SC Labs | Mad Labs - Lemoncello Jack 5g

Certificate of Analysis

REGULATORY COMPLIANCE

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Sample Name:

Mad Labs - Lemoncello Jack 5g

Flower, Inhalable

Sum Cannabinoids 23.1453%

Total Cannabinoids 20.3886%

Total THC 19.7924%

Total CBD 0.0637%

Total Terpenoids 1.1052%
PhytoFacts^®

Top 3 Terpenoids

Myrcene 0.3401%
α-Pinene 0.2317%
β-Caryophyllene 0.1628%

Sample Information

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Sample Details

Sample ID:240418V004

Batch Number:ML-LCJ-032524

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Cultivator / Manufacturer

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Distributor

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Sampling Method: QSP 1265 - Sampling of Cannabis and Product Batches

PhytoFacts® Report

aroma

flavor

effect

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The PhytoFacts chemometric report provides additional cannabinoid and terpenoid details, including dominant terpenes, entourage effects, aroma, flavor, and more.

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Cannabinoid Analysis - Summary

Calculated using Dry-Weight

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Sum of Cannabinoids: 23.1453%

Total Cannabinoids: 20.3886%

Total THC: 19.7924%

Total CBD: 0.0637%

Moisture:9.2%

Sum of Cannabinoids = Δ⁹-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ⁸-THC + CBL + CBN

Total Cannabinoids = (Δ⁹-THC+0.877*THCa+Δ⁸-THC) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + CBL + CBN

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ⁹-THC + (THCa (0.877)) + Δ⁸-THC
Total CBD = CBD + (CBDa (0.877))

What is dry weight, and how is it calculated?

Dry weight: The weight of a sample after it goes through the drying process.

Pursuant to section § 5724 of California Code of Regulations Title 16 Division 42. Department of Cannabis Control, the equation for moisture correction is: Dry-weight percent cannabinoid = wet-weight percent cannabinoid / (1 − percent moisture / 100)

Why are Sum of Cannabinoids and Total Cannabinoids calculated separately?

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

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Total Terpenoids: 1.1052%

Myrcene (0.3401%)

α-Pinene (0.2317%)

β-Caryophyllene (0.1628%)

Safety Analysis - Summary

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Pesticides: Pass

Mycotoxins: Pass

Heavy Metals: Pass

Microbiology: Pass

Foreign Material: Pass

Water Activity: Pass

View Complete Test Results:

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Cannabinoid Analysis

Tested

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD). Calculated using Dry-Weight.

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total Cannabinoids: 20.3886%

Total THC: 19.7924%

(Δ⁹-THC+0.877*THCa+Δ⁸-THC)

Total CBD: 0.0637%

(CBD+0.877*CBDa)

Total CBG: 0.2878%

Total CBG (CBG+0.877*CBGa)

Total THCV: 0.0567%

Total THCV (THCV+0.877*THCVa)

Total CBC: 0.188%

Total CBC (CBC+0.877*CBCa)

Total CBDV: ND

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

04/19/2024

Result Views

Table Pie Chart

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Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
Tetrahydrocannabinolic Acid (THCa)	0.062 / 0.250	±4.0329	217.993	21.7993
Δ9 Tetrahydrocannabinol (Δ9THC)	0.047 / 0.250	±0.1268	6.744	0.6744
Cannabigerolic Acid (CBGa)	0.040 / 0.250	±0.0735	2.617	0.2617
Cannabichromenic Acid (CBCa)	0.199 / 0.500	±0.0851	2.144	0.2144
Cannabidiolic Acid (CBDa)	0.031 / 0.250	±0.0132	0.726	0.0726
Tetrahydrocannabivarinic Acid (THCVa)	0.040 / 0.250	±0.0058	0.646	0.0646
Cannabigerol (CBG)	0.037 / 0.250	±0.0076	0.583	0.0583
Cannabinol (CBN)	0.033 / 0.250	N/A	<LOQ	<LOQ
Cannabichromene (CBC)	0.072 / 0.250	N/A	<LOQ	<LOQ
∆8 Tetrahydrocannabinol (Δ8THC)	0.075 / 0.250	N/A	ND	ND
Tetrahydrocannabivarin (THCV)	0.052 / 0.250	N/A	ND	ND
Cannabidiol (CBD)	0.062 / 0.250	N/A	ND	ND
Cannabidivarin (CBDV)	0.044 / 0.250	N/A	ND	ND
Cannabidivarinic Acid (CBDVa)	0.017 / 0.250	N/A	ND	ND
Cannabicyclol (CBL)	0.126 / 0.382	N/A	ND	ND
SUM OF CANNABINOIDS			231.453 mg/g	23.1453%

