Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

Heads Heavy Terps

Other

Date Issued:

11/07/2022

Total THC 26.1839%
Total CBD 0.0808%
Sum Cannabinoids 27.133%
Total Cannabinoids 27.133%
Total Terpenoids 18.2490%
Top 3 Terpenoids
  1. β-Caryophyllene 8.7274%
  2. α-Humulene 3.2283%
  3. α-Bisabolol 1.2696%

Sample Information

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Sample Details

Sample ID:221103N040

Batch Number:

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Cultivator / Manufacturer

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Distributor / Tested For

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Cannabinoid Analysis - Summary

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Total THC: 26.1839%

Total CBD: 0.0808%

Sum of Cannabinoids: 27.133%

Total Cannabinoids: 27.133%

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Terpenoid Analysis - Summary

39 tested, Top 3 Highlighted

View Full Results

Total Terpenoids: 18.2490%

 
 
 

1

β-Caryophyllene (8.7274%)

2

α-Humulene (3.2283%)

3

α-Bisabolol (1.2696%)

Safety Analysis - Summary

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Pesticides: Pass

View Complete Test Results:

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Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 26.1839%

(Δ9-THC+0.877*THCa)

Total CBD: 0.0808%

(CBD+0.877*CBDa)

Total Cannabinoids: 27.133%

Total CBG: 0.1246%

Total CBG (CBG+0.877*CBGa)

Total THCV: 0.2618%

Total THCV (THCV+0.877*THCVa)

Total CBC: 0.2720%

Total CBC (CBC+0.877*CBCa)

Total CBDV: ND

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

11/06/2022

Result Views

Table Pie Chart

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g) 		Measurement
Uncertainty
(mg/g) 		Result
(mg/g) 		Result
(%)
Δ9 Tetrahydrocannabinol (Δ9THC) 0.002 / 0.014 ±14.3750 261.839 26.1839
Cannabichromene (CBC) 0.003 / 0.010 ±0.0876 2.720 0.2720
Tetrahydrocannabivarin (THCV) 0.002 / 0.012 ±0.1285 2.618 0.2618
Cannabinol (CBN) 0.001 / 0.007 ±0.0445 1.550 0.1550
Cannabigerol (CBG) 0.002 / 0.006 ±0.0604 1.246 0.1246
Cannabidiol (CBD) 0.004 / 0.011 ±0.0301 0.808 0.0808
∆8 Tetrahydrocannabinol (Δ8THC) 0.01 / 0.02 ±0.027 0.55 0.055
Cannabicyclol (CBL) 0.003 / 0.010 N/A ND ND
Cannabichromenic Acid (CBCa) 0.001 / 0.015 N/A ND ND
Cannabidivarin (CBDV) 0.002 / 0.012 N/A ND ND
Cannabidiolic Acid (CBDa) 0.001 / 0.026 N/A ND ND
Cannabigerolic Acid (CBGa) 0.002 / 0.007 N/A ND ND
Tetrahydrocannabinolic Acid (THCa) 0.001 / 0.005 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.001 / 0.018 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.002 / 0.019 N/A ND ND
SUM OF CANNABINOIDS 271.33 mg/g 27.133%
Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Terpene analysis utilizing gas chromatography-flame ionization detection (GC-FID).

Method: QSP 1192 - Analysis of Terpenoids by GC-FID

Deviations1: See Notes section at bottom.

Summary

Total Terpenoids (mg/g): 182.490 mg/g

Total Terpenoids (%): 18.2490%

Dominant Terpenoids

Below are this sample's 3 most abundant terpenoids by volume.

  1. β-Caryophyllene 8.7274%

    A sesquiterpene with a fragrance that can be described as spicy, woody, dry, dusty and mildly sweet. It was one of the first organic compounds to fully synthesized in a laboratory and plays a role in the endocannabinoid system as it is a functional CB2 receptor agonist. Found in black pepper, clove, hops, rosemary, black-jack, perilla, spicebush, Indian pennywort, celery, frankincense, vitex, parsley, marigold, tamarind...etc.

  2. α-Humulene 3.2283%

    Also known as α-caryophyllene, it is an isomer of the sesquiterpene β-Caryophyllene which frequently occurs in nature with many aromatic plants across the globe. It has a fragrance that can be described as earthy or musky with spicy undertones. Found in hops, forskohlii, skullcaps, basil, nutmeg, cloves, sage, cotton, tamarind, black pepper, guava, Scotch pine...etc.

  3. α-Bisabolol 1.2696%

    A sesquiterpene alcohol with a fragrance that can be described as floral, peppery, sweet and clean. Found in chamomile, figwort, yarrow, skullcaps, lavender, ironwort, germander...etc.

Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Terpenoid Test Results

11/06/2022

Result Views

Table Bar Graph

Swipe left on table to see additional columns

Compound LOD/LOQ
(mg/g) 		Measurement
Uncertainty
(mg/g) 		Result
(mg/g) 		Result
(%)
β-Caryophyllene 0.004 / 0.012 ±2.4175 87.274 8.7274
α-Humulene 0.009 / 0.029 ±0.8071 32.283 3.2283
α-Bisabolol 0.008 / 0.026 ±0.5269 12.696 1.2696
trans-β-Farnesene 0.008 / 0.025 ±0.3325 12.046 1.2046
Guaiol 0.009 / 0.030 ±0.3592 9.788 0.9788
Linalool 0.009 / 0.032 ±0.2845 9.613 0.9613
Nerolidol 0.006 / 0.019 ±0.3659 7.467 0.7467
Fenchol 0.010 / 0.034 ±0.0892 2.962 0.2962
Terpineol 0.009 / 0.031 ±0.1354 2.832 0.2832
Limonene 0.005 / 0.016 ±0.0264 2.378 0.2378
Borneol 0.005 / 0.016 ±0.0296 0.904 0.0904
Valencene 0.009 / 0.030 ±0.0482 0.900 0.0900
Caryophyllene Oxide 0.010 / 0.033 ±0.0221 0.616 0.0616
Myrcene 0.008 / 0.025 ±0.0026 0.258 0.0258
Geraniol 0.002 / 0.007 ±0.0047 0.136 0.0136
Citronellol 0.003 / 0.010 ±0.0046 0.120 0.0120
Fenchone 0.009 / 0.028 ±0.0019 0.084 0.0084
Nerol 0.003 / 0.011 ±0.0017 0.048 0.0048
Menthol 0.008 / 0.025 ±0.0015 0.047 0.0047
Eucalyptol 0.006 / 0.018 ±0.0007 0.038 0.0038
Camphor 0.006 / 0.019 N/A <LOQ <LOQ
Cedrol 0.008 / 0.027 N/A ND ND
Camphene 0.005 / 0.015 N/A ND ND
Pulegone 0.003 / 0.011 N/A ND ND
Sabinene 0.004 / 0.014 N/A ND ND
p-Cymene 0.005 / 0.016 N/A ND ND
Isoborneol 0.004 / 0.012 N/A ND ND
Isopulegol 0.005 / 0.016 N/A ND ND
Terpinolene 0.008 / 0.026 N/A ND ND
β-Pinene 0.004 / 0.014 N/A ND ND
α-Pinene 0.005 / 0.017 N/A ND ND
β-Ocimene 0.006 / 0.020 N/A ND ND
Δ3-Carene 0.005 / 0.018 N/A ND ND
α-Cedrene 0.005 / 0.016 N/A ND ND
Geranyl Acetate 0.004 / 0.014 N/A ND ND
α-Terpinene 0.005 / 0.017 N/A ND ND
γ-Terpinene 0.006 / 0.018 N/A ND ND
Sabinene Hydrate 0.006 / 0.022 N/A ND ND
α-Phellandrene 0.006 / 0.020 N/A ND ND
TOTAL 182.490 mg/g 18.2490%
Learn more

Terpenoid analysis is crucial for differentiating between strains of cannabis, as terpenoids have a major influence on the medical and psychological effects of a plant. The relationship between cannabinoids and terpeneoids is known as the "entourage effect."

