Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

500mg Chill Paws Tincture-CBD

Infused, Hemp Infused

Date Issued:

06/30/2021

Total THC Not Detected
Total CBD 447.360 mg/unit
Sum Cannabinoids 488.970 mg/unit
Total Cannabinoids 488.970 mg/unit

Sample Information

Sample Details

Sample ID:210626T002

Batch Number:

Cultivator / Manufacturer

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Distributor / Tested For

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Cannabinoid Analysis - Summary

Total THC: Not Detected

Total CBD: 447.360 mg/unit

Sum of Cannabinoids: 488.970 mg/unit

Total Cannabinoids: 488.970 mg/unit

Density:0.9474 g/mL

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Safety Analysis - Summary

Pesticides: ND

Residual Solvents: Detected

Heavy Metals: ND

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: Not Detected

9-THC+0.877*THCa)

Total CBD: 447.360 mg/unit

(CBD+0.877*CBDa)

Total Cannabinoids: 488.970 mg/unit

Total CBG: 4.950 mg/unit

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 18.120 mg/unit

Total CBC (CBC+0.877*CBCa)

Total CBDV: 3.030 mg/unit

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

06/28/2021

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/mL)
Measurement
Uncertainty
(mg/mL)
Result
(mg/mL)
Result
(%)
Cannabidiol (CBD) 0.004 / 0.011 ±0.7143 14.912 1.5740
Cannabichromene (CBC) 0.003 / 0.010 ±0.0250 0.604 0.0638
Cannabinol (CBN) 0.001 / 0.007 ±0.0169 0.457 0.0482
Cannabigerol (CBG) 0.002 / 0.006 ±0.0103 0.165 0.0174
Cannabidivarin (CBDV) 0.002 / 0.012 ±0.0053 0.101 0.0107
Cannabicyclol (CBL) 0.003 / 0.010 ±0.0028 0.060 0.0063
Cannabichromenic Acid (CBCa) 0.001 / 0.015 N/A ND ND
Cannabidiolic Acid (CBDa) 0.001 / 0.026 N/A ND ND
Cannabigerolic Acid (CBGa) 0.002 / 0.007 N/A ND ND
Tetrahydrocannabivarin (THCV) 0.002 / 0.012 N/A ND ND
Tetrahydrocannabinolic Acid (THCa) 0.001 / 0.005 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.001 / 0.018 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.002 / 0.019 N/A ND ND
∆8 Tetrahydrocannabinol (Δ8THC) 0.01 / 0.02 N/A ND ND
Δ9 Tetrahydrocannabinol (Δ9THC) 0.002 / 0.014 N/A ND ND
SUM OF CANNABINOIDS 16.299 mg/mL 1.7204%
Unit Mass:

30 milliliters

Swipe left on table to see additional columns

Δ9-THC per Unit ND
Total THC per Unit ND
CBD per Unit 447.360 mg/unit
Total CBD per Unit 447.360 mg/unit
Sum of Cannabinoids per Unit 488.970 mg/unit
Total Cannabinoids per Unit 488.970 mg/unit
Density Test Result

0.9474 g/mL Tested 06/28/2021 Method: QSP 7870 - Sample Preparation

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

06/28/2021

ND

Swipe left on table to see additional columns

Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Abamectin 0.03 / 0.10 0.07 N/A ND
Azoxystrobin 0.01 / 0.04 0.01 N/A ND
Bifenazate 0.01 / 0.02 0.01 N/A ND
Bifenthrin 0.01 / 0.02 0.2 N/A ND
Boscalid 0.02 / 0.06 0.01 N/A ND
Chlorpyrifos 0.02 / 0.06 0.04 N/A ND
Cypermethrin 0.1 / 0.3 0.3 N/A ND
Etoxazole 0.010 / 0.028 0.01 N/A ND
Hexythiazox 0.01 / 0.04 0.01 N/A ND
Imidacloprid 0.01 / 0.04 0.01 N/A ND
Malathion 0.02 / 0.05 0.02 N/A ND
Myclobutanil 0.03 / 0.1 0.01 N/A ND
Permethrin 0.03 / 0.09 0.04 N/A ND
Piperonyl Butoxide 0.003 / 0.009 0.2 N/A ND
Propiconazole 0.01 / 0.03 0.1 N/A ND
Spiromesifen 0.02 / 0.05 0.03 N/A ND
Tebuconazole 0.02 / 0.07 0.01 N/A ND
Trifloxystrobin 0.01 / 0.03 0.02 N/A ND

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

06/28/2021

DETECTED

Swipe left on table to see additional columns

Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
1,2-Dichloroethane 0.05 / 0.1 5 N/A ND
Benzene 0.03 / 0.09 0 N/A ND
Chloroform 0.1 / 0.2 1 N/A ND
Dichloromethane (Methylene Chloride) 0.3 / 0.9 600 N/A ND
Ethylene Oxide 0.3 / 0.8 5 N/A ND
Trichloroethylene 0.1 / 0.3 80 N/A ND
2-Propanol (Isopropyl Alcohol) 10 / 40 500 N/A <LOQ
Acetone 20 / 50 5000 N/A ND
Acetonitrile 2 / 7 0.41 N/A ND
Ethanol 20 / 50 1000 N/A ND
Ethyl Acetate 20 / 60 1000 N/A ND
Ethyl Ether 20 / 50 5000 N/A ND
Methanol 50 / 200 500 N/A ND
n-Butane 10 / 50 2000 N/A ND
n-Heptane 20 / 60 500 N/A ND
n-Hexane 2 / 5 0 N/A ND
n-Pentane 20 / 50 1000 N/A ND
Propane 10 / 20 500 N/A ND
Toluene 7 / 21 0 N/A ND
Total Xylenes 50 / 160 217 N/A ND

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

06/30/2021

ND

Swipe left on table to see additional columns

Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Arsenic 0.02 / 0.1 0.42 N/A ND
Cadmium 0.02 / 0.05 0.27 N/A ND
Lead 0.04 / 0.1 0.5 N/A ND
Mercury 0.002 / 0.01 0.4 N/A ND

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