Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

Miracle Eyes

Infused, Topical

Date Issued:

11/01/2019

Total THC Not Detected
Total CBD 64.630 mg/unit
Sum Cannabinoids 65.750 mg/unit
Total Cannabinoids 65.750 mg/unit
Total Terpenoids 0.7162%
Top 3 Terpenoids
  1. Limonene 0.3194%
  2. Camphor 0.0956%
  3. α-Pinene 0.0823%

Sample Information

Sample Details

Sample ID:191003U027

Batch Number:

Cultivator / Manufacturer

Show Details

Distributor / Tested For

Show Details

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Cannabinoid Analysis - Summary

Total THC: Not Detected

Total CBD: 64.630 mg/unit

Sum of Cannabinoids: 65.750 mg/unit

Total Cannabinoids: 65.750 mg/unit

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

36 tested, Top 3 Highlighted

Total Terpenoids: 0.7162%

 
 
 

1

Limonene (0.3194%)

2

Camphor (0.0956%)

3

α-Pinene (0.0823%)

Safety Analysis - Summary

Δ9-THC per Unit: Pass

Pesticides: Pass

Residual Solvents: Pass

Heavy Metals: Pass

Microbiology (PCR): Pass

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: Not Detected

9-THC+0.877*THCa)

Total CBD: 64.630 mg/unit

(CBD+0.877*CBDa)

Total Cannabinoids: 65.750 mg/unit

Total CBG: ND

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: ND

Total CBC (CBC+0.877*CBCa)

Total CBDV: 1.120 mg/unit

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

10/04/2019

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Result
(mg/g)
Result
(%)
Cannabidiol (CBD) 0.0009 / 0.003 6.463 0.6463
Cannabidivarin (CBDV) 0.0004 / 0.001 0.112 0.0112
Cannabidiolic Acid (CBDa) 0.0009 / 0.003 <LOQ <LOQ
Δ9 Tetrahydrocannabinol (Δ9THC) 0.0009 / 0.003 ND ND
∆8 Tetrahydrocannabinol (Δ8THC) 0.0009 / 0.003 ND ND
Tetrahydrocannabinolic Acid (THCa) 0.0009 / 0.003 ND ND
Tetrahydrocannabivarin (THCV) 0.0004 / 0.001 ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.0013 / 0.004 ND ND
Cannabidivarinic Acid (CBDVa) 0.0003 / 0.001 ND ND
Cannabigerol (CBG) 0.001 / 0.003 ND ND
Cannabigerolic Acid (CBGa) 0.0008 / 0.002 ND ND
Cannabicyclol (CBL) 0.0021 / 0.006 ND ND
Cannabinol (CBN) 0.0009 / 0.003 ND ND
Cannabichromene (CBC) 0.0011 / 0.003 ND ND
Cannabichromenic Acid (CBCa) 0.0015 / 0.005 ND ND
SUM OF CANNABINOIDS 6.575 mg/g 0.6575%
Unit Mass:

10 grams

Swipe left on table to see additional columns

Δ9-THC per Unit 1100 per-package limit ND Pass
Total THC per Unit ND
CBD per Unit 64.630 mg/unit
Total CBD per Unit 64.630 mg/unit
Sum of Cannabinoids per Unit 65.750 mg/unit
Total Cannabinoids per Unit 65.750 mg/unit
Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

Summary

Total Terpenoids (mg/g): 7.162 mg/g

Total Terpenoids (%): 0.7162%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume.

  1. Limonene 0.3194%

    A monoterpene with a fragrance that can be described as orangey, citrusy, sweet and tart. It is most commonly found in nature as D-Limonene and is a primary contributor to the distinct scent of orange peels, from which it is commonly derived. Found in numerous pines, red maple, silver maple, aspens, cottonwoods, hemlocks, sumac, cedar, junipers...etc.

  2. Camphor 0.0956%

    A monoterpenoid ketone with a pungent fragrance that is as reminiscent of mothballs. It is commonly derived from Cinnamomum camphora, from which it lends its lame. It is a constituent of turpentine and has been used by certain cultures as an embalming fluid due to its antimicrobial effects. Found in camphor laurel, rosemary, East African camphorwood, goldenasters, coriander, feverfew, tarragon, nutmeg, sweet wormwood, yerba buena, mountain mint, hyssop, forskohlii, tansy, thyme, turmeric...etc.