Unit Mass:

5 grams

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Δ⁹-THC per Unit		33.720 mg/unit
Total THC per Unit		989.620 mg/unit
CBD per Unit		ND
Total CBD per Unit		3.185 mg/unit
Sum of Cannabinoids per Unit		1157.265 mg/unit
Total Cannabinoids per Unit		1019.430 mg/unit

Moisture Test Result

9.2% Tested 04/20/2024 Method: QSP 1224 - Loss on Drying (Moisture)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpenoid Analysis

Tested

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

View PhytoFacts COA

See a visual representation of this sample's cannabinoid and terpenoid properties, including entourage effects, aroma, and flavor profile.

Summary

Total Terpenoids (mg/g): 11.052 mg/g

Total Terpenoids (%): 1.1052%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume. To see more detail for terpenoid content, view the PhytoFacts report.

Myrcene 0.3401%
A monoterpene with a fragrance that can be described as peppery, spicy, herbal, floral and woody. Although it has a pleasant odor, it is typically used by the perfume industry as precursor for developing other fragrances. Found in hops, houttuynia, bay, thyme, lemon grass, mango, verbena, cardamom, citrus...etc.

α-Pinene 0.2317%
One of two isomers of the monoterpene Pinene, the most abundant terpene in the natural world. It is responsible for the distinct aroma of many coniferous trees, particularly pines, from which it derives its name. It is a primary constituent of turpentine. Found in pines, rose gun, parsley, frankincense, guava, juniper, rosemary, nutmeg, blue gum, valerian...etc.

β-Caryophyllene 0.1628%
A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB² receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

04/21/2024

Result Views

Table Bar Graph

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Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
Myrcene	0.007 / 0.025	±0.1204	3.401	0.3401
α-Pinene	0.005 / 0.015	±0.0829	2.317	0.2317
β-Caryophyllene	0.004 / 0.013	±0.0876	1.628	0.1628
β-Pinene	0.004 / 0.015	±0.0347	1.073	0.1073
α-Humulene	0.009 / 0.031	±0.0323	0.601	0.0601
Limonene	0.005 / 0.016	±0.0154	0.471	0.0471
Linalool	0.009 / 0.030	±0.0151	0.384	0.0384
trans-β-Farnesene	0.008 / 0.028	±0.0203	0.357	0.0357
α-Bisabolol	0.008 / 0.026	±0.0129	0.300	0.0300
Nerolidol	0.006 / 0.020	±0.0076	0.096	0.0096
Fenchol	0.009 / 0.029	±0.0031	0.084	0.0084
Caryophyllene Oxide	0.011 / 0.038	±0.0050	0.084	0.0084
Terpineol	0.008 / 0.025	±0.0051	0.083	0.0083
Camphene	0.004 / 0.014	±0.0018	0.055	0.0055
α-Cedrene	0.005 / 0.017	±0.0026	0.047	0.0047
Terpinolene	0.008 / 0.027	±0.0005	0.032	0.0032
Borneol	0.004 / 0.014	±0.0013	0.028	0.0028
Citronellol	0.003 / 0.010	±0.0003	0.011	0.0011
Eucalyptol	0.005 / 0.018	N/A	<LOQ	<LOQ
Sabinene Hydrate	0.007 / 0.022	N/A	<LOQ	<LOQ
Fenchone	0.008 / 0.026	N/A	<LOQ	<LOQ
Valencene	0.010 / 0.033	N/A	<LOQ	<LOQ
Sabinene	0.004 / 0.014	N/A	ND	ND
α-Phellandrene	0.006 / 0.019	N/A	ND	ND
Δ³-Carene	0.005 / 0.018	N/A	ND	ND
α-Terpinene	0.006 / 0.019	N/A	ND	ND
p-Cymene	0.005 / 0.015	N/A	ND	ND
β-Ocimene	0.005 / 0.018	N/A	ND	ND
γ-Terpinene	0.005 / 0.018	N/A	ND	ND
Isopulegol	0.004 / 0.013	N/A	ND	ND
Camphor	0.005 / 0.015	N/A	ND	ND
Isoborneol	0.003 / 0.011	N/A	ND	ND
Menthol	0.008 / 0.025	N/A	ND	ND
Nerol	0.003 / 0.011	N/A	ND	ND
Pulegone	0.003 / 0.010	N/A	ND	ND
Geraniol	0.002 / 0.007	N/A	ND	ND
Geranyl Acetate	0.004 / 0.012	N/A	ND	ND
Guaiol	0.011 / 0.035	N/A	ND	ND
Cedrol	0.009 / 0.032	N/A	ND	ND
TOTAL			11.052 mg/g	1.1052%

