R&R 60mg Full Spectrum Softgels

Certificate of Analysis

HEMP QUALITY ASSURANCE TEST

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Sample Name:

R&R 60mg Full Spectrum Softgels

Infused, Colorado Infused

Total THC 1.469 mg/unit

Total CBD 60.322 mg/unit

Sum Cannabinoids 66.105 mg/unit

Total Cannabinoids 66.019 mg/unit

Total Terpenoids 0.0838%

Top 3 Terpenoids

α-Bisabolol 0.0424%
Guaiol 0.0261%
β-Caryophyllene 0.0102%

Sample Information

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Sample Details

Sample ID:230411M021

Batch Number:Lot 0870

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Cannabinoid Analysis - Summary

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Total THC: 1.469 mg/unit

Total CBD: 60.322 mg/unit

Sum of Cannabinoids: 66.105 mg/unit

Total Cannabinoids: 66.019 mg/unit

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ⁹-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ⁹-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ⁸-THC + CBL + CBN

Total Cannabinoids = (Δ⁹-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ⁸-THC + CBL + CBN

Why are Sum of Cannabinoids and Total Cannabinoids calculated separately?

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

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Total Terpenoids: 0.0838%

α-Bisabolol (0.0424%)

Guaiol (0.0261%)

β-Caryophyllene (0.0102%)

Safety Analysis - Summary

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Pesticides: ND

Mycotoxins: Pass

Residual Solvents: ND

Heavy Metals: Pass

Microbiology (PCR): Pass

Microbiology (Plating): Pass

View Complete Test Results:

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Cannabinoid Analysis

Tested

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 1.469 mg/unit

(Δ⁹-THC+0.877*THCa)

Total CBD: 60.322 mg/unit

(CBD+0.877*CBDa)

Total Cannabinoids: 66.019 mg/unit

Total CBG: 1.006 mg/unit

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 1.735 mg/unit

Total CBC (CBC+0.877*CBCa)

Total CBDV: 0.546 mg/unit

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

04/16/2023

Result Views

Table Pie Chart

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Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
Cannabidiol (CBD)	0.004 / 0.011	±3.1824	85.320	8.5320
Cannabichromene (CBC)	0.003 / 0.010	±0.0789	2.450	0.2450
Δ9 Tetrahydrocannabinol (Δ9THC)	0.002 / 0.014	±0.1152	2.098	0.2098
Cannabigerol (CBG)	0.002 / 0.006	±0.0697	1.437	0.1437
Cannabinol (CBN)	0.001 / 0.007	±0.0336	1.172	0.1172
Cannabidiolic Acid (CBDa)	0.001 / 0.026	±0.0277	0.974	0.0974
Cannabidivarin (CBDV)	0.002 / 0.012	±0.0318	0.780	0.0780
Cannabicyclol (CBL)	0.003 / 0.010	±0.0064	0.173	0.0173
Cannabichromenic Acid (CBCa)	0.001 / 0.015	±0.0012	0.032	0.0032
Cannabigerolic Acid (CBGa)	0.002 / 0.007	N/A	ND	ND
Tetrahydrocannabivarin (THCV)	0.002 / 0.012	N/A	ND	ND
Tetrahydrocannabinolic Acid (THCa)	0.001 / 0.005	N/A	ND	ND
Cannabidivarinic Acid (CBDVa)	0.001 / 0.018	N/A	ND	ND
Tetrahydrocannabivarinic Acid (THCVa)	0.002 / 0.019	N/A	ND	ND
∆8 Tetrahydrocannabinol (Δ8THC)	0.01 / 0.02	N/A	ND	ND
Total THC		±0.1211	2.098 mg/g	0.2098%
SUM OF CANNABINOIDS			94.436 mg/g	9.4436%

Unit Mass:

0.7 grams

Serving Size:

0.7 grams

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Δ⁹-THC per Unit		1.469 mg/unit
Δ⁹-THC per Serving		1.469 mg/serving
Total THC per Unit		1.469 mg/unit
Total THC Per Serving		1.469 mg/serving
CBD per Unit		59.724 mg/unit
CBD per Serving		59.724 mg/serving
Total CBD per Unit		60.322 mg/unit
Total CBD per Serving		60.322 mg/serving
Sum of Cannabinoids per Unit		66.105 mg/unit
Sum of Cannabinoids per Serving		66.105 mg/serving
Total Cannabinoids per Unit		66.019 mg/unit
Total Cannabinoids per Serving		66.019 mg/serving

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpenoid Analysis

Tested

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

Summary

Total Terpenoids (mg/g): 0.838 mg/g

Total Terpenoids (%): 0.0838%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume.

α-Bisabolol 0.0424%
A sesquiterpene alcohol with a fragrance that can be described as floral, peppery, sweet and clean. Found in chamomile, figwort, yarrow, skullcaps, lavender, ironwort, germander...etc.

