Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

Stage 2 - Distillate

Concentrate, Product Inhalable

Date Issued:

10/05/2022

Total THC 87.781%
Total CBD 0.472%
Sum Cannabinoids 95.40%
Total Cannabinoids 95.40%
Total Terpenoids 0.1002%
PhytoFacts®
Top 3 Terpenoids
  1. α-Bisabolol 0.0882%
  2. Caryophyllene Oxide 0.0120%
  3. Cedrol <LOQ

Sample Information

Sample Details

Sample ID:220930S054

Batch Number:MPP-0251

Cultivator / Manufacturer

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Distributor / Tested For

Show Details

PhytoFacts® Report

aroma
flavor
effect

The PhytoFacts chemometric report provides additional cannabinoid and terpenoid details, including dominant terpenes, entourage effects, aroma, flavor, and more.

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Cannabinoid Analysis - Summary

Total THC: 87.781%

Total CBD: 0.472%

Sum of Cannabinoids: 95.40%

Total Cannabinoids: 95.40%

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

Total Terpenoids: 0.1002%

 
 
 

1

α-Bisabolol (0.0882%)

2

Caryophyllene Oxide (0.0120%)

3

Cedrol (<LOQ)

Safety Analysis - Summary

Pesticides: Fail

Residual Solvents: Pass

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 87.781%

(Δ9-THC+0.877*THCa)

Total CBD: 0.472%

(CBD+0.877*CBDa)

Total Cannabinoids: 95.40%

Total CBG: 2.566%

Total CBG (CBG+0.877*CBGa)

Total THCV: 0.75%

Total THCV (THCV+0.877*THCVa)

Total CBC: 1.70%

Total CBC (CBC+0.877*CBCa)

Total CBDV: ND

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

10/03/2022

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
Δ9 Tetrahydrocannabinol (Δ9THC) 0.06 / 0.26 ±23.525 877.81 87.781
Cannabigerol (CBG) 0.06 / 0.19 ±0.788 25.66 2.566
Cannabinol (CBN) 0.1 / 0.3 ±1.08 21.3 2.13
Cannabichromene (CBC) 0.2 / 0.5 ±0.39 17.0 1.70
Tetrahydrocannabivarin (THCV) 0.1 / 0.2 ±0.29 7.5 0.75
Cannabidiol (CBD) 0.07 / 0.29 ±0.170 4.72 0.472
Cannabicyclol (CBL) 0.06 / 0.24 N/A ND ND
Cannabichromenic Acid (CBCa) 0.07 / 0.28 N/A ND ND
Cannabidivarin (CBDV) 0.04 / 0.15 N/A ND ND
Cannabidiolic Acid (CBDa) 0.02 / 0.19 N/A ND ND
Cannabigerolic Acid (CBGa) 0.1 / 0.2 N/A ND ND
Tetrahydrocannabinolic Acid (THCa) 0.05 / 0.14 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.03 / 0.53 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.07 / 0.20 N/A ND ND
∆8 Tetrahydrocannabinol (Δ8THC) 0.1 / 0.4 N/A ND ND
SUM OF CANNABINOIDS 954.0 mg/g 95.40%
Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

View PhytoFacts COA

See a visual representation of this sample's cannabinoid and terpenoid properties, including entourage effects, aroma, and flavor profile.

Summary

Total Terpenoids (mg/g): 1.002 mg/g

Total Terpenoids (%): 0.1002%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume. To see more detail for terpenoid content, view the PhytoFacts report.

  1. α-Bisabolol 0.0882%

    A sesquiterpene alcohol with a fragrance that can be described as floral, peppery, sweet and clean. Found in chamomile, figwort, yarrow, skullcaps, lavender, ironwort, germander...etc.

  2. Caryophyllene Oxide 0.0120%

    A sesquiterpene epoxide with a fragrance that can be described as fresh, sweet, dry, woody and spicy. It is a component used by drug-sniffing dogs to identify cannabis. It does interact with the endocannabinoid system. Found in field wormwood, salt heliotrope, cinnamon, sticky sage, basil, waterbessie...etc.

  3. Cedrol <LOQ

    A sesquiterpene alcohol with a fragrance that can be described as dry, sweet, floral and woody. Found in conifers, cumin, apple, rosemary, sage, tea tree, lilac, nutmeg...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

