Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

Relief & Recovery Gel

Infused, Hemp

Date Issued:

08/30/2022

Serving Size:

1 milliliters

Total THC Not Detected
Total CBD 11.117 mg/mL
Sum Cannabinoids 11.135 mg/mL
Total Cannabinoids 11.135 mg/mL

Sample Information

Sample Details

Sample ID:220826U014

Batch Number:DN605

Cultivator / Manufacturer

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Distributor / Tested For

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Cannabinoid Analysis - Summary

Total THC: Not Detected

Total CBD: 11.117 mg/mL

Sum of Cannabinoids: 11.135 mg/mL

Total Cannabinoids: 11.135 mg/mL

Density:1.0791 g/mL

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Safety Analysis - Summary

Pesticides: ND

Residual Solvents: Detected

Heavy Metals: ND

Microbiology (PCR): ND

Microbiology (Plating): ND

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: Not Detected

9-THC+0.877*THCa)

Total CBD: 11.117 mg/mL

(CBD+0.877*CBDa)

Total Cannabinoids: 11.135 mg/mL

Total CBG: ND

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: ND

Total CBC (CBC+0.877*CBCa)

Total CBDV: 0.018 mg/mL

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

08/29/2022

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/mL)
Measurement
Uncertainty
(mg/mL)
Result
(mg/mL)
Result
(%)
Cannabidiol (CBD) 0.004 / 0.011 ±0.4147 11.117 1.0302
Cannabidivarin (CBDV) 0.002 / 0.012 ±0.0007 0.018 0.0017
Δ9 Tetrahydrocannabinol (Δ9THC) 0.002 / 0.014 N/A ND ND
∆8 Tetrahydrocannabinol (Δ8THC) 0.01 / 0.02 N/A ND ND
Tetrahydrocannabinolic Acid (THCa) 0.001 / 0.005 N/A ND ND
Tetrahydrocannabivarin (THCV) 0.002 / 0.012 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.002 / 0.019 N/A ND ND
Cannabidiolic Acid (CBDa) 0.001 / 0.026 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.001 / 0.018 N/A ND ND
Cannabigerol (CBG) 0.002 / 0.006 N/A ND ND
Cannabigerolic Acid (CBGa) 0.002 / 0.007 N/A ND ND
Cannabicyclol (CBL) 0.003 / 0.010 N/A ND ND
Cannabinol (CBN) 0.001 / 0.007 N/A ND ND
Cannabichromene (CBC) 0.003 / 0.010 N/A ND ND
Cannabichromenic Acid (CBCa) 0.001 / 0.015 N/A ND ND
SUM OF CANNABINOIDS 11.135 mg/mL 1.0319%
Serving Size:

1 milliliters

Swipe left on table to see additional columns

Δ9-THC per Serving ND
Total THC Per Serving ND
CBD per Serving 11.117 mg/serving
Total CBD per Serving 11.117 mg/serving
Sum of Cannabinoids per Serving 11.135 mg/serving
Total Cannabinoids per Serving 11.135 mg/serving
Density Test Result

1.0791 g/mL Tested 08/29/2022 Method: QSP 7870 - Sample Preparation

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

08/28/2022

ND

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Compound LOD/LOQ
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Abamectin 0.03 / 0.10 N/A ND
Azoxystrobin 0.02 / 0.07 N/A ND
Bifenazate 0.01 / 0.04 N/A ND
Bifenthrin 0.02 / 0.05 N/A ND
Boscalid 0.03 / 0.09 N/A ND
Chlorpyrifos 0.02 / 0.06 N/A ND
Cypermethrin 0.11 / 0.32 N/A ND
Etoxazole 0.02 / 0.06 N/A ND
Hexythiazox 0.02 / 0.07 N/A ND
Imidacloprid 0.04 / 0.11 N/A ND
Malathion 0.03 / 0.09 N/A ND
Myclobutanil 0.03 / 0.09 N/A ND
Permethrin 0.04 / 0.12 N/A ND
Piperonyl Butoxide 0.02 / 0.07 N/A ND
Propiconazole 0.02 / 0.07 N/A ND
Spiromesifen 0.02 / 0.05 N/A ND
Tebuconazole 0.02 / 0.07 N/A ND
Trifloxystrobin 0.03 / 0.08 N/A ND

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

08/27/2022

DETECTED

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Compound LOD/LOQ
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
1,2-Dichloroethane 0.05 / 0.1 N/A ND
Benzene 0.03 / 0.09 N/A <LOQ
Chloroform 0.1 / 0.2 N/A ND
Ethylene Oxide 0.3 / 0.8 N/A ND
Dichloromethane (Methylene Chloride) 0.3 / 0.9 N/A ND
Trichloroethylene 0.1 / 0.3 N/A ND
Acetone 20 / 50 N/A ND
Acetonitrile 2 / 7 N/A ND
n-Butane 10 / 50 N/A ND
Ethanol 20 / 50 N/A ND
Ethyl Acetate 20 / 60 N/A ND
Ethyl Ether 20 / 50 N/A ND
n-Heptane 20 / 60 N/A ND
n-Hexane 2 / 5 N/A ND
2-Propanol (Isopropyl Alcohol) 10 / 40 N/A ND
Methanol 50 / 200 N/A ND
n-Pentane 20 / 50 N/A ND
Propane 10 / 20 N/A ND
Toluene 7 / 21 N/A ND
Total Xylenes 50 / 160 N/A ND

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

08/27/2022

ND

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Compound LOD/LOQ
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Arsenic 0.02 / 0.1 N/A ND
Cadmium 0.02 / 0.05 N/A ND
Lead 0.04 / 0.1 N/A ND
Mercury 0.002 / 0.01 N/A ND

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants. And Analysis conducted by 3MTM PetrifilmTM and plate counts of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants and QSP 6794 - Plating with 3MTM PetrifilmTM

Microbiology Test Results (PCR)

08/30/2022

ND

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Compound Result
Salmonella spp. ND
Shiga toxin-producing Escherichia coli ND
Microbiology Test Results (PLATING)

08/30/2022

ND

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Compound Result
(cfu/g)
Coliforms ND
Total Aerobic Bacteria ND
Total Yeast and Mold ND

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