Guaiol 0.0261%
A sesquiterpene alcohol with a fragrance that can be described as floral, piney, herbal and woody. Found in guaiacum, cypress pine, ginseng, melaleuca, goatweed, incense grass...etc.

β-Caryophyllene 0.0102%
A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB² receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

04/16/2023

Result Views

Table Bar Graph

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Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
α-Bisabolol	0.008 / 0.026	±0.0176	0.424	0.0424
Guaiol	0.009 / 0.030	±0.0096	0.261	0.0261
β-Caryophyllene	0.004 / 0.012	±0.0028	0.102	0.0102
α-Humulene	0.009 / 0.029	±0.0013	0.051	0.0051
Nerolidol	0.006 / 0.019	N/A	<LOQ	<LOQ
Nerol	0.003 / 0.011	N/A	ND	ND
Cedrol	0.008 / 0.027	N/A	ND	ND
Borneol	0.005 / 0.016	N/A	ND	ND
Camphor	0.006 / 0.019	N/A	ND	ND
Fenchol	0.010 / 0.034	N/A	ND	ND
Menthol	0.008 / 0.025	N/A	ND	ND
Myrcene	0.008 / 0.025	N/A	ND	ND
Camphene	0.005 / 0.015	N/A	ND	ND
Fenchone	0.009 / 0.028	N/A	ND	ND
Geraniol	0.002 / 0.007	N/A	ND	ND
Limonene	0.005 / 0.016	N/A	ND	ND
Linalool	0.009 / 0.032	N/A	ND	ND
Pulegone	0.003 / 0.011	N/A	ND	ND
Sabinene	0.004 / 0.014	N/A	ND	ND
p-Cymene	0.005 / 0.016	N/A	ND	ND
Terpineol	0.009 / 0.031	N/A	ND	ND
Valencene	0.009 / 0.030	N/A	ND	ND
Eucalyptol	0.006 / 0.018	N/A	ND	ND
Isoborneol	0.004 / 0.012	N/A	ND	ND
Isopulegol	0.005 / 0.016	N/A	ND	ND
Citronellol	0.003 / 0.010	N/A	ND	ND
Terpinolene	0.008 / 0.026	N/A	ND	ND
β-Pinene	0.004 / 0.014	N/A	ND	ND
α-Pinene	0.005 / 0.017	N/A	ND	ND
β-Ocimene	0.006 / 0.020	N/A	ND	ND
Δ³-Carene	0.005 / 0.018	N/A	ND	ND
α-Cedrene	0.005 / 0.016	N/A	ND	ND
Geranyl Acetate	0.004 / 0.014	N/A	ND	ND
α-Terpinene	0.005 / 0.017	N/A	ND	ND
γ-Terpinene	0.006 / 0.018	N/A	ND	ND
Sabinene Hydrate	0.006 / 0.022	N/A	ND	ND
α-Phellandrene	0.006 / 0.020	N/A	ND	ND
Caryophyllene Oxide	0.010 / 0.033	N/A	ND	ND
trans-β-Farnesene	0.008 / 0.025	N/A	ND	ND
TOTAL			0.838 mg/g	0.0838%