10/03/2022

Result Views

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
α-Bisabolol 0.008 / 0.026 ±0.0366 0.882 0.0882
Caryophyllene Oxide 0.010 / 0.033 ±0.0043 0.120 0.0120
Cedrol 0.008 / 0.027 N/A <LOQ <LOQ
Guaiol 0.009 / 0.030 N/A <LOQ <LOQ
Nerolidol 0.006 / 0.019 N/A <LOQ <LOQ
Nerol 0.003 / 0.011 N/A ND ND
Borneol 0.005 / 0.016 N/A ND ND
Camphor 0.006 / 0.019 N/A ND ND
Fenchol 0.010 / 0.034 N/A ND ND
Menthol 0.008 / 0.025 N/A ND ND
Myrcene 0.008 / 0.025 N/A ND ND
Camphene 0.005 / 0.015 N/A ND ND
Fenchone 0.009 / 0.028 N/A ND ND
Geraniol 0.002 / 0.007 N/A ND ND
Limonene 0.005 / 0.016 N/A ND ND
Linalool 0.009 / 0.032 N/A ND ND
Pulegone 0.003 / 0.011 N/A ND ND
Sabinene 0.004 / 0.014 N/A ND ND
p-Cymene 0.005 / 0.016 N/A ND ND
Terpineol 0.009 / 0.031 N/A ND ND
Valencene 0.009 / 0.030 N/A ND ND
Eucalyptol 0.006 / 0.018 N/A ND ND
Isoborneol 0.004 / 0.012 N/A ND ND
Isopulegol 0.005 / 0.016 N/A ND ND
Citronellol 0.003 / 0.010 N/A ND ND
Terpinolene 0.008 / 0.026 N/A ND ND
β-Pinene 0.004 / 0.014 N/A ND ND
α-Pinene 0.005 / 0.017 N/A ND ND
β-Ocimene 0.006 / 0.020 N/A ND ND
Δ3-Carene 0.005 / 0.018 N/A ND ND
α-Cedrene 0.005 / 0.016 N/A ND ND
α-Humulene 0.009 / 0.029 N/A ND ND
Geranyl Acetate 0.004 / 0.014 N/A ND ND
α-Terpinene 0.005 / 0.017 N/A ND ND
γ-Terpinene 0.006 / 0.018 N/A ND ND
Sabinene Hydrate 0.006 / 0.022 N/A ND ND
α-Phellandrene 0.006 / 0.020 N/A ND ND
β-Caryophyllene 0.004 / 0.012 N/A ND ND
trans-β-Farnesene 0.008 / 0.025 N/A ND ND
TOTAL 1.002 mg/g 0.1002%
Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

10/03/2022

FAIL

Swipe left on table to see additional columns

Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Aldicarb 0.03 / 0.08 ≥ LOD N/A ND Pass
Carbofuran 0.02 / 0.05 ≥ LOD N/A ND Pass
Chlordane* 0.03 / 0.08 ≥ LOD N/A ND Pass
Chlorfenapyr* 0.03 / 0.10 ≥ LOD N/A <LOQ Fail
Chlorpyrifos 0.02 / 0.06 ≥ LOD N/A ND Pass
Coumaphos 0.02 / 0.07 ≥ LOD N/A ND Pass
Daminozide 0.02 / 0.07 ≥ LOD N/A ND Pass
Dichlorvos (DDVP) 0.03 / 0.09 ≥ LOD N/A ND Pass
Dimethoate 0.03 / 0.08 ≥ LOD N/A ND Pass
Ethoprophos 0.03 / 0.10 ≥ LOD N/A ND Pass
Etofenprox 0.02 / 0.06 ≥ LOD N/A ND Pass
Fenoxycarb 0.03 / 0.08 ≥ LOD N/A ND Pass
Fipronil 0.03 / 0.08 ≥ LOD N/A ND Pass
Imazalil 0.02 / 0.06 ≥ LOD N/A ND Pass
Methiocarb 0.02 / 0.07 ≥ LOD N/A ND Pass
Mevinphos 0.03 / 0.09 ≥ LOD N/A ND Pass
Paclobutrazol 0.02 / 0.05 ≥ LOD N/A ND Pass
Parathion-methyl 0.03 / 0.10 ≥ LOD N/A ND Pass
Propoxur 0.03 / 0.09 ≥ LOD N/A ND Pass
Spiroxamine 0.03 / 0.08 ≥ LOD N/A ND Pass
Thiacloprid 0.03 / 0.10 ≥ LOD N/A ND Pass
Abamectin 0.03 / 0.10 0.1 N/A ND Pass
Acephate 0.02 / 0.07 0.1 N/A ND Pass
Acequinocyl 0.02 / 0.07 0.1 N/A ND Pass
Acetamiprid 0.02 / 0.05 0.1 N/A ND Pass
Azoxystrobin 0.02 / 0.07 0.1 N/A ND Pass
Bifenazate 0.01 / 0.04 0.1 ±>0.168 >4.00 Fail
Bifenthrin 0.02 / 0.05 3 ±0.015 0.38 Pass
Boscalid 0.03 / 0.09 0.1 N/A ND Pass
Captan 0.19 / 0.57 0.7 N/A ND Pass
Carbaryl 0.02 / 0.06 0.5 N/A ND Pass
Chlorantraniliprole 0.04 / 0.12 10 N/A ND Pass
Clofentezine 0.03 / 0.09 0.1 N/A ND Pass
Cyfluthrin 0.12 / 0.38 2 N/A ND Pass
Cypermethrin 0.11 / 0.32 1 N/A ND Pass
Diazinon 0.02 / 0.05 0.1 N/A ND Pass
Dimethomorph 0.03 / 0.09 2 N/A ND Pass
Etoxazole 0.02 / 0.06 0.1 N/A ND Pass
Fenhexamid 0.03 / 0.09 0.1 N/A ND Pass
Fenpyroximate 0.02 / 0.06 0.1 N/A ND Pass
Flonicamid 0.03 / 0.10 0.1 N/A ND Pass
Fludioxonil 0.03 / 0.10 0.1 N/A ND Pass
Hexythiazox 0.02 / 0.07 0.1 N/A ND Pass
Imidacloprid 0.04 / 0.11 5 ±0.011 0.24 Pass
Kresoxim-methyl 0.02 / 0.07 0.1 N/A ND Pass
Malathion 0.03 / 0.09 0.5 ±>0.151 >4.00 Fail
Metalaxyl 0.02 / 0.07 2 N/A <LOQ Pass
Methomyl 0.03 / 0.10 1 N/A ND Pass
Myclobutanil 0.03 / 0.09 0.1 ±0.061 1.22 Fail
Naled 0.02 / 0.07 0.1 N/A ND Pass
Oxamyl 0.04 / 0.11 0.5 N/A ND Pass
Pentachloronitrobenzene (Quintozene)* 0.03 / 0.09 0.1 N/A ND Pass
Permethrin 0.04 / 0.12 0.5 N/A ND Pass
Phosmet 0.03 / 0.10 0.1 N/A ND Pass
Piperonyl Butoxide 0.02 / 0.07 3 N/A ND Pass
Prallethrin 0.03 / 0.08 0.1 N/A ND Pass
Propiconazole 0.02 / 0.07 0.1 N/A <LOQ Pass
Pyrethrins 0.04 / 0.12 0.5 ±0.016 0.36 Pass
Pyridaben 0.02 / 0.07 0.1 N/A ND Pass
Spinetoram 0.02 / 0.07 0.1 N/A ND Pass
Spinosad 0.02 / 0.07 0.1 N/A ND Pass
Spiromesifen 0.02 / 0.05 0.1 N/A <LOQ Pass
Spirotetramat 0.02 / 0.06 0.1 N/A ND Pass
Tebuconazole 0.02 / 0.07 0.1 N/A <LOQ Pass
Thiamethoxam 0.03 / 0.10 5 N/A ND Pass
Trifloxystrobin 0.03 / 0.08 0.1 N/A ND Pass

