Stage 1- Terpene Heads

Certificate of Analysis

HEMP QUALITY ASSURANCE TEST

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Sample Name:

Stage 1- Terpene Heads

Concentrate, Product Inhalable

Total THC 32.753%

Total CBD Not Detected

Sum Cannabinoids 35.27%

Total Cannabinoids 35.27%

Total Terpenoids 12.3437%
PhytoFacts^®

Top 3 Terpenoids

α-Bisabolol 5.1007%
β-Caryophyllene 2.3059%
Caryophyllene Oxide 1.7160%

Sample Information

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Sample Details

Sample ID:220930S048

Batch Number:MPP-0245

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Cultivator / Manufacturer

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PhytoFacts® Report

aroma

flavor

effect

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The PhytoFacts chemometric report provides additional cannabinoid and terpenoid details, including dominant terpenes, entourage effects, aroma, flavor, and more.

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Cannabinoid Analysis - Summary

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Total THC: 32.753%

Total CBD: Not Detected

Sum of Cannabinoids: 35.27%

Total Cannabinoids: 35.27%

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ⁹-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ⁹-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ⁸-THC + CBL + CBN

Total Cannabinoids = (Δ⁹-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ⁸-THC + CBL + CBN

Why are Sum of Cannabinoids and Total Cannabinoids calculated separately?

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

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Total Terpenoids: 12.3437%

α-Bisabolol (5.1007%)

β-Caryophyllene (2.3059%)

Caryophyllene Oxide (1.7160%)

Safety Analysis - Summary

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Residual Solvents: Pass

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Cannabinoid Analysis

Tested

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 32.753%

(Δ⁹-THC+0.877*THCa)

Total CBD: Not Detected

(CBD+0.877*CBDa)

Total Cannabinoids: 35.27%

Total CBG: 0.870%

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 0.96%

Total CBC (CBC+0.877*CBCa)

Total CBDV: ND

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

10/03/2022

Result Views

Table Pie Chart

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Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
Δ9 Tetrahydrocannabinol (Δ9THC)	0.06 / 0.26	±8.778	327.53	32.753
Cannabichromene (CBC)	0.2 / 0.5	±0.22	9.6	0.96
Cannabigerol (CBG)	0.06 / 0.19	±0.267	8.70	0.870
Cannabinol (CBN)	0.1 / 0.3	±0.35	6.9	0.69
Cannabidiol (CBD)	0.07 / 0.29	N/A	ND	ND
Cannabicyclol (CBL)	0.06 / 0.24	N/A	ND	ND
Cannabichromenic Acid (CBCa)	0.07 / 0.28	N/A	ND	ND
Cannabidivarin (CBDV)	0.04 / 0.15	N/A	ND	ND
Cannabidiolic Acid (CBDa)	0.02 / 0.19	N/A	ND	ND
Cannabigerolic Acid (CBGa)	0.1 / 0.2	N/A	ND	ND
Tetrahydrocannabivarin (THCV)	0.1 / 0.2	N/A	ND	ND
Tetrahydrocannabinolic Acid (THCa)	0.05 / 0.14	N/A	ND	ND
Cannabidivarinic Acid (CBDVa)	0.03 / 0.53	N/A	ND	ND
Tetrahydrocannabivarinic Acid (THCVa)	0.07 / 0.20	N/A	ND	ND
∆8 Tetrahydrocannabinol (Δ8THC)	0.1 / 0.4	N/A	ND	ND
SUM OF CANNABINOIDS			352.7 mg/g	35.27%

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpenoid Analysis

Tested

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

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See a visual representation of this sample's cannabinoid and terpenoid properties, including entourage effects, aroma, and flavor profile.

Summary

Total Terpenoids (mg/g): 123.437 mg/g

Total Terpenoids (%): 12.3437%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume. To see more detail for terpenoid content, view the PhytoFacts report.

α-Bisabolol 5.1007%
A sesquiterpene alcohol with a fragrance that can be described as floral, peppery, sweet and clean. Found in chamomile, figwort, yarrow, skullcaps, lavender, ironwort, germander...etc.

β-Caryophyllene 2.3059%
A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB² receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

Caryophyllene Oxide 1.7160%
A sesquiterpene epoxide with a fragrance that can be described as fresh, sweet, dry, woody and spicy. It is a component used by drug-sniffing dogs to identify cannabis. It does interact with the endocannabinoid system. Found in field wormwood, salt heliotrope, cinnamon, sticky sage, basil, waterbessie...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