  3. α-Pinene 0.0823%

    One of two isomers of the monoterpene Pinene, the most abundant terpene in the natural world. It is responsible for the distinct aroma of many coniferous trees, particularly pines, from which it derives its name. It is a primary constituent of turpentine. Found in pines, rose gun, parsley, frankincense, guava, juniper, rosemary, nutmeg, blue gum, valerian...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

10/05/2019

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Result
(mg/g)
Result
(%)
Limonene 0.013 / 0.039 3.194 0.3194
Camphor 0.054 / 0.163 0.956 0.0956
α-Pinene 0.022 / 0.067 0.823 0.0823
Eucalyptol 0.021 / 0.063 0.723 0.0723
Nerolidol 0.035 / 0.106 0.389 0.0389
Camphene 0.027 / 0.08 0.38 0.038
Myrcene 0.027 / 0.082 0.210 0.0210
Linalool 0.019 / 0.058 0.190 0.0190
β-Pinene 0.027 / 0.081 0.135 0.0135
Sabinene 0.027 / 0.082 0.092 0.0092
β-Caryophyllene 0.018 / 0.054 0.070 0.0070
Δ3-Carene 0.029 / 0.087 <LOQ <LOQ
Isoborneol 0.033 / 0.101 <LOQ <LOQ
Borneol 0.048 / 0.146 <LOQ <LOQ
Terpineol 0.022 / 0.068 <LOQ <LOQ
Valencene 0.008 / 0.023 <LOQ <LOQ
Guaiol 0.022 / 0.066 <LOQ <LOQ
α-Phellandrene 0.037 / 0.111 ND ND
α-Terpinene 0.03 / 0.09 ND ND
β-Ocimene 0.028 / 0.085 ND ND
γ-Terpinene 0.03 / 0.09 ND ND
Sabinene Hydrate 0.018 / 0.054 ND ND
Fenchone 0.03 / 0.092 ND ND
Terpinolene 0.022 / 0.067 ND ND
Fenchol 0.023 / 0.069 ND ND
Isopulegol 0.013 / 0.04 ND ND
Menthol 0.022 / 0.067 ND ND
Nerol 0.023 / 0.068 ND ND
Pulegone 0.022 / 0.068 ND ND
Geraniol 0.017 / 0.05 ND ND
Geranyl Acetate 0.016 / 0.048 ND ND
α-Cedrene 0.017 / 0.051 ND ND
α-Humulene 0.013 / 0.038 ND ND
Caryophyllene Oxide 0.028 / 0.084 ND ND
Cedrol 0.029 / 0.086 ND ND
α-Bisabolol 0.017 / 0.051 ND ND
TOTAL 7.162 mg/g 0.7162%
Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