Hide Failed Pesticide Details

Fail

Malathion | Trade Names: Fyfanon 440, Karbofos, Cythion, Maltox, Malixol, Cekumal, Elthion, Dielathion, El 4049, Emmaton, Fyfanon, Exathion...etc.; The most commonly used organophosphate insecticide in the U.S. It is non-systemic and also effective against mites and ticks. It is frequently used for mosquito eradication in urban environments. It is moderately toxic to birds and mammals, but highly toxic to aquatic organisms with the notable exception of algae.

Fail

Bifenazate | Trade Names: Floramite, Acramite, Prevamite; A non-systemic insecticide and acaricide, effective against most plant-eating mites. It is highly toxic to mammals and is a known irritant.

Fail

Chlorfenapyr* | Trade Names: Pylon, Phantom, Spectre 2 SC, Piston, Pirate, Shark; A type of pesticide called a "pro-insecticide", which means that the actual active insecticide is a metabolite formed within the host. It is also an effective miticide and displays limited systemic activity. It is not approved for use on food-crops in the U.S.

Fail

Myclobutanil | Trade Names: Eagle, Nova, Rally, Systhane 20 EW, Masalon...etc.; A widely used systemic fungicide that is effective against Ascomycetes, Deuteromycota, and Basidiomycetes species. Since it has a long residual effect, it can also be applied prior to contraction as a protective. When heated, myclobutanil forms harmful degradation products including carbon monoxide, carbon dioxide, hydrogen chloride, hydrogen cyanide, and nitrogen oxides.

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

10/02/2022

PASS

Swipe left on table to see additional columns

Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
1,2-Dichloroethane 0.05 / 0.1 1 N/A ND Pass
Benzene 0.03 / 0.09 1 N/A ND Pass
Chloroform 0.1 / 0.2 1 N/A ND Pass
Dichloromethane (Methylene Chloride) 0.3 / 0.9 1 N/A ND Pass
Ethylene Oxide 0.3 / 0.8 1 N/A ND Pass
Trichloroethylene 0.1 / 0.3 1 N/A ND Pass
2-Propanol (Isopropyl Alcohol) 10 / 40 5000 N/A ND Pass
Acetone 20 / 50 5000 N/A ND Pass
Acetonitrile 2 / 7 410 N/A ND Pass
Ethanol 20 / 50 5000 N/A ND Pass
Ethyl Acetate 20 / 60 5000 N/A ND Pass
Ethyl Ether 20 / 50 5000 N/A ND Pass
Methanol 50 / 200 3000 N/A ND Pass
n-Butane 10 / 50 5000 N/A ND Pass
n-Heptane 20 / 60 5000 N/A ND Pass
n-Hexane 2 / 5 290 N/A ND Pass
n-Pentane 20 / 50 5000 N/A ND Pass
Propane 10 / 20 5000 N/A ND Pass
Toluene 7 / 21 890 N/A ND Pass
Total Xylenes 50 / 160 2170 N/A ND Pass

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