Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

R&R 30mg THC-Free Broad-Spectrum CBD Softgels

Pill/Capsule, Colorado Concentrate/Extract

Date Issued:

05/03/2024

Serving Size:

0.6678 grams

Total THC Not Detected
Total CBD 30.858 mg/unit
Sum Cannabinoids 33.134 mg/unit
Total Cannabinoids 33.103 mg/unit
Total Terpenoids 0.0289%
Top 3 Terpenoids
  1. α-Bisabolol 0.0210%
  2. Guaiol 0.0079%

Sample Information

Sample Details

Sample ID:240418M032

Batch Number:Lot 9005B

Cultivator / Manufacturer

Show Details

Distributor / Tested For

Show Details

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Cannabinoid Analysis - Summary

Total THC: Not Detected

Total CBD: 30.858 mg/unit

Sum of Cannabinoids: 33.134 mg/unit

Total Cannabinoids: 33.103 mg/unit

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

Total Terpenoids: 0.0289%

 
 

1

α-Bisabolol (0.0210%)

2

Guaiol (0.0079%)

Safety Analysis - Summary

Pesticides: Pass

Mycotoxins: Pass

Residual Solvents: ND

Heavy Metals: Pass

Microbiology (PCR): Pass

Microbiology (Plating): Pass

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: Not Detected

(Δ9-THC+0.877*THCa)

Total CBD: 30.858 mg/unit

(CBD+0.877*CBDa)

Total Cannabinoids: 33.103 mg/unit

Total CBG: 0.512 mg/unit

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 0.769 mg/unit

Total CBC (CBC+0.877*CBCa)

Total CBDV: 0.254 mg/unit

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

04/25/2024

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
Cannabidiol (CBD) 0.004 / 0.011 ±1.7115 45.884 4.5884
Cannabichromene (CBC) 0.003 / 0.010 ±0.0371 1.152 0.1152
Cannabinol (CBN) 0.001 / 0.007 ±0.0284 0.988 0.0988
Cannabigerol (CBG) 0.002 / 0.006 ±0.0372 0.766 0.0766
Cannabidivarin (CBDV) 0.002 / 0.012 ±0.0155 0.381 0.0381
Cannabidiolic Acid (CBDa) 0.001 / 0.026 ±0.0105 0.371 0.0371
Cannabicyclol (CBL) 0.003 / 0.010 ±0.0027 0.074 0.0074
Cannabichromenic Acid (CBCa) 0.001 / 0.015 N/A <LOQ <LOQ
Cannabigerolic Acid (CBGa) 0.002 / 0.007 N/A ND ND
Tetrahydrocannabivarin (THCV) 0.002 / 0.012 N/A ND ND
Tetrahydrocannabinolic Acid (THCa) 0.001 / 0.005 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.001 / 0.018 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.002 / 0.019 N/A ND ND
∆8 Tetrahydrocannabinol (Δ8THC) 0.01 / 0.02 N/A ND ND
Δ9 Tetrahydrocannabinol (Δ9THC) 0.002 / 0.014 N/A ND ND
Total THC N/A ND ND
SUM OF CANNABINOIDS 49.616 mg/g 4.9616%
Unit Mass:

0.6678 grams

/

Serving Size:

0.6678 grams

Swipe left on table to see additional columns

Δ9-THC per Unit ND
Δ9-THC per Serving ND
Total THC per Unit ND
Total THC Per Serving ND
CBD per Unit 30.641 mg/unit
CBD per Serving 30.641 mg/serving
Total CBD per Unit 30.858 mg/unit
Total CBD per Serving 30.858 mg/serving
Sum of Cannabinoids per Unit 33.134 mg/unit
Sum of Cannabinoids per Serving 33.134 mg/serving
Total Cannabinoids per Unit 33.103 mg/unit
Total Cannabinoids per Serving 33.103 mg/serving
Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

Summary

Total Terpenoids (mg/g): 0.289 mg/g

Total Terpenoids (%): 0.0289%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume.

  1. α-Bisabolol 0.0210%

    A sesquiterpene alcohol with a fragrance that can be described as floral, peppery, sweet and clean. Found in chamomile, figwort, yarrow, skullcaps, lavender, ironwort, germander...etc.