10/06/2019

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Result
(μg/g)
Result
Aldicarb 0.030 / 0.091 ≥ LOD ND Pass
Carbofuran 0.029 / 0.089 ≥ LOD ND Pass
Chlordane* 0.032 / 0.097 ≥ LOD ND Pass
Chlorfenapyr* 0.030 / 0.090 ≥ LOD ND Pass
Chlorpyrifos 0.029 / 0.089 ≥ LOD ND Pass
Coumaphos 0.029 / 0.089 ≥ LOD ND Pass
Daminozide 0.030 / 0.091 ≥ LOD ND Pass
Dichlorvos (DDVP) 0.029 / 0.089 ≥ LOD ND Pass
Dimethoate 0.029 / 0.089 ≥ LOD ND Pass
Ethoprophos 0.029 / 0.089 ≥ LOD ND Pass
Etofenprox 0.029 / 0.089 ≥ LOD ND Pass
Fenoxycarb 0.029 / 0.089 ≥ LOD ND Pass
Fipronil 0.029 / 0.089 ≥ LOD ND Pass
Imazalil 0.029 / 0.089 ≥ LOD ND Pass
Methiocarb 0.029 / 0.089 ≥ LOD ND Pass
Parathion-methyl 0.029 / 0.089 ≥ LOD ND Pass
Mevinphos 0.029 / 0.089 ≥ LOD ND Pass
Paclobutrazol 0.029 / 0.089 ≥ LOD ND Pass
Propoxur 0.029 / 0.089 ≥ LOD ND Pass
Spiroxamine 0.029 / 0.089 ≥ LOD ND Pass
Thiacloprid 0.029 / 0.089 ≥ LOD ND Pass
Abamectin 0.030 / 0.091 0.3 ND Pass
Acephate 0.013 / 0.039 5 ND Pass
Acequinocyl 0.010 / 0.031 4 ND Pass
Acetamiprid 0.013 / 0.038 5 ND Pass
Azoxystrobin 0.015 / 0.047 40 ND Pass
Bifenazate 0.012 / 0.035 5 ND Pass
Bifenthrin 0.013 / 0.038 0.5 ND Pass
Boscalid 0.008 / 0.023 10 ND Pass
Captan 0.099 / 0.300 5 ND Pass
Carbaryl 0.014 / 0.043 0.5 ND Pass
Chlorantraniliprole 0.020 / 0.061 40 ND Pass
Clofentezine 0.009 / 0.027 0.5 ND Pass
Cyfluthrin 0.099 / 0.299 1 ND Pass
Cypermethrin 0.030 / 0.091 1 ND Pass
Diazinon 0.009 / 0.027 0.2 ND Pass
Dimethomorph 0.018 / 0.055 20 ND Pass
Etoxazole 0.007 / 0.022 1.5 ND Pass
Fenhexamid 0.015 / 0.045 10 ND Pass
Fenpyroximate 0.012 / 0.036 2 ND Pass
Flonicamid 0.022 / 0.066 2 ND Pass
Fludioxonil 0.020 / 0.061 30 ND Pass
Hexythiazox 0.009 / 0.027 2 ND Pass
Imidacloprid 0.017 / 0.050 3 ND Pass
Kresoxim-methyl 0.010 / 0.029 1 ND Pass
Malathion 0.006 / 0.019 5 ND Pass
Metalaxyl 0.011 / 0.033 15 ND Pass
Methomyl 0.022 / 0.067 0.1 ND Pass
Myclobutanil 0.015 / 0.044 9 ND Pass
Naled 0.010 / 0.031 0.5 ND Pass
Oxamyl 0.014 / 0.042 0.2 ND Pass
Pentachloronitrobenzene* 0.020 / 0.061 0.2 ND Pass
Permethrin 0.027 / 0.082 20 ND Pass
Phosmet 0.010 / 0.030 0.2 ND Pass
Piperonyl Butoxide 0.007 / 0.020 8 ND Pass
Prallethrin 0.011 / 0.032 0.4 ND Pass
Propiconazole 0.004 / 0.013 20 ND Pass
Pyrethrins 0.012 / 0.036 1 ND Pass
Pyridaben 0.007 / 0.020 3 ND Pass
Spinetoram 0.006 / 0.017 3 ND Pass
Spinosad 0.010 / 0.031 3 ND Pass
Spiromesifen 0.005 / 0.015 12 ND Pass
Spirotetramat 0.014 / 0.042 13 ND Pass
Tebuconazole 0.006 / 0.018 2 ND Pass
Thiamethoxam 0.011 / 0.033 4.5 ND Pass
Trifloxystrobin 0.007 / 0.020 30 ND Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

10/05/2019

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Result
(μg/g)
Result
1,2-Dichloroethane 0.111 / 0.336 1 ND Pass
Benzene 0.043 / 0.132 1 ND Pass
Chloroform 0.064 / 0.195 1 ND Pass
Ethylene Oxide 0.136 / 0.413 1 ND Pass
Dichloromethane (Methylene Chloride) 0.172 / 0.521 1 ND Pass
Trichloroethylene 0.040 / 0.120 1 ND Pass
Acetone 14.703 / 44.549 5000 ND Pass
Acetonitrile 2.727 / 8.262 410 ND Pass
n-Butane 5.672 / 17.185 5000 ND Pass
Ethanol 11.775 / 35.679 <LOQ
Ethyl Acetate 16.227 / 49.169 5000 ND Pass
Ethyl Ether 11.608 / 35.172 5000 ND Pass
n-Heptane 12.982 / 39.336 5000 ND Pass
n-Hexane 1.816 / 5.502 290 ND Pass
2-Propanol (Isopropyl Alcohol) 15.358 / 46.536 ND
Methanol 15.584 / 47.220 3000 ND Pass
n-Pentane 12.355 / 37.434 5000 ND Pass
Propane 1.359 / 4.117 5000 ND Pass
Toluene 7.174 / 21.736 890 ND Pass
Total Xylenes 34.438 / 104.347 2170 ND Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

10/04/2019

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Result
(μg/g)
Result
Arsenic 0.013 / 0.039 1.5 ND Pass
Cadmium 0.012 / 0.035 0.5 ND Pass
Lead 0.031 / 0.095 0.5 ND Pass
Mercury 0.002 / 0.005 3 ND Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants

Microbiology Test Results (PCR)

10/05/2019

PASS

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Compound Action Limit Result Result
Shiga toxin-producing Escherichia coli Detect ND Pass
Salmonella spp. Detect ND Pass
Aspergillus fumigatus Detect ND Pass
Aspergillus flavus Detect ND Pass
Aspergillus niger Detect ND Pass
Aspergillus terreus Detect ND Pass

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