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Pesticide Analysis

Pass

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Category 1 Pesticide Test Results

04/20/2024

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
Aldicarb	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Carbofuran	0.02 / 0.05	≥ LOD	N/A	ND	Pass
Chlordane*	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Chlorfenapyr*	0.03 / 0.10	≥ LOD	N/A	ND	Pass
Chlorpyrifos	0.02 / 0.06	≥ LOD	N/A	ND	Pass
Coumaphos	0.02 / 0.07	≥ LOD	N/A	ND	Pass
Daminozide	0.02 / 0.07	≥ LOD	N/A	ND	Pass
Dichlorvos (DDVP)	0.03 / 0.09	≥ LOD	N/A	ND	Pass
Dimethoate	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Ethoprophos	0.03 / 0.10	≥ LOD	N/A	ND	Pass
Etofenprox	0.02 / 0.06	≥ LOD	N/A	ND	Pass
Fenoxycarb	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Fipronil	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Imazalil	0.02 / 0.06	≥ LOD	N/A	ND	Pass
Methiocarb	0.02 / 0.07	≥ LOD	N/A	ND	Pass
Parathion-methyl	0.03 / 0.10	≥ LOD	N/A	ND	Pass
Mevinphos	0.03 / 0.09	≥ LOD	N/A	ND	Pass
Paclobutrazol	0.02 / 0.05	≥ LOD	N/A	ND	Pass
Propoxur	0.03 / 0.09	≥ LOD	N/A	ND	Pass
Spiroxamine	0.03 / 0.08	≥ LOD	N/A	ND	Pass
Thiacloprid	0.03 / 0.10	≥ LOD	N/A	ND	Pass

Category 2 Pesticide Test Results

04/20/2024

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
Abamectin	0.03 / 0.10	0.1	N/A	ND	Pass
Acephate	0.02 / 0.07	0.1	N/A	ND	Pass
Acequinocyl	0.02 / 0.07	0.1	N/A	ND	Pass
Acetamiprid	0.02 / 0.05	0.1	N/A	ND	Pass
Azoxystrobin	0.02 / 0.07	0.1	N/A	ND	Pass
Bifenazate	0.01 / 0.04	0.1	N/A	ND	Pass
Bifenthrin	0.02 / 0.05	3	N/A	ND	Pass
Boscalid	0.03 / 0.09	0.1	N/A	ND	Pass
Captan	0.19 / 0.57	0.7	N/A	ND	Pass
Carbaryl	0.02 / 0.06	0.5	N/A	ND	Pass
Chlorantraniliprole	0.04 / 0.12	10	N/A	ND	Pass
Clofentezine	0.03 / 0.09	0.1	N/A	ND	Pass
Cyfluthrin	0.12 / 0.38	2	N/A	ND	Pass
Cypermethrin	0.11 / 0.32	1	N/A	ND	Pass
Diazinon	0.02 / 0.05	0.1	N/A	ND	Pass
Dimethomorph	0.03 / 0.09	2	N/A	ND	Pass
Etoxazole	0.02 / 0.06	0.1	N/A	ND	Pass
Fenhexamid	0.03 / 0.09	0.1	N/A	ND	Pass
Fenpyroximate	0.02 / 0.06	0.1	N/A	ND	Pass
Flonicamid	0.03 / 0.10	0.1	N/A	ND	Pass
Fludioxonil	0.03 / 0.10	0.1	N/A	ND	Pass
Hexythiazox	0.02 / 0.07	0.1	N/A	ND	Pass
Imidacloprid	0.04 / 0.11	5	N/A	ND	Pass
Kresoxim-methyl	0.02 / 0.07	0.1	N/A	ND	Pass
Malathion	0.03 / 0.09	0.5	N/A	ND	Pass
Metalaxyl	0.02 / 0.07	2	N/A	ND	Pass
Methomyl	0.03 / 0.10	1	N/A	ND	Pass
Myclobutanil	0.03 / 0.09	0.1	N/A	ND	Pass
Naled	0.02 / 0.07	0.1	N/A	ND	Pass
Oxamyl	0.04 / 0.11	0.5	N/A	ND	Pass
Pentachloronitrobenzene*	0.03 / 0.09	0.1	N/A	ND	Pass
Permethrin	0.04 / 0.12	0.5	N/A	ND	Pass
Phosmet	0.03 / 0.10	0.1	N/A	ND	Pass
Piperonyl Butoxide	0.02 / 0.07	3	N/A	ND	Pass
Prallethrin	0.03 / 0.08	0.1	N/A	ND	Pass
Propiconazole	0.02 / 0.07	0.1	N/A	ND	Pass
Pyrethrins	0.04 / 0.12	0.5	N/A	ND	Pass
Pyridaben	0.02 / 0.07	0.1	N/A	ND	Pass
Spinetoram	0.02 / 0.07	0.1	N/A	ND	Pass
Spinosad	0.02 / 0.07	0.1	N/A	ND	Pass
Spiromesifen	0.02 / 0.05	0.1	N/A	ND	Pass
Spirotetramat	0.02 / 0.06	0.1	N/A	ND	Pass
Tebuconazole	0.02 / 0.07	0.1	N/A	ND	Pass
Thiamethoxam	0.03 / 0.10	5	N/A	ND	Pass
Trifloxystrobin	0.03 / 0.08	0.1	N/A	ND	Pass