  2. Guaiol 0.0079%

    A sesquiterpene alcohol with a fragrance that can be described as floral, piney, herbal and woody. Found in guaiacum, cypress pine, ginseng, melaleuca, goatweed, incense grass...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

04/21/2024

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
α-Bisabolol 0.008 / 0.026 ±0.0087 0.210 0.0210
Guaiol 0.009 / 0.030 ±0.0029 0.079 0.0079
Nerol 0.003 / 0.011 N/A ND ND
Cedrol 0.008 / 0.027 N/A ND ND
Borneol 0.005 / 0.016 N/A ND ND
Camphor 0.006 / 0.019 N/A ND ND
Fenchol 0.010 / 0.034 N/A ND ND
Menthol 0.008 / 0.025 N/A ND ND
Myrcene 0.008 / 0.025 N/A ND ND
Camphene 0.005 / 0.015 N/A ND ND
Fenchone 0.009 / 0.028 N/A ND ND
Geraniol 0.002 / 0.007 N/A ND ND
Limonene 0.005 / 0.016 N/A ND ND
Linalool 0.009 / 0.032 N/A ND ND
Pulegone 0.003 / 0.011 N/A ND ND
Sabinene 0.004 / 0.014 N/A ND ND
p-Cymene 0.005 / 0.016 N/A ND ND
Nerolidol 0.006 / 0.019 N/A ND ND
Terpineol 0.009 / 0.031 N/A ND ND
Valencene 0.009 / 0.030 N/A ND ND
Eucalyptol 0.006 / 0.018 N/A ND ND
Isoborneol 0.004 / 0.012 N/A ND ND
Isopulegol 0.005 / 0.016 N/A ND ND
Citronellol 0.003 / 0.010 N/A ND ND
Terpinolene 0.008 / 0.026 N/A ND ND
β-Pinene 0.004 / 0.014 N/A ND ND
α-Pinene 0.005 / 0.017 N/A ND ND
β-Ocimene 0.006 / 0.020 N/A ND ND
Δ3-Carene 0.005 / 0.018 N/A ND ND
α-Cedrene 0.005 / 0.016 N/A ND ND
α-Humulene 0.009 / 0.029 N/A ND ND
Geranyl Acetate 0.004 / 0.014 N/A ND ND
α-Terpinene 0.005 / 0.017 N/A ND ND
γ-Terpinene 0.006 / 0.018 N/A ND ND
Sabinene Hydrate 0.006 / 0.022 N/A ND ND
α-Phellandrene 0.006 / 0.020 N/A ND ND
β-Caryophyllene 0.004 / 0.012 N/A ND ND
Caryophyllene Oxide 0.010 / 0.033 N/A ND ND
trans-β-Farnesene 0.008 / 0.025 N/A ND ND
TOTAL 0.289 mg/g 0.0289%
Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