Learn more

Pesticide Analysis

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

04/13/2023

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Compound	LOD/LOQ (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)
Abamectin	0.032 / 0.097	N/A	ND
Acephate	0.006 / 0.018	N/A	ND
Acequinocyl	0.009 / 0.027	N/A	ND
Acetamiprid	0.016 / 0.049	N/A	ND
Aldicarb	0.030 / 0.090	N/A	ND
Allethrin	0.030 / 0.092	N/A	ND
Atrazine	0.006 / 0.019	N/A	ND
Azadirachtin	0.082 / 0.248	N/A	ND
Azoxystrobin	0.003 / 0.009	N/A	ND
Benzovindiflupyr	0.003 / 0.009	N/A	ND
Bifenazate	0.003 / 0.009	N/A	ND
Bifenthrin	0.021 / 0.064	N/A	ND
Boscalid	0.003 / 0.009	N/A	ND
Buprofezin^‡	0.006 / 0.019	N/A	ND
Carbaryl	0.007 / 0.020	N/A	ND
Carbofuran	0.003 / 0.008	N/A	ND
Chlorantraniliprole	0.006 / 0.018	N/A	ND
Chlorfenapyr*	0.005 / 0.015	N/A	ND
Chlorpyrifos	0.013 / 0.039	N/A	ND
Clofentezine	0.003 / 0.009	N/A	ND
Clothianidin	0.008 / 0.025	N/A	ND
Coumaphos	0.003 / 0.010	N/A	ND
Cyantraniliprole	0.003 / 0.010	N/A	ND
Cyfluthrin	0.052 / 0.159	N/A	ND
Cypermethrin	0.051 / 0.153	N/A	ND
Cyprodinil^‡	0.003 / 0.008	N/A	ND
Daminozide	0.026 / 0.077	N/A	ND
Deltamethrin	0.059 / 0.180	N/A	ND
Diazinon	0.006 / 0.017	N/A	ND
Dichlorvos (DDVP)	0.012 / 0.038	N/A	ND
Dimethoate	0.003 / 0.009	N/A	ND
Dimethomorph	0.016 / 0.050	N/A	ND
Dinotefuran	0.010 / 0.030	N/A	ND
Diuron	0.013 / 0.040	N/A	ND
Dodemorph	0.012 / 0.035	N/A	ND
Endosulfan sulfate^†^‡	0.016 / 0.048	N/A	ND
Endosulfan-α*^†^‡	0.004 / 0.014	N/A	ND
Endosulfan-β*^†^‡	0.006 / 0.019	N/A	ND
Ethoprophos	0.003 / 0.009	N/A	ND
Etofenprox	0.014 / 0.042	N/A	ND
Etoxazole	0.007 / 0.020	N/A	ND
Etridiazole*	0.002 / 0.005	N/A	ND
Fenhexamid	0.003 / 0.008	N/A	ND
Fenoxycarb	0.003 / 0.010	N/A	ND
Fenpyroximate	0.007 / 0.020	N/A	ND
Fensulfothion	0.003 / 0.010	N/A	ND
Fenthion	0.003 / 0.010	N/A	ND
Fenvalerate^‡	0.033 / 0.099	N/A	ND
Fipronil	0.003 / 0.010	N/A	ND
Flonicamid	0.007 / 0.022	N/A	ND
Fludioxonil	0.003 / 0.010	N/A	ND
Fluopyram^‡	0.003 / 0.009	N/A	ND
Hexythiazox	0.003 / 0.010	N/A	ND
Imazalil	0.003 / 0.009	N/A	ND
Imidacloprid	0.003 / 0.010	N/A	ND
Iprodione	0.077 / 0.233	N/A	ND
Kinoprene	0.077 / 0.233	N/A	ND
Kresoxim-methyl	0.006 / 0.019	N/A	ND
λ-Cyhalothrin	0.068 / 0.206	N/A	ND
Malathion	0.003 / 0.009	N/A	ND
Metalaxyl	0.003 / 0.010	N/A	ND
Methiocarb	0.003 / 0.008	N/A	ND
Methomyl	0.008 / 0.025	N/A	ND
Methoprene	0.172 / 0.521	N/A	ND
Mevinphos	0.008 / 0.024	N/A	ND
MGK-264	0.015 / 0.047	N/A	ND
Myclobutanil	0.003 / 0.009	N/A	ND
Naled	0.021 / 0.064	N/A	ND
Novaluron	0.002 / 0.005	N/A	ND
Oxamyl	0.017 / 0.051	N/A	ND
Paclobutrazol	0.003 / 0.010	N/A	ND
Parathion-methyl	0.016 / 0.050	N/A	ND
Pentachloronitrobenzene (Quintozene)*	0.004 / 0.012	N/A	ND
Permethrin	0.056 / 0.168	N/A	ND
Phenothrin	0.016 / 0.047	N/A	ND
Phosmet	0.007 / 0.020	N/A	ND
Piperonyl Butoxide	0.010 / 0.029	N/A	ND
Pirimicarb	0.003 / 0.009	N/A	ND
Prallethrin	0.015 / 0.046	N/A	ND
Propiconazole	0.027 / 0.080	N/A	ND
Propoxur	0.003 / 0.008	N/A	ND
Pyraclostrobin	0.003 / 0.010	N/A	ND
Pyrethrins	0.016 / 0.049	N/A	ND
Pyridaben	0.005 / 0.017	N/A	ND
Pyriproxyfen	0.003 / 0.009	N/A	ND
Resmethrin	0.013 / 0.039	N/A	ND
Spinetoram	0.003 / 0.010	N/A	ND
Spinosad	0.003 / 0.010	N/A	ND
Spirodiclofen	0.031 / 0.093	N/A	ND
Spiromesifen	0.016 / 0.050	N/A	ND
Spirotetramat	0.003 / 0.010	N/A	ND
Spiroxamine	0.020 / 0.062	N/A	ND
Tebuconazole	0.003 / 0.010	N/A	ND
Tebufenozide	0.003 / 0.008	N/A	ND
Teflubenzuron	0.007 / 0.022	N/A	ND
Tetrachlorvinphos	0.003 / 0.008	N/A	ND
Tetramethrin	0.021 / 0.063	N/A	ND
Thiabendazole	0.006 / 0.020	N/A	ND
Thiacloprid	0.003 / 0.009	N/A	ND
Thiamethoxam	0.003 / 0.010	N/A	ND
Thiophanate-methyl	0.013 / 0.040	N/A	ND
Trifloxystrobin	0.003 / 0.009	N/A	ND

