Stage 1- Terpene Heads

Certificate of Analysis

HEMP QUALITY ASSURANCE TEST

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Sample Name:

Stage 1- Terpene Heads

Other

Total THC 29.3696%

Total CBD Not Detected

Sum Cannabinoids 31.3054%

Total Cannabinoids 31.3054%

Total Terpenoids 10.6007%

Top 3 Terpenoids

α-Bisabolol 2.9796%
β-Caryophyllene 2.9265%
α-Humulene 1.1650%

Sample Information

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Sample Details

Sample ID:220930S046

Batch Number:MPP-0243

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Cannabinoid Analysis - Summary

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Total THC: 29.3696%

Total CBD: Not Detected

Sum of Cannabinoids: 31.3054%

Total Cannabinoids: 31.3054%

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ⁹-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ⁹-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ⁸-THC + CBL + CBN

Total Cannabinoids = (Δ⁹-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ⁸-THC + CBL + CBN

Why are Sum of Cannabinoids and Total Cannabinoids calculated separately?

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

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Total Terpenoids: 10.6007%

α-Bisabolol (2.9796%)

β-Caryophyllene (2.9265%)

α-Humulene (1.1650%)

Safety Analysis - Summary

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Residual Solvents: Pass

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Cannabinoid Analysis

Tested

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 29.3696%

(Δ⁹-THC+0.877*THCa)

Total CBD: Not Detected

(CBD+0.877*CBDa)

Total Cannabinoids: 31.3054%

Total CBG: 0.4819%

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 0.7722%

Total CBC (CBC+0.877*CBCa)

Total CBDV: ND

Total CBDV (CBDV+0.877*CBDVa)

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The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

10/03/2022

Result Views

Table Pie Chart

Swipe left on table to see additional columns

Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
Δ9 Tetrahydrocannabinol (Δ9THC)	0.040 / 0.280	±16.1239	293.696	29.3696
Cannabichromene (CBC)	0.003 / 0.010	±0.2486	7.722	0.7722
Cannabinol (CBN)	0.001 / 0.007	±0.1755	6.114	0.6114
Cannabigerol (CBG)	0.002 / 0.006	±0.2337	4.819	0.4819
Cannabicyclol (CBL)	0.003 / 0.010	±0.0259	0.703	0.0703
Cannabidiol (CBD)	0.004 / 0.011	N/A	ND	ND
Cannabichromenic Acid (CBCa)	0.001 / 0.015	N/A	ND	ND
Cannabidivarin (CBDV)	0.002 / 0.012	N/A	ND	ND
Cannabidiolic Acid (CBDa)	0.001 / 0.026	N/A	ND	ND
Cannabigerolic Acid (CBGa)	0.002 / 0.007	N/A	ND	ND
Tetrahydrocannabivarin (THCV)	0.002 / 0.012	N/A	ND	ND
Tetrahydrocannabinolic Acid (THCa)	0.020 / 0.100	N/A	ND	ND
Cannabidivarinic Acid (CBDVa)	0.001 / 0.018	N/A	ND	ND
Tetrahydrocannabivarinic Acid (THCVa)	0.002 / 0.019	N/A	ND	ND
∆8 Tetrahydrocannabinol (Δ8THC)	0.01 / 0.02	N/A	ND	ND
SUM OF CANNABINOIDS			313.054 mg/g	31.3054%

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpenoid Analysis

Tested

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

Summary

Total Terpenoids (mg/g): 106.007 mg/g

Total Terpenoids (%): 10.6007%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume.

α-Bisabolol 2.9796%
A sesquiterpene alcohol with a fragrance that can be described as floral, peppery, sweet and clean. Found in chamomile, figwort, yarrow, skullcaps, lavender, ironwort, germander...etc.

β-Caryophyllene 2.9265%
A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB² receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

α-Humulene 1.1650%
Also known as α-caryophyllene, it is an isomer of the sesquiterpene β-Caryophyllene which frequently occurs in nature with many aromatic plants across the globe. It has a fragrance that can be described as earthy or musky with spicy undertones. Found in hops, forskohlii, skullcaps, basil, nutmeg, cloves, sage, cotton, tamarind, black pepper, guava, Scotch pine...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