04/22/2024

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Abamectin 0.032 / 0.097 0.25 N/A ND Pass
Acephate 0.006 / 0.018 0.05 N/A ND Pass
Acequinocyl 0.009 / 0.027 ≥ LOQ N/A ND Pass
Acetamiprid 0.016 / 0.049 0.05 N/A ND Pass
Aldicarb 0.030 / 0.090 0.5 N/A ND Pass
Allethrin 0.030 / 0.092 0.1 N/A ND Pass
Atrazine 0.006 / 0.019 ≥ LOQ N/A ND Pass
Azadirachtin 0.082 / 0.248 0.5 N/A ND Pass
Azoxystrobin 0.003 / 0.009 0.01 N/A ND Pass
Benzovindiflupyr 0.003 / 0.009 0.01 N/A ND Pass
Bifenazate 0.003 / 0.009 0.01 N/A ND Pass
Bifenthrin 0.021 / 0.064 ≥ LOQ N/A ND Pass
Boscalid 0.003 / 0.009 0.01 N/A ND Pass
Buprofezin‡ 0.006 / 0.019 ≥ LOQ N/A ND Pass
Carbaryl 0.007 / 0.020 0.025 N/A ND Pass
Carbofuran 0.003 / 0.008 0.01 N/A ND Pass
Chlorantraniliprole 0.006 / 0.018 ≥ LOQ N/A ND Pass
Chlorfenapyr* 0.005 / 0.015 N/A ND
Chlorpyrifos 0.013 / 0.039 0.5 N/A ND Pass
cis-Permethrin ± 0.00
Clofentezine 0.003 / 0.009 0.01 N/A ND Pass
Clothianidin 0.008 / 0.025 0.025 N/A ND Pass
Coumaphos 0.003 / 0.010 0.01 N/A ND Pass
Cyantraniliprole 0.003 / 0.010 0.01 N/A ND Pass
Cyfluthrin 0.052 / 0.159 ≥ LOQ N/A ND Pass
Cypermethrin 0.051 / 0.153 ≥ LOQ N/A ND Pass
Cyprodinil‡ 0.003 / 0.008 0.01 N/A ND Pass
Daminozide 0.026 / 0.077 ≥ LOQ N/A ND Pass
Deltamethrin 0.059 / 0.180 ≥ LOQ N/A ND Pass
Diazinon 0.006 / 0.017 ≥ LOQ N/A ND Pass
Dichlorvos (DDVP) 0.012 / 0.038 0.05 N/A ND Pass
Dimethoate 0.003 / 0.009 0.01 N/A ND Pass
Dimethomorph 0.016 / 0.050 ≥ LOQ N/A ND Pass
Dinotefuran 0.010 / 0.030 0.05 N/A ND Pass
Diuron 0.013 / 0.040 ≥ LOQ N/A ND Pass
Dodemorph 0.012 / 0.035 ≥ LOQ N/A ND Pass
Endosulfan sulfate†‡ 0.016 / 0.048 2.5 N/A ND Pass
Endosulfan-α*†‡ 0.004 / 0.014 N/A ND
Endosulfan-β*†‡ 0.006 / 0.019 N/A ND
Ethoprophos 0.003 / 0.009 0.01 N/A ND Pass
Etofenprox 0.014 / 0.042 ≥ LOQ N/A ND Pass
Etoxazole 0.007 / 0.020 ≥ LOQ N/A ND Pass
Etridiazole* 0.002 / 0.005 N/A ND
Fenhexamid 0.003 / 0.008 ≥ LOQ N/A ND Pass
Fenoxycarb 0.003 / 0.010 0.01 N/A ND Pass
Fenpyroximate 0.007 / 0.020 ≥ LOQ N/A ND Pass
Fensulfothion 0.003 / 0.010 0.01 N/A ND Pass
Fenthion 0.003 / 0.010 0.01 N/A ND Pass
Fenvalerate‡ 0.033 / 0.099 ≥ LOQ N/A ND Pass
Fipronil 0.003 / 0.010 0.01 N/A ND Pass
Flonicamid 0.007 / 0.022 0.025 N/A ND Pass
Fludioxonil 0.003 / 0.010 0.01 N/A ND Pass
Fluopyram‡ 0.003 / 0.009 0.01 N/A ND Pass
Hexythiazox 0.003 / 0.010 ≥ LOQ N/A ND Pass
Imazalil 0.003 / 0.009 0.01 N/A ND Pass
Imidacloprid 0.003 / 0.010 0.01 N/A ND Pass
Iprodione 0.077 / 0.233 0.5 N/A ND Pass
Kinoprene 0.077 / 0.233 1.25 N/A ND Pass
Kresoxim-methyl 0.006 / 0.019 0.15 N/A ND Pass
λ-Cyhalothrin 0.068 / 0.206 ≥ LOQ N/A ND Pass
Malathion 0.003 / 0.009 0.01 N/A ND Pass
Metalaxyl 0.003 / 0.010 0.01 N/A <LOQ Pass
Methiocarb 0.003 / 0.008 0.01 N/A ND Pass
Methomyl 0.008 / 0.025 0.025 N/A ND Pass
Methoprene 0.172 / 0.521 ≥ LOQ N/A ND Pass
Mevinphos 0.008 / 0.024 0.025 N/A ND Pass
MGK-264 0.015 / 0.047 ≥ LOQ N/A ND Pass
Myclobutanil 0.003 / 0.009 0.01 N/A ND Pass
Naled 0.021 / 0.064 ≥ LOQ N/A ND Pass
Novaluron 0.002 / 0.005 0.025 N/A ND Pass
Oxamyl 0.017 / 0.051 1.5 N/A ND Pass
Paclobutrazol 0.003 / 0.010 0.01 N/A ND Pass
Parathion-methyl 0.016 / 0.050 ≥ LOQ N/A ND Pass
Pentachloronitrobenzene (Quintozene)* 0.004 / 0.012 N/A ND
Permethrin 0.056 / 0.168 ≥ LOQ N/A ND Pass
Phenothrin 0.016 / 0.047 ≥ LOQ N/A ND Pass
Phosmet 0.007 / 0.020 ≥ LOQ N/A ND Pass
Piperonyl Butoxide 0.010 / 0.029 1.25 N/A ND Pass
Pirimicarb 0.003 / 0.009 0.01 N/A ND Pass
Prallethrin 0.015 / 0.046 ≥ LOQ N/A ND Pass
Propiconazole 0.027 / 0.080 ≥ LOQ N/A ND Pass
Propoxur 0.003 / 0.008 0.01 N/A ND Pass
Pyraclostrobin 0.003 / 0.010 0.01 N/A ND Pass
Pyrethrins 0.016 / 0.049 ≥ LOQ N/A ND Pass
Pyridaben 0.005 / 0.017 0.02 N/A ND Pass
Pyriproxyfen 0.003 / 0.009 ≥ LOQ N/A ND Pass
Resmethrin 0.013 / 0.039 0.05 N/A ND Pass
Spinetoram 0.003 / 0.010 0.01 N/A ND Pass
Spinosad 0.003 / 0.010 0.01 N/A ND Pass
Spirodiclofen 0.031 / 0.093 ≥ LOQ N/A ND Pass
Spiromesifen 0.016 / 0.050 ≥ LOQ N/A ND Pass
Spirotetramat 0.003 / 0.010 0.01 N/A ND Pass
Spiroxamine 0.020 / 0.062 ≥ LOQ N/A ND Pass
Tebuconazole 0.003 / 0.010 0.01 N/A ND Pass
Tebufenozide 0.003 / 0.008 0.01 N/A ND Pass
Teflubenzuron 0.007 / 0.022 0.025 N/A ND Pass
Tetrachlorvinphos 0.003 / 0.008 0.01 N/A ND Pass
Tetramethrin 0.021 / 0.063 ≥ LOQ N/A ND Pass
Thiabendazole 0.006 / 0.020 ≥ LOQ N/A ND Pass
Thiacloprid 0.003 / 0.009 0.01 N/A ND Pass
Thiamethoxam 0.003 / 0.010 0.01 N/A ND Pass
Thiophanate-methyl 0.013 / 0.040 ≥ LOQ N/A ND Pass
trans-Permethrin ± 0.00
Trifloxystrobin 0.003 / 0.009 0.01 N/A ND Pass