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

11/07/2022

PASS

Swipe left on table to see additional columns

Compound LOD/LOQ
(μg/g) 		Action Limit
(μg/g) 		Measurement
Uncertainty
(μg/g) 		Result
(μg/g) 		Result
Aldicarb 0.03 / 0.08 ≥ LOD N/A ND Pass
Carbofuran 0.02 / 0.05 ≥ LOD N/A ND Pass
Chlordane* 0.03 / 0.08 ≥ LOD N/A ND Pass
Chlorfenapyr* 0.03 / 0.10 ≥ LOD N/A ND Pass
Chlorpyrifos 0.02 / 0.06 ≥ LOD N/A ND Pass
Coumaphos 0.02 / 0.07 ≥ LOD N/A ND Pass
Daminozide 0.02 / 0.07 ≥ LOD N/A ND Pass
Dichlorvos (DDVP) 0.03 / 0.09 ≥ LOD N/A ND Pass
Dimethoate 0.03 / 0.08 ≥ LOD N/A ND Pass
Ethoprophos 0.03 / 0.10 ≥ LOD N/A ND Pass
Etofenprox 0.02 / 0.06 ≥ LOD N/A ND Pass
Fenoxycarb 0.03 / 0.08 ≥ LOD N/A ND Pass
Fipronil 0.03 / 0.08 ≥ LOD N/A ND Pass
Imazalil 0.02 / 0.06 ≥ LOD N/A ND Pass
Methiocarb 0.02 / 0.07 ≥ LOD N/A ND Pass
Mevinphos 0.03 / 0.09 ≥ LOD N/A ND Pass
Paclobutrazol 0.02 / 0.05 ≥ LOD N/A ND Pass
Parathion-methyl 0.03 / 0.10 ≥ LOD N/A ND Pass
Propoxur 0.03 / 0.09 ≥ LOD N/A ND Pass
Spiroxamine 0.03 / 0.08 ≥ LOD N/A ND Pass
Thiacloprid 0.03 / 0.10 ≥ LOD N/A ND Pass
Abamectin 0.03 / 0.10 0.3 N/A ND Pass
Acephate 0.02 / 0.07 5 N/A ND Pass
Acequinocyl 0.02 / 0.07 4 N/A ND Pass
Acetamiprid 0.02 / 0.05 5 N/A ND Pass
Azoxystrobin 0.02 / 0.07 40 N/A ND Pass
Bifenazate 0.01 / 0.04 5 N/A ND Pass
Bifenthrin 0.02 / 0.05 0.5 N/A ND Pass
Boscalid 0.03 / 0.09 10 N/A ND Pass
Captan 0.19 / 0.57 5 N/A ND Pass
Carbaryl 0.02 / 0.06 0.5 N/A ND Pass
Chlorantraniliprole 0.04 / 0.12 40 N/A ND Pass
Clofentezine 0.03 / 0.09 0.5 N/A ND Pass
Cyfluthrin 0.12 / 0.38 1 N/A ND Pass
Cypermethrin 0.11 / 0.32 1 N/A ND Pass
Diazinon 0.02 / 0.05 0.2 N/A ND Pass
Dimethomorph 0.03 / 0.09 20 N/A ND Pass
Etoxazole 0.02 / 0.06 1.5 N/A ND Pass
Fenhexamid 0.03 / 0.09 10 N/A ND Pass
Fenpyroximate 0.02 / 0.06 2 N/A ND Pass
Flonicamid 0.03 / 0.10 2 N/A ND Pass
Fludioxonil 0.03 / 0.10 30 N/A ND Pass
Hexythiazox 0.02 / 0.07 2 N/A ND Pass
Imidacloprid 0.04 / 0.11 3 N/A ND Pass
Kresoxim-methyl 0.02 / 0.07 1 N/A ND Pass
Malathion 0.03 / 0.09 5 N/A ND Pass
Metalaxyl 0.02 / 0.07 15 N/A ND Pass
Methomyl 0.03 / 0.10 0.1 N/A ND Pass
Myclobutanil 0.03 / 0.09 9 N/A ND Pass
Naled 0.02 / 0.07 0.5 N/A ND Pass
Oxamyl 0.04 / 0.11 0.2 N/A ND Pass
Pentachloronitrobenzene (Quintozene)* 0.03 / 0.09 0.2 N/A ND Pass
Permethrin 0.04 / 0.12 20 N/A ND Pass
Phosmet 0.03 / 0.10 0.2 N/A ND Pass
Piperonyl Butoxide 0.02 / 0.07 8 N/A ND Pass
Prallethrin 0.03 / 0.08 0.4 N/A ND Pass
Propiconazole 0.02 / 0.07 20 N/A ND Pass
Pyrethrins 0.04 / 0.12 1 N/A ND Pass
Pyridaben 0.02 / 0.07 3 N/A ND Pass
Spinetoram 0.02 / 0.07 3 N/A ND Pass
Spinosad 0.02 / 0.07 3 N/A ND Pass
Spiromesifen 0.02 / 0.05 12 N/A ND Pass
Spirotetramat 0.02 / 0.06 13 N/A ND Pass
Tebuconazole 0.02 / 0.07 2 N/A ND Pass
Thiamethoxam 0.03 / 0.10 4.5 N/A ND Pass
Trifloxystrobin 0.03 / 0.08 30 N/A ND Pass

Notes

Deviations:

1. Preparation mass outside of normal acceptance range.

COA ID: 221103N040-001

These results relate only to the sample included on this report. This report shall not be reproduced, except in full, without written approval of the laboratory.

Sample Certification: California Code of Regulations Title 4 Division 19. Department of Cannabis Control Business and Professions Code. Reference: Sections 26100, 26104 and 26110, Business and Professions Code.

Decision Rule: Statements of conformity (e.g. Pass/Fail) to specifications are made in this report without taking measurement uncertainty into account. Where statements of conformity are made in this report, the following decision rules are applied: PASS - Results within limits/specifications, FAIL - Results exceed limits/specifications.

References: limit of detection (LOD), limit of quantification (LOQ), not detected (ND), not tested (NT), μg/g = ppm, μg/kg = ppb

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