Mycotoxin Analysis

Pass

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS

Mycotoxin Test Results

04/13/2023

PASS

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Compound	LOD/LOQ (μg/kg)	Action Limit (μg/kg)	Measurement Uncertainty (μg/kg)	Result (μg/kg)	Result
Aflatoxin B1	1.6 / 5.0	5	N/A	ND	Pass
Aflatoxin B2	1.4 / 4.1		N/A	ND
Aflatoxin G1	1.6 / 4.9		N/A	ND
Aflatoxin G2	1.6 / 5.0		N/A	ND
Ochratoxin A	1.6 / 5.0	5	N/A	ND	Pass
Total Aflatoxin		20	±	ND	Pass

Residual Solvents Analysis

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

04/18/2023

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Compound	LOD/LOQ (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)
Propane	0.234 / 0.781	N/A	ND
2-Methylpropane (Isobutane)	0.052 / 0.173	N/A	ND
n-Butane	0.019 / 0.063	N/A	ND
Total Butanes		±	ND
n-Pentane	0.310 / 1.033	N/A	ND
n-Hexane	0.110 / 0.366	N/A	ND
2,2-Dimethylpentane (Neoheptane)	0.493 / 1.642	N/A	ND
2,3-Dimethylpentane	1.009 / 3.365	N/A	ND
2,4-Dimethylpentane	0.737 / 2.458	N/A	ND
3,3-Dimethylpentane	0.198 / 0.660	N/A	ND
2,2,3-Trimethylbutane (Triptane)	0.521 / 1.738	N/A	ND
2-Methylhexane (Isoheptane)	0.610 / 2.034	N/A	ND
3-Methylhexane	0.235 / 0.785	N/A	ND
3-Ethylpentane	0.304 / 1.012	N/A	ND
n-Heptane	13.12 / 43.72	N/A	ND
Total Heptanes		±	ND
Benzene	0.089 / 0.295	N/A	ND
Toluene	0.115 / 0.382	N/A	ND
1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene)	0.451 / 1.502	N/A	ND
1,2-Dimethylbenzene (o-Xylene)	0.387 / 1.289	N/A	ND
Total Xylenes		±	ND
Methanol	53.92 / 163.4	N/A	ND
Ethanol	8.984 / 27.23	N/A	ND
2-Propanol (Isopropyl Alcohol)	8.421 / 25.52	N/A	ND
Acetone	10.59 / 32.08	N/A	ND
Ethyl Acetate	1.123 / 3.745	N/A	ND

Total Butanes = n-Butane + 2-Methylpropane (Isobutane)

Total Heptanes = 2,2-Dimethylpentane (Neoheptane) + 2,3-Dimethylpentane + 2,4-Dimethylpentane + 3,3-Dimethylpentane + 2,2,3-Trimethylbutane (Triptane) + 2-Methylhexane (Isoheptane) + 3-Methylhexane + 3-Ethylpentane + n-Heptane

Total Xylenes = 1,2-Dimethylbenzene (o-Xylene) + 1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene)

Heavy Metals Analysis

Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

04/14/2023

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
Arsenic	0.02 / 0.1	1.5	N/A	ND	Pass
Cadmium	0.02 / 0.05	0.5	N/A	ND	Pass
Lead	0.04 / 0.1	0.5	N/A	ND	Pass
Mercury	0.002 / 0.01	1.5	N/A	ND	Pass

Microbiology Analysis

Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants. And Analysis conducted by 3M^TM Petrifilm^TM and plate counts of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants and QSP 6794 - Plating with 3M^TM Petrifilm^TM

Microbiology Test Results (PCR)

04/17/2023

PASS

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Compound	Action Limit	Result	Result
Salmonella spp.	Not Detected in 25g	ND	Pass
Shiga toxin-producing Escherichia coli	Not Detected in 25g	ND	Pass

Microbiology Test Results (PLATING)

04/17/2023

PASS

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Compound	Action Limit (cfu/g)	Result (cfu/g)	Result
Coliforms	100	ND	Pass
Total Yeast and Mold	1000	ND	Pass
Total Aerobic Bacteria	10000	ND	Pass

COA ID: 230411M021-003

These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

Sample Certification: 6 CCR 1010-24 Colorado Hemp Product and Safe Harbor Hemp Product Regulations

Decision Rule: Statements of conformity (e.g. Pass/Fail) to specifications are made in this report without taking measurement uncertainty into account. Where statements of conformity are made in this report, the following decision rules are applied: PASS - Results within limits/specifications, FAIL - Results exceed limits/specifications.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT), μg/g = ppm, μg/kg = ppb, too numerous to count >250 cfu/plate (TNTC), colony-forming unit (cfu)