Certificate of Analysis
REGULATORY COMPLIANCE

Sample Name:

In The Pines - Flower

Flower, Inhalable

Date Issued:

02/07/2020

Overall Batch Result:

Pass

Sum Cannabinoids 36.3842%
Total Cannabinoids 31.9765%
Total THC 30.2295%
Total CBD 0.0753%

Sample Information

Sample Details

Sample ID:200204W001

Batch Number:IT000230

Cultivator / Manufacturer

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Distributor

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Sampling Method: QSP 1265 - Sampling of Cannabis and Product Batches

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Cannabinoid Analysis - Summary

Calculated using Dry-Weight

Sum of Cannabinoids: 36.3842%

Total Cannabinoids: 31.9765%

Total THC: 30.2295%

Total CBD: 0.0753%

Moisture:12.3%

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Dry weight: The weight of a sample after it goes through the drying process.

Pursuant to section § 5724 of California Code of Regulations Title 16 Division 42. Department of Cannabis Control, the equation for moisture correction is:  Dry-weight percent cannabinoid = wet-weight percent cannabinoid / (1 − percent moisture / 100)

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Safety Analysis - Summary

Pesticides: Pass

Mycotoxins: Pass

Heavy Metals: Pass

Microbiology: Pass

Foreign Material: Pass

Water Activity: Pass

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD). Calculated using Dry-Weight.

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total Cannabinoids: 31.9765%

Total THC: 30.2295%

9-THC+0.877*THCa)

Total CBD: 0.0753%

(CBD+0.877*CBDa)

Total CBG: 0.4750%

Total CBG (CBG+0.877*CBGa)

Total THCV: 0.6662%

Total THCV (THCV+0.877*THCVa)

Total CBC: 0.5305%

Total CBC (CBC+0.877*CBCa)

Total CBDV: ND

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

02/06/2020

Result Views

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Compound LOD/LOQ
(mg/g)
Result
(mg/g)
Result
(%)
Tetrahydrocannabinolic Acid (THCa) 0.052 / 0.156 339.794 33.9794
Tetrahydrocannabivarinic Acid (THCVa) 0.088 / 0.267 7.596 0.7596
Cannabichromenic Acid (CBCa) 0.233 / 0.705 6.049 0.6049
Δ9 Tetrahydrocannabinol (Δ9THC) 0.052 / 0.158 4.296 0.4296
Cannabigerolic Acid (CBGa) 0.034 / 0.102 4.046 0.4046
Cannabigerol (CBG) 0.048 / 0.144 1.202 0.1202
Cannabidiolic Acid (CBDa) 0.052 / 0.156 0.859 0.0859
Cannabichromene (CBC) 0.048 / 0.146 ND ND
Cannabidiol (CBD) 0.059 / 0.180 ND ND
Cannabicyclol (CBL) 0.114 / 0.346 ND ND
Cannabinol (CBN) 0.052 / 0.157 ND ND
Cannabidivarin (CBDV) 0.027 / 0.080 ND ND
Tetrahydrocannabivarin (THCV) 0.045 / 0.137 ND ND
Cannabidivarinic Acid (CBDVa) 0.030 / 0.090 ND ND
∆8 Tetrahydrocannabinol (Δ8THC) 0.074 / 0.224 ND ND
SUM OF CANNABINOIDS 363.842 mg/g 36.3842%
Moisture Test Result

12.3% Tested 02/05/2020 Method: QSP 1224 - Loss on Drying (Moisture)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Category 1 Pesticide Test Results

02/06/2020

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Result
(μg/g)
Result
Aldicarb 0.030 / 0.091 ≥ LOD ND Pass
Fipronil 0.029 / 0.089 ≥ LOD ND Pass
Imazalil 0.029 / 0.089 ≥ LOD ND Pass
Propoxur 0.029 / 0.089 ≥ LOD ND Pass
Chlordane* 0.032 / 0.097 ≥ LOD ND Pass
Coumaphos 0.029 / 0.089 ≥ LOD ND Pass
Mevinphos 0.029 / 0.089 ≥ LOD ND Pass
Carbofuran 0.029 / 0.089 ≥ LOD ND Pass
Daminozide 0.030 / 0.091 ≥ LOD ND Pass
Dimethoate 0.029 / 0.089 ≥ LOD ND Pass
Etofenprox 0.029 / 0.089 ≥ LOD ND Pass
Fenoxycarb 0.029 / 0.089 ≥ LOD ND Pass
Methiocarb 0.029 / 0.089 ≥ LOD ND Pass
Ethoprophos 0.029 / 0.089 ≥ LOD ND Pass
Spiroxamine 0.029 / 0.089 ≥ LOD ND Pass
Thiacloprid 0.029 / 0.089 ≥ LOD ND Pass
Chlorfenapyr* 0.030 / 0.090 ≥ LOD ND Pass
Chlorpyrifos 0.029 / 0.089 ≥ LOD ND Pass
Paclobutrazol 0.029 / 0.089 ≥ LOD ND Pass
Parathion-methyl 0.029 / 0.089 ≥ LOD ND Pass
Dichlorvos (DDVP) 0.029 / 0.089 ≥ LOD ND Pass
Category 2 Pesticide Test Results

