Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

Relief Gummies

Infused, Hemp

Date Issued:

02/08/2025

Serving Size:

3.8075 grams

Sample Information

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Sample Details

Sample ID:250203R012

Batch Number:2410031

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Cultivator / Manufacturer

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Distributor / Tested For

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Safety Analysis - Summary

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Pesticides: ND

Mycotoxins: ND

Residual Solvents: Detected

Heavy Metals: ND

Microbiology (PCR): ND

Microbiology (Plating): ND

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Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

02/08/2025

ND

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Compound LOD/LOQ
(μg/g) 		Measurement
Uncertainty
(μg/g) 		Result
(μg/g)
Abamectin 0.03 / 0.10 N/A ND
Azoxystrobin 0.02 / 0.07 N/A ND
Bifenazate 0.01 / 0.04 N/A ND
Bifenthrin 0.02 / 0.05 N/A ND
Boscalid 0.03 / 0.09 N/A ND
Chlorpyrifos 0.02 / 0.06 N/A ND
Cypermethrin 0.11 / 0.32 N/A ND
Etoxazole 0.02 / 0.06 N/A ND
Hexythiazox 0.02 / 0.07 N/A ND
Imidacloprid 0.04 / 0.11 N/A ND
Malathion 0.03 / 0.09 N/A ND
Myclobutanil 0.03 / 0.09 N/A ND
Permethrin 0.04 / 0.12 N/A ND
Piperonyl Butoxide 0.02 / 0.07 N/A ND
Propiconazole 0.02 / 0.07 N/A ND
Spiromesifen 0.02 / 0.05 N/A ND
Tebuconazole 0.02 / 0.07 N/A ND
Trifloxystrobin 0.03 / 0.08 N/A ND

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS

Mycotoxin Test Results

02/08/2025

ND

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Compound LOD/LOQ
(μg/kg) 		Measurement
Uncertainty
(μg/kg) 		Result
(μg/kg)
Aflatoxin B1 2.0 / 6.0 N/A ND
Aflatoxin B2 1.8 / 5.6 N/A ND
Aflatoxin G1 1.0 / 3.1 N/A ND
Aflatoxin G2 1.2 / 3.5 N/A ND
Ochratoxin A 6.3 / 19.2 N/A ND
Total Aflatoxin ± ND

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

02/05/2025

DETECTED

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Compound LOD/LOQ
(μg/g) 		Measurement
Uncertainty
(μg/g) 		Result
(μg/g)
Propane 0.234 / 0.781 N/A ND
2-Methylpropane (Isobutane) 0.052 / 0.173 N/A ND
n-Butane 0.019 / 0.063 N/A ND
Total Butanes ± ND
n-Pentane 0.310 / 1.033 N/A ND
n-Hexane 0.110 / 0.366 N/A ND
2,2-Dimethylpentane (Neoheptane) 0.493 / 1.642 N/A ND
2,3-Dimethylpentane 1.009 / 3.365 N/A ND
2,4-Dimethylpentane 0.737 / 2.458 N/A ND
3,3-Dimethylpentane 0.198 / 0.660 N/A ND
2,2,3-Trimethylbutane (Triptane) 0.521 / 1.738 N/A ND
2-Methylhexane (Isoheptane) 0.610 / 2.034 N/A ND
3-Methylhexane 0.235 / 0.785 N/A ND
3-Ethylpentane 0.304 / 1.012 N/A ND
n-Heptane 13.12 / 43.72 N/A ND
Total Heptanes ± ND
Benzene 0.089 / 0.295 N/A ND
Toluene 0.115 / 0.382 N/A ND
1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene) 0.451 / 1.502 N/A ND
1,2-Dimethylbenzene (o-Xylene) 0.387 / 1.289 N/A ND
Total Xylenes ± ND
Methanol 53.92 / 163.4 N/A ND
Ethanol 8.984 / 27.23 N/A <LOQ
2-Propanol (Isopropyl Alcohol) 8.421 / 25.52 N/A ND
Acetone 10.59 / 32.08 N/A ND
Ethyl Acetate 1.123 / 3.745 N/A ND

Total Butanes = n-Butane + 2-Methylpropane (Isobutane)

Total Heptanes = 2,2-Dimethylpentane (Neoheptane) + 2,3-Dimethylpentane + 2,4-Dimethylpentane + 3,3-Dimethylpentane + 2,2,3-Trimethylbutane (Triptane) + 2-Methylhexane (Isoheptane) + 3-Methylhexane + 3-Ethylpentane + n-Heptane

Total Xylenes = 1,2-Dimethylbenzene (o-Xylene) + 1,3-Dimethylbenzene (m-Xylene) / 1,4-Dimethylbenzene (p-Xylene)

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

02/06/2025

ND

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Compound LOD/LOQ
(μg/g) 		Measurement
Uncertainty
(μg/g) 		Result
(μg/g)
Arsenic 0.02 / 0.1 N/A ND
Cadmium 0.02 / 0.05 N/A ND
Lead 0.04 / 0.1 N/A ND
Mercury 0.002 / 0.01 N/A ND

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants. And Analysis conducted by 3MTM PetrifilmTM and plate counts of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants

Microbiology Test Results (PCR)

02/07/2025

ND

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Compound Result
Salmonella spp. ND
Shiga toxin-producing Escherichia coli ND
Microbiology Test Results (PLATING)

02/07/2025

ND

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Compound Result
(cfu/g)
Coliforms ND
Total Yeast and Mold ND
Total Aerobic Bacteria ND

Notes

COA Notes:

Sample unit mass provided by client.

COA ID: 250203R012-001

For quality assurance purposes. Not a Regulatory Hemp Lab Test Report. These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT), μg/g = ppm, μg/kg = ppb, too numerous to count >250 cfu/plate (TNTC), colony-forming unit (cfu)

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