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS

Mycotoxin Test Results

04/22/2024

PASS

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Compound LOD/LOQ
(μg/kg)
Action Limit
(μg/kg)
Measurement
Uncertainty
(μg/kg)
Result
(μg/kg)
Result
Aflatoxin B1 1.6 / 5.0 5 N/A ND Pass
Aflatoxin B2 1.4 / 4.1 N/A ND
Aflatoxin G1 1.6 / 4.9 N/A ND
Aflatoxin G2 1.6 / 5.0 N/A ND
Ochratoxin A 1.6 / 5.0 5 N/A ND Pass
Total Aflatoxin 20 ± ND Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

04/22/2024

ND

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Compound LOD/LOQ
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Propane 0.234 / 0.781 N/A ND
2-Methylpropane (Isobutane) 0.052 / 0.173 N/A ND
n-Butane 0.019 / 0.063 N/A ND
Total Butanes ± ND
n-Pentane 0.310 / 1.033 N/A ND
n-Hexane 0.110 / 0.366 N/A ND
2,2-Dimethylpentane (Neoheptane) 0.493 / 1.642 N/A ND
2,3-Dimethylpentane 1.009 / 3.365 N/A ND
2,4-Dimethylpentane 0.737 / 2.458 N/A ND
3,3-Dimethylpentane 0.198 / 0.660 N/A ND
2,2,3-Trimethylbutane (Triptane) 0.521 / 1.738 N/A ND
2-Methylhexane (Isoheptane) 0.610 / 2.034 N/A ND
3-Methylhexane 0.235 / 0.785 N/A ND
3-Ethylpentane 0.304 / 1.012 N/A ND
n-Heptane 13.12 / 43.72 N/A ND
Total Heptanes ± ND
Benzene 0.089 / 0.295 N/A ND
Toluene 0.115 / 0.382 N/A ND
1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene) 0.451 / 1.502 N/A ND
1,2-Dimethylbenzene (o-Xylene) 0.387 / 1.289 N/A ND
Total Xylenes ± ND
Methanol 53.92 / 163.4 N/A ND
Ethanol 8.984 / 27.23 N/A ND
2-Propanol (Isopropyl Alcohol) 8.421 / 25.52 N/A ND
Acetone 10.59 / 32.08 N/A ND
Ethyl Acetate 1.123 / 3.745 N/A ND

Total Butanes = n-Butane + 2-Methylpropane (Isobutane)

Total Heptanes = 2,2-Dimethylpentane (Neoheptane) + 2,3-Dimethylpentane + 2,4-Dimethylpentane + 3,3-Dimethylpentane + 2,2,3-Trimethylbutane (Triptane) + 2-Methylhexane (Isoheptane) + 3-Methylhexane + 3-Ethylpentane + n-Heptane

Total Xylenes = 1,2-Dimethylbenzene (o-Xylene) + 1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene)

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

04/22/2024

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Arsenic 0.02 / 0.1 1.5 N/A ND Pass
Cadmium 0.02 / 0.05 0.5 N/A ND Pass
Lead 0.04 / 0.1 0.5 N/A ND Pass
Mercury 0.002 / 0.01 1.5 N/A ND Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants. And Analysis conducted by 3MTM PetrifilmTM and plate counts of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants and QSP 6794 - Plating with 3MTM PetrifilmTM

Microbiology Test Results (PCR)

04/22/2024

PASS

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Compound Action Limit Result Result
Salmonella spp. Not Detected in 25g ND Pass
Shiga toxin-producing Escherichia coli Not Detected in 25g ND Pass
Microbiology Test Results (PLATING)

04/22/2024

PASS

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Compound Action Limit
(cfu/g)
Result
(cfu/g)
Result
Coliforms 100 ND Pass
Total Yeast and Mold 1000 ND Pass
Total Aerobic Bacteria 10000 ND Pass

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