02/06/2020

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Result
(μg/g)
Result
Naled 0.010 / 0.031 0.1 ND Pass
Captan 0.099 / 0.300 0.7 ND Pass
Oxamyl 0.014 / 0.042 0.5 ND Pass
Phosmet 0.010 / 0.030 0.1 ND Pass
Acephate 0.013 / 0.039 0.1 ND Pass
Boscalid 0.008 / 0.023 0.1 ND Pass
Carbaryl 0.014 / 0.043 0.5 ND Pass
Diazinon 0.009 / 0.027 0.1 ND Pass
Methomyl 0.022 / 0.067 1 ND Pass
Spinosad 0.010 / 0.031 0.1 ND Pass
Abamectin 0.030 / 0.091 0.1 ND Pass
Etoxazole 0.007 / 0.022 0.1 ND Pass
Malathion 0.006 / 0.019 0.5 ND Pass
Metalaxyl 0.011 / 0.033 2 ND Pass
Pyridaben 0.007 / 0.020 0.1 ND Pass
Bifenazate 0.012 / 0.035 0.1 ND Pass
Bifenthrin 0.013 / 0.038 3 ND Pass
Cyfluthrin 0.099 / 0.299 2 ND Pass
Fenhexamid 0.015 / 0.045 0.1 ND Pass
Flonicamid 0.022 / 0.066 0.1 ND Pass
Permethrin 0.027 / 0.082 0.5 ND Pass
Pyrethrins 0.012 / 0.036 0.5 ND Pass
Spinetoram 0.006 / 0.017 0.1 ND Pass
Acequinocyl 0.010 / 0.031 0.1 ND Pass
Acetamiprid 0.013 / 0.038 0.1 ND Pass
Fludioxonil 0.020 / 0.061 0.1 ND Pass
Hexythiazox 0.009 / 0.027 0.1 ND Pass
Prallethrin 0.011 / 0.032 0.1 ND Pass
Azoxystrobin 0.015 / 0.047 0.1 ND Pass
Clofentezine 0.009 / 0.027 0.1 ND Pass
Cypermethrin 0.030 / 0.091 1 ND Pass
Dimethomorph 0.018 / 0.055 2 ND Pass
Imidacloprid 0.017 / 0.050 5 ND Pass
Myclobutanil 0.015 / 0.044 0.1 ND Pass
Spiromesifen 0.005 / 0.015 0.1 ND Pass
Tebuconazole 0.006 / 0.018 0.1 ND Pass
Thiamethoxam 0.011 / 0.033 5 ND Pass
Fenpyroximate 0.012 / 0.036 0.1 ND Pass
Propiconazole 0.004 / 0.013 0.1 ND Pass
Spirotetramat 0.014 / 0.042 0.1 ND Pass
Kresoxim-methyl 0.010 / 0.029 0.1 ND Pass
Trifloxystrobin 0.007 / 0.020 0.1 ND Pass
Piperonyl Butoxide 0.007 / 0.020 3 ND Pass
Chlorantraniliprole 0.020 / 0.061 10 ND Pass
Pentachloronitrobenzene (Quintozene)* 0.020 / 0.061 0.1 ND Pass

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS

Mycotoxin Test Results

02/06/2020

PASS

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Compound LOD/LOQ
(μg/kg)
Action Limit
(μg/kg)
Result
(μg/kg)
Result
Aflatoxin B1 1.0 / 3.0 20 ND Pass
Aflatoxin B2 2.0 / 6.0 20 ND Pass
Aflatoxin G1 1.0 / 3.0 20 ND Pass
Aflatoxin G2 2.0 / 6.0 20 ND Pass
Ochratoxin A 6.0 / 18.0 20 ND Pass
Total Aflatoxin 20 ND Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

02/06/2020

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Result
(μg/g)
Result
Arsenic 0.013 / 0.039 0.2 ND Pass
Cadmium 0.012 / 0.035 0.2 ND Pass
Lead 0.031 / 0.095 0.5 ND Pass
Mercury 0.002 / 0.005 0.1 0.013 Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants

Microbiology Test Results

02/06/2020

PASS

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Compound Action Limit Result Result
Salmonella spp. Not Detected in 1g ND Pass
Aspergillus niger Not Detected in 1g ND Pass
Aspergillus flavus Not Detected in 1g ND Pass
Aspergillus terreus Not Detected in 1g ND Pass
Aspergillus fumigatus Not Detected in 1g ND Pass
Shiga toxin-producing Escherichia coli Not Detected in 1g ND Pass

Visual analysis includes, but is not limited to, sand, soil, cinders, dirt, mold, hair, insect fragments, and mammalian excreta.

Method: QSP 1226 - Analysis of Foreign Material in Cannabis and Cannabis Products

Foreign Material Test Results

02/05/2020

PASS

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Compound Action Limit Result Result
Hair Count > 1 per 3 grams 0.0 Pass
Insect Fragment Count > 1 per 3 grams 0.0 Pass
Mammalian Excreta Count > 1 per 3 grams 0.0 Pass
Total Sample Area Covered by Mold >25% None Pass
Total Sample Area Covered by Sand, Soil, Cinders, or Dirt >25% None Pass
Total Sample Area Covered by an Imbedded Foreign Material >25% None Pass

Method: QSP 1227 - Analysis of Water Activity in Cannabis and Cannabis Products

Water Activity Test Results

02/05/2020

PASS

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Compound Action Limit
(Aw)
Result
(Aw)
Result
Water Activity 0.65 0.4815 Pass

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