10/03/2022

Result Views

Table Bar Graph

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Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
α-Bisabolol	0.008 / 0.026	±2.1168	51.007	5.1007
β-Caryophyllene	0.004 / 0.012	±0.6387	23.059	2.3059
Caryophyllene Oxide	0.010 / 0.033	±0.6143	17.160	1.7160
Guaiol	0.009 / 0.030	±0.4078	11.112	1.1112
α-Humulene	0.009 / 0.029	±0.2615	10.459	1.0459
Terpineol	0.009 / 0.031	±0.1145	2.395	0.2395
trans-β-Farnesene	0.008 / 0.025	±0.0657	2.382	0.2382
Linalool	0.009 / 0.032	±0.0677	2.288	0.2288
Valencene	0.009 / 0.030	±0.0615	1.148	0.1148
Fenchol	0.010 / 0.034	±0.0295	0.980	0.0980
Borneol	0.005 / 0.016	±0.0159	0.487	0.0487
Citronellol	0.003 / 0.010	±0.0097	0.256	0.0256
Geranyl Acetate	0.004 / 0.014	±0.0065	0.200	0.0200
Geraniol	0.002 / 0.007	±0.0062	0.180	0.0180
Limonene	0.005 / 0.016	±0.0019	0.173	0.0173
Fenchone	0.009 / 0.028	±0.0016	0.072	0.0072
Nerol	0.003 / 0.011	±0.0011	0.032	0.0032
Eucalyptol	0.006 / 0.018	±0.0005	0.025	0.0025
α-Cedrene	0.005 / 0.016	±0.0005	0.022	0.0022
Pulegone	0.003 / 0.011	N/A	<LOQ	<LOQ
Sabinene Hydrate	0.006 / 0.022	N/A	<LOQ	<LOQ
Cedrol	0.008 / 0.027	N/A	ND	ND
Camphor	0.006 / 0.019	N/A	ND	ND
Menthol	0.008 / 0.025	N/A	ND	ND
Myrcene	0.008 / 0.025	N/A	ND	ND
Camphene	0.005 / 0.015	N/A	ND	ND
Sabinene	0.004 / 0.014	N/A	ND	ND
p-Cymene	0.005 / 0.016	N/A	ND	ND
Nerolidol	0.006 / 0.019	N/A	ND	ND
Isoborneol	0.004 / 0.012	N/A	ND	ND
Isopulegol	0.005 / 0.016	N/A	ND	ND
Terpinolene	0.008 / 0.026	N/A	ND	ND
β-Pinene	0.004 / 0.014	N/A	ND	ND
α-Pinene	0.005 / 0.017	N/A	ND	ND
β-Ocimene	0.006 / 0.020	N/A	ND	ND
Δ³-Carene	0.005 / 0.018	N/A	ND	ND
α-Terpinene	0.005 / 0.017	N/A	ND	ND
γ-Terpinene	0.006 / 0.018	N/A	ND	ND
α-Phellandrene	0.006 / 0.020	N/A	ND	ND
TOTAL			123.437 mg/g	12.3437%

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Residual Solvents Analysis

Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

10/02/2022

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
1,2-Dichloroethane	0.05 / 0.1	1	N/A	ND	Pass
Benzene	0.03 / 0.09	1	N/A	ND	Pass
Chloroform	0.1 / 0.2	1	N/A	ND	Pass
Dichloromethane (Methylene Chloride)	0.3 / 0.9	1	N/A	ND	Pass
Ethylene Oxide	0.3 / 0.8	1	N/A	ND	Pass
Trichloroethylene	0.1 / 0.3	1	N/A	ND	Pass
2-Propanol (Isopropyl Alcohol)	10 / 40	5000	N/A	ND	Pass
Acetone	20 / 50	5000	±1.7	51	Pass
Acetonitrile	2 / 7	410	N/A	ND	Pass
Ethanol	20 / 50	5000	N/A	ND	Pass
Ethyl Acetate	20 / 60	5000	N/A	ND	Pass
Ethyl Ether	20 / 50	5000	N/A	ND	Pass
Methanol	50 / 200	3000	N/A	ND	Pass
n-Butane	10 / 50	5000	N/A	ND	Pass
n-Heptane	20 / 60	5000	N/A	ND	Pass
n-Hexane	2 / 5	290	N/A	ND	Pass
n-Pentane	20 / 50	5000	N/A	ND	Pass
Propane	10 / 20	5000	N/A	ND	Pass
Toluene	7 / 21	890	N/A	ND	Pass
Total Xylenes	50 / 160	2170	N/A	ND	Pass

COA ID: 220930S048-001

These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

Sample Certification: California Code of Regulations Title 4 Division 19. Department of Cannabis Control Business and Professions Code. Reference: Sections 26100, 26104 and 26110, Business and Professions Code.

Decision Rule: Statements of conformity (e.g. Pass/Fail) to specifications are made in this report without taking measurement uncertainty into account. Where statements of conformity are made in this report, the following decision rules are applied: PASS - Results within limits/specifications, FAIL - Results exceed limits/specifications.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT), μg/g = ppm, μg/kg = ppb