Mycotoxin Analysis

Pass

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS

Mycotoxin Test Results

04/20/2024

PASS

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Compound	LOD/LOQ (μg/kg)	Action Limit (μg/kg)	Measurement Uncertainty (μg/kg)	Result (μg/kg)	Result
Aflatoxin B1	2.0 / 6.0		N/A	ND
Aflatoxin B2	1.8 / 5.6		N/A	ND
Aflatoxin G1	1.0 / 3.1		N/A	ND
Aflatoxin G2	1.2 / 3.5		N/A	ND
Total Aflatoxin		20	±	ND	Pass
Ochratoxin A	6.3 / 19.2	20	N/A	ND	Pass

Heavy Metals Analysis

Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

04/20/2024

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
Arsenic	0.02 / 0.1	0.2	N/A	ND	Pass
Cadmium	0.02 / 0.05	0.2	N/A	<LOQ	Pass
Lead	0.04 / 0.1	0.5	N/A	ND	Pass
Mercury	0.002 / 0.01	0.1	N/A	<LOQ	Pass

Microbiology Analysis

Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants

Microbiology Test Results

04/20/2024

PASS

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Compound	Action Limit	Result	Result
Aspergillus flavus	Not Detected in 1g	ND	Pass
Aspergillus fumigatus	Not Detected in 1g	ND	Pass
Aspergillus niger	Not Detected in 1g	ND	Pass
Aspergillus terreus	Not Detected in 1g	ND	Pass
Salmonella spp.	Not Detected in 1g	ND	Pass
Shiga toxin-producing Escherichia coli	Not Detected in 1g	ND	Pass

Foreign Material Analysis

Pass

Visual analysis includes, but is not limited to, sand, soil, cinders, dirt, mold, hair, insect fragments, and mammalian excreta.

Method: QSP 1226 - Analysis of Foreign Material in Cannabis and Cannabis Products

Foreign Material Test Results

04/20/2024

PASS

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Compound	Action Limit	Result	Result
Total Sample Area Covered by Sand, Soil, Cinders, or Dirt	>25%	None	Pass
Total Sample Area Covered by Mold	>25%	None	Pass
Total Sample Area Covered by an Imbedded Foreign Material	>25%	None	Pass
Insect Fragment Count	> 1 per 3 grams	0.0	Pass
Hair Count	> 1 per 3 grams	0.0	Pass
Mammalian Excreta Count	> 1 per 3 grams	0.0	Pass

Water Activity Analysis

Pass

Method: QSP 1227 - Analysis of Water Activity in Cannabis and Cannabis Products

Water Activity Test Results

04/20/2024

PASS

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Compound	LOD/LOQ (Aw)	Action Limit (Aw)	Measurement Uncertainty (Aw)	Result (Aw)	Result
Water Activity	0.030 / 0.15	0.65	±0.003	0.49	Pass

COA ID: 240418V004-001

These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

Sample Certification: California Code of Regulations Title 4 Division 19. Department of Cannabis Control Business and Professions Code. Reference: Sections 26100, 26104 and 26110, Business and Professions Code.

Decision Rule: Statements of conformity (e.g. Pass/Fail) to specifications are made in this report without taking measurement uncertainty into account. Where statements of conformity are made in this report, the following decision rules are applied: PASS - Results within limits/specifications, FAIL - Results exceed limits/specifications.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT)