthrin	0.02 / 0.05	0.5	N/A	ND	Pass
Boscalid	0.03 / 0.09	10	N/A	ND	Pass
Captan	0.19 / 0.57	5	N/A	ND	Pass
Carbaryl	0.02 / 0.06	0.5	N/A	ND	Pass
Chlorantraniliprole	0.04 / 0.12	40	N/A	ND	Pass
Clofentezine	0.03 / 0.09	0.5	N/A	ND	Pass
Cyfluthrin	0.12 / 0.38	1	N/A	ND	Pass
Cypermethrin	0.11 / 0.32	1	N/A	ND	Pass
Diazinon	0.02 / 0.05	0.2	N/A	ND	Pass
Dimethomorph	0.03 / 0.09	20	N/A	ND	Pass
Etoxazole	0.02 / 0.06	1.5	N/A	ND	Pass
Fenhexamid	0.03 / 0.09	10	N/A	ND	Pass
Fenpyroximate	0.02 / 0.06	2	N/A	ND	Pass
Flonicamid	0.03 / 0.10	2	N/A	ND	Pass
Fludioxonil	0.03 / 0.10	30	N/A	ND	Pass
Hexythiazox	0.02 / 0.07	2	N/A	ND	Pass
Imidacloprid	0.04 / 0.11	3	N/A	ND	Pass
Kresoxim-methyl	0.02 / 0.07	1	N/A	ND	Pass
Malathion	0.03 / 0.09	5	N/A	ND	Pass
Metalaxyl	0.02 / 0.07	15	N/A	ND	Pass
Methomyl	0.03 / 0.10	0.1	N/A	ND	Pass
Myclobutanil	0.03 / 0.09	9	N/A	ND	Pass
Naled	0.02 / 0.07	0.5	N/A	ND	Pass
Oxamyl	0.04 / 0.11	0.2	N/A	ND	Pass
Pentachloronitrobenzene (Quintozene)*	0.03 / 0.09	0.2	N/A	ND	Pass
Permethrin	0.04 / 0.12	20	N/A	ND	Pass
Phosmet	0.03 / 0.10	0.2	N/A	ND	Pass
Piperonyl Butoxide	0.02 / 0.07	8	N/A	ND	Pass
Prallethrin	0.03 / 0.08	0.4	N/A	ND	Pass
Propiconazole	0.02 / 0.07	20	N/A	ND	Pass
Pyrethrins	0.04 / 0.12	1	N/A	ND	Pass
Pyridaben	0.02 / 0.07	3	N/A	ND	Pass
Spinetoram	0.02 / 0.07	3	N/A	ND	Pass
Spinosad	0.02 / 0.07	3	N/A	ND	Pass
Spiromesifen	0.02 / 0.05	12	N/A	ND	Pass
Spirotetramat	0.02 / 0.06	13	N/A	ND	Pass
Tebuconazole	0.02 / 0.07	2	N/A	ND	Pass
Thiamethoxam	0.03 / 0.10	4.5	N/A	ND	Pass
Trifloxystrobin	0.03 / 0.08	30	N/A	ND	Pass

Heavy Metals Analysis

Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

07/13/2024

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
Arsenic	0.02 / 0.1	1.5	N/A	ND	Pass
Cadmium	0.02 / 0.05	0.5	N/A	ND	Pass
Lead	0.04 / 0.1	0.5	N/A	ND	Pass
Mercury	0.002 / 0.01	1.5	N/A	ND	Pass

Notes

Exclusions:

1. QSP 1213 - Sample Certification: California Code of Regulation Title 4 Division 19

2. QSP 1212 - Sample Certification: California Code of Regulation Title 4 Division 19

COA ID: 240711K021-001

These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

Sample Certification: 6 CCR 1010-24 Colorado Hemp Product and Safe Harbor Hemp Product Regulations

Decision Rule: Statements of conformity (e.g. Pass/Fail) to specifications are made in this report without taking measurement uncertainty into account. Where statements of conformity are made in this report, the following decision rules are applied: PASS - Results within limits/specifications, FAIL - Results exceed limits/specifications.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT), μg/g = ppm, μg/kg = ppb