Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

Chill Paws 500mg

Infused, Non-Inhalable

Date Issued:

03/10/2020

Total THC 0.660 mg/unit
Total CBD 562.950 mg/unit
Sum Cannabinoids 574.590 mg/unit
Total Cannabinoids 574.590 mg/unit

Sample Information

Sample Details

Sample ID:200304P002

Batch Number:

Cultivator / Manufacturer

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Distributor / Tested For

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Cannabinoid Analysis - Summary

Total THC: 0.660 mg/unit

Total CBD: 562.950 mg/unit

Sum of Cannabinoids: 574.590 mg/unit

Total Cannabinoids: 574.590 mg/unit

Density:0.9357 g/mL

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Safety Analysis - Summary

Δ9-THC per Unit: Pass

Pesticides: Pass

Residual Solvents: Pass

Heavy Metals: Pass

Microbiology (Plating): ND

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 0.660 mg/unit

9-THC+0.877*THCa)

Total CBD: 562.950 mg/unit

(CBD+0.877*CBDa)

Total Cannabinoids: 574.590 mg/unit

Total CBG: 7.830 mg/unit

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 0.120 mg/unit

Total CBC (CBC+0.877*CBCa)

Total CBDV: 2.850 mg/unit

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

03/05/2020

Result Views

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Compound LOD/LOQ
(mg/mL)
Result
(mg/mL)
Result
(%)
Cannabidiol (CBD) 0.0009 / 0.003 18.765 2.0055
Cannabigerol (CBG) 0.001 / 0.003 0.261 0.0279
Cannabidivarin (CBDV) 0.0004 / 0.001 0.095 0.0102
Δ9 Tetrahydrocannabinol (Δ9THC) 0.0009 / 0.003 0.022 0.0024
Cannabinol (CBN) 0.0009 / 0.003 0.006 0.0006
Cannabichromene (CBC) 0.0011 / 0.003 0.004 0.0004
Cannabicyclol (CBL) 0.0021 / 0.006 ND ND
Cannabichromenic Acid (CBCa) 0.0015 / 0.005 ND ND
Cannabidiolic Acid (CBDa) 0.0009 / 0.003 ND ND
Cannabigerolic Acid (CBGa) 0.0008 / 0.002 ND ND
Tetrahydrocannabivarin (THCV) 0.0004 / 0.001 ND ND
Tetrahydrocannabinolic Acid (THCa) 0.0009 / 0.003 ND ND
Cannabidivarinic Acid (CBDVa) 0.0003 / 0.001 ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.0013 / 0.004 ND ND
∆8 Tetrahydrocannabinol (Δ8THC) 0.0009 / 0.003 ND ND
SUM OF CANNABINOIDS 19.153 mg/mL 2.0469%
Unit Mass:

30 milliliters

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Δ9-THC per Unit 1100 per-package limit 0.660 mg/unit Pass
Total THC per Unit 0.660 mg/unit
CBD per Unit 562.950 mg/unit
Total CBD per Unit 562.950 mg/unit
Sum of Cannabinoids per Unit 574.590 mg/unit
Total Cannabinoids per Unit 574.590 mg/unit
Density Test Result

0.9357 g/mL Tested 03/05/2020 Method: QSP 7870 - Sample Preparation

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

03/10/2020

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Abamectin 0.030 / 0.091 0.3 N/A ND Pass
Azoxystrobin 0.015 / 0.047 40 N/A ND Pass
Bifenazate 0.012 / 0.035 5 N/A ND Pass
Bifenthrin 0.013 / 0.038 0.5 N/A ND Pass
Boscalid 0.008 / 0.023 10 N/A ND Pass
Chlorpyrifos 0.029 / 0.089 ≥ LOD N/A ND Pass
Cypermethrin 0.030 / 0.091 1 N/A ND Pass
Etoxazole 0.007 / 0.022 1.5 N/A ND Pass
Hexythiazox 0.009 / 0.027 2 N/A ND Pass
Imidacloprid 0.017 / 0.050 3 N/A ND Pass
Malathion 0.006 / 0.019 5 N/A ND Pass
Myclobutanil 0.015 / 0.044 9 N/A ND Pass
Permethrin 0.027 / 0.082 20 N/A ND Pass
Piperonyl Butoxide 0.007 / 0.020 8 N/A ND Pass
Propiconazole 0.004 / 0.013 20 N/A ND Pass
Spiromesifen 0.005 / 0.015 12 N/A ND Pass
Tebuconazole 0.006 / 0.018 2 N/A ND Pass
Trifloxystrobin 0.007 / 0.020 30 N/A ND Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

03/06/2020

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Result
(μg/g)
Result
1,2-Dichloroethane 0.111 / 0.336 1 ND Pass
Benzene 0.043 / 0.132 1 ND Pass
Chloroform 0.064 / 0.195 1 ND Pass
Dichloromethane (Methylene Chloride) 0.172 / 0.521 1 ND Pass
Ethylene Oxide 0.136 / 0.413 1 ND Pass
Trichloroethylene 0.040 / 0.120 1 ND Pass
2-Propanol (Isopropyl Alcohol) 15.358 / 46.536 5000 ND Pass
Acetone 14.703 / 44.549 5000 ND Pass
Acetonitrile 2.727 / 8.262 410 ND Pass
Ethanol 11.775 / 35.679 5000 ND Pass
Ethyl Acetate 16.227 / 49.169 5000 ND Pass
Ethyl Ether 11.608 / 35.172 5000 ND Pass
Methanol 15.584 / 47.220 3000 ND Pass
n-Butane 5.672 / 17.185 5000 ND Pass
n-Heptane 12.982 / 39.336 5000 ND Pass
n-Hexane 1.816 / 5.502 290 ND Pass
n-Pentane 12.355 / 37.434 5000 ND Pass
Propane 1.359 / 4.117 5000 ND Pass
Toluene 7.174 / 21.736 890 ND Pass
Total Xylenes 34.438 / 104.347 2170 ND Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

03/06/2020

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Result
(μg/g)
Result
Arsenic 0.013 / 0.039 1.5 ND Pass
Cadmium 0.012 / 0.035 0.5 ND Pass
Lead 0.031 / 0.095 0.5 ND Pass
Mercury 0.002 / 0.005 3 ND Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants. And Analysis conducted by 3MTM PetrifilmTM and plate counts of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants and QSP 6794 - Plating with 3MTM PetrifilmTM

Microbiology Test Results (PLATING)

03/08/2020

ND

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Compound Result
(cfu/g)
Total Yeast and Mold ND
Total Aerobic Bacteria ND

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