10/03/2022

Result Views

Table Bar Graph

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Compound	LOD/LOQ (mg/g)	Measurement Uncertainty (mg/g)	Result (mg/g)	Result (%)
α-Bisabolol	0.008 / 0.026	±1.2365	29.796	2.9796
β-Caryophyllene	0.004 / 0.012	±0.8106	29.265	2.9265
α-Humulene	0.009 / 0.029	±0.2912	11.650	1.1650
Caryophyllene Oxide	0.010 / 0.033	±0.3957	11.053	1.1053
Guaiol	0.009 / 0.030	±0.2419	6.591	0.6591
Linalool	0.009 / 0.032	±0.1402	4.737	0.4737
trans-β-Farnesene	0.008 / 0.025	±0.1106	4.007	0.4007
Terpineol	0.009 / 0.031	±0.1686	3.528	0.3528
Fenchol	0.010 / 0.034	±0.0545	1.811	0.1811
Valencene	0.009 / 0.030	±0.0605	1.129	0.1129
Borneol	0.005 / 0.016	±0.0254	0.778	0.0778
Limonene	0.005 / 0.016	±0.0042	0.382	0.0382
Citronellol	0.003 / 0.010	±0.0129	0.339	0.0339
Geraniol	0.002 / 0.007	±0.0110	0.321	0.0321
Geranyl Acetate	0.004 / 0.014	±0.0090	0.277	0.0277
Fenchone	0.009 / 0.028	±0.0024	0.106	0.0106
Myrcene	0.008 / 0.025	±0.0006	0.065	0.0065
Terpinolene	0.008 / 0.026	±0.0007	0.046	0.0046
Nerol	0.003 / 0.011	±0.0014	0.041	0.0041
Eucalyptol	0.006 / 0.018	±0.0008	0.039	0.0039
Sabinene Hydrate	0.006 / 0.022	±0.0008	0.026	0.0026
Pulegone	0.003 / 0.011	±0.0006	0.020	0.0020
Menthol	0.008 / 0.025	N/A	<LOQ	<LOQ
Isoborneol	0.004 / 0.012	N/A	<LOQ	<LOQ
β-Pinene	0.004 / 0.014	N/A	<LOQ	<LOQ
β-Ocimene	0.006 / 0.020	N/A	<LOQ	<LOQ
Cedrol	0.008 / 0.027	N/A	ND	ND
Camphor	0.006 / 0.019	N/A	ND	ND
Camphene	0.005 / 0.015	N/A	ND	ND
Sabinene	0.004 / 0.014	N/A	ND	ND
p-Cymene	0.005 / 0.016	N/A	ND	ND
Nerolidol	0.006 / 0.019	N/A	ND	ND
Isopulegol	0.005 / 0.016	N/A	ND	ND
α-Pinene	0.005 / 0.017	N/A	ND	ND
Δ³-Carene	0.005 / 0.018	N/A	ND	ND
α-Cedrene	0.005 / 0.016	N/A	ND	ND
α-Terpinene	0.005 / 0.017	N/A	ND	ND
γ-Terpinene	0.006 / 0.018	N/A	ND	ND
α-Phellandrene	0.006 / 0.020	N/A	ND	ND
TOTAL			106.007 mg/g	10.6007%

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Residual Solvents Analysis

Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

10/02/2022

PASS

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Compound	LOD/LOQ (μg/g)	Action Limit (μg/g)	Measurement Uncertainty (μg/g)	Result (μg/g)	Result
1,2-Dichloroethane	0.05 / 0.1	1	N/A	ND	Pass
Benzene	0.03 / 0.09	1	N/A	ND	Pass
Chloroform	0.1 / 0.2	1	N/A	ND	Pass
Dichloromethane (Methylene Chloride)	0.3 / 0.9	1	N/A	ND	Pass
Ethylene Oxide	0.3 / 0.8	1	N/A	ND	Pass
Trichloroethylene	0.1 / 0.3	1	N/A	ND	Pass
2-Propanol (Isopropyl Alcohol)	10 / 40	5000	N/A	ND	Pass
Acetone	20 / 50	5000	±1.9	64	Pass
Acetonitrile	2 / 7	410	N/A	ND	Pass
Ethanol	20 / 50	5000	N/A	ND	Pass
Ethyl Acetate	20 / 60	5000	N/A	ND	Pass
Ethyl Ether	20 / 50	5000	N/A	ND	Pass
Methanol	50 / 200	3000	N/A	ND	Pass
n-Butane	10 / 50	5000	N/A	ND	Pass
n-Heptane	20 / 60	5000	N/A	ND	Pass
n-Hexane	2 / 5	290	N/A	ND	Pass
n-Pentane	20 / 50	5000	N/A	ND	Pass
Propane	10 / 20	5000	N/A	ND	Pass
Toluene	7 / 21	890	N/A	ND	Pass
Total Xylenes	50 / 160	2170	N/A	ND	Pass

COA ID: 220930S046-001

These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

Sample Certification: California Code of Regulations Title 4 Division 19. Department of Cannabis Control Business and Professions Code. Reference: Sections 26100, 26104 and 26110, Business and Professions Code.

Decision Rule: Statements of conformity (e.g. Pass/Fail) to specifications are made in this report without taking measurement uncertainty into account. Where statements of conformity are made in this report, the following decision rules are applied: PASS - Results within limits/specifications, FAIL - Results exceed limits/specifications.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT), μg/g = ppm, μg/kg = ppb