Certificate of Analysis
HEMP QUALITY ASSURANCE TEST

Sample Name:

9Leaves Good Sleep Tincture

Infused, Liquid Edible

Date Issued:

07/31/2022

Total THC 34.159 mg/unit
Total CBD 997.396 mg/unit
Sum Cannabinoids 1124.286 mg/unit
Total Cannabinoids 1124.287 mg/unit

Sample Information

Sample Details

Sample ID:220728R020

Batch Number:NLT04S0722

Cultivator / Manufacturer

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Distributor / Tested For

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Cannabinoid Analysis - Summary

Total THC: 34.159 mg/unit

Total CBD: 997.396 mg/unit

Sum of Cannabinoids: 1124.286 mg/unit

Total Cannabinoids: 1124.287 mg/unit

Density:0.9175 g/mL

Total THC/CBD is calculated using the following formulas to take into account the loss of a carboxyl group during the decarboxylation step:
Total THC = Δ9-THC + (THCa (0.877))
Total CBD = CBD + (CBDa (0.877))

Sum of Cannabinoids = Δ9-THC + THCa + CBD + CBDa + CBG + CBGa + THCV + THCVa + CBC + CBCa + CBDV + CBDVa + Δ8-THC + CBL + CBN

Total Cannabinoids = (Δ9-THC+0.877*THCa) + (CBD+0.877*CBDa) + (CBG+0.877*CBGa) + (THCV+0.877*THCVa) + (CBC+0.877*CBCa) + (CBDV+0.877*CBDVa) + Δ8-THC + CBL + CBN

Sum of Cannabinoids: The concentration of each individual cannabinoid added together as they are, without accounting for decarboxylation. This measurement is of particular importance for certain cannabis products that are not intended to be heated prior to application or consumption.

Total Cannabinoids: The concentration of each acidic cannabinoid, multiplied by 0.877 to account for the loss of molecular mass that happens as it is converted to a neutral cannabinoid when heated. Then this calculated concentration is added to the concentrations of the corresponding neutral cannabinoid already present. This corrected data is of particular importance to both producers and consumers of products intended to be heated prior to application or consumption.

Safety Analysis - Summary

Δ9-THC per Unit: Pass

Pesticides: Pass

Mycotoxins: Pass

Residual Solvents: Pass

Heavy Metals: Pass

Microbiology (PCR): Pass

Foreign Material: Pass

View Complete Test Results:

Tested by high-performance liquid chromatography with diode-array detection (HPLC-DAD).

Method: QSP 1157 - Analysis of Cannabinoids by HPLC-DAD

Summary

Total THC: 34.159 mg/unit

9-THC+0.877*THCa)

Total CBD: 997.396 mg/unit

(CBD+0.877*CBDa)

Total Cannabinoids: 1124.287 mg/unit

Total CBG: 43.847 mg/unit

Total CBG (CBG+0.877*CBGa)

Total THCV: ND

Total THCV (THCV+0.877*THCVa)

Total CBC: 42.113 mg/unit

Total CBC (CBC+0.877*CBCa)

Total CBDV: 3.551 mg/unit

Total CBDV (CBDV+0.877*CBDVa)

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Cannabinoid Test Results

07/31/2022

Result Views

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Compound LOD/LOQ
(mg/g)
Measurement
Uncertainty
(mg/g)
Result
(mg/g)
Result
(%)
Cannabidiol (CBD) 0.004 / 0.011 ±1.3516 36.236 3.6236
Cannabigerol (CBG) 0.002 / 0.006 ±0.0773 1.593 0.1593
Cannabichromene (CBC) 0.003 / 0.010 ±0.0493 1.530 0.1530
Δ9 Tetrahydrocannabinol (Δ9THC) 0.002 / 0.014 ±0.0681 1.241 0.1241
Cannabidivarin (CBDV) 0.002 / 0.012 ±0.0053 0.129 0.0129
Cannabinol (CBN) 0.001 / 0.007 ±0.0026 0.089 0.0089
Cannabicyclol (CBL) 0.003 / 0.010 ±0.0010 0.028 0.0028
Cannabichromenic Acid (CBCa) 0.001 / 0.015 N/A ND ND
Cannabidiolic Acid (CBDa) 0.001 / 0.026 N/A ND ND
Cannabigerolic Acid (CBGa) 0.002 / 0.007 N/A ND ND
Tetrahydrocannabivarin (THCV) 0.002 / 0.012 N/A ND ND
Tetrahydrocannabinolic Acid (THCa) 0.001 / 0.005 N/A ND ND
Cannabidivarinic Acid (CBDVa) 0.001 / 0.018 N/A ND ND
Tetrahydrocannabivarinic Acid (THCVa) 0.002 / 0.019 N/A ND ND
∆8 Tetrahydrocannabinol (Δ8THC) 0.01 / 0.02 N/A ND ND
SUM OF CANNABINOIDS 40.846 mg/g 4.0846%
Unit Mass:

27.525 grams

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Δ9-THC per Unit 110 per-package limit 34.159 mg/unit Pass
Total THC per Unit 34.159 mg/unit
CBD per Unit 997.396 mg/unit
Total CBD per Unit 997.396 mg/unit
Sum of Cannabinoids per Unit 1124.286 mg/unit
Total Cannabinoids per Unit 1124.287 mg/unit
Density Test Result

0.9175 g/mL Tested 07/31/2022 Method: QSP 7870 - Sample Preparation

Learn more

The cannabis plant contains dozens of active compounds called cannabinoids. These compounds are the primary contributors to the psychoactive effects of cannabis.

Cannabinoid testing determines the potency of a sample to aid in dosage considerations.

Pesticide and plant growth regulator analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS) or gas chromatography-mass spectrometry (GC-MS).

*GC-MS utilized where indicated.

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS or QSP 1213 - Analysis of Pesticides by GC-MS

Pesticide Test Results

07/30/2022

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Aldicarb 0.03 / 0.08 ≥ LOD N/A ND Pass
Carbofuran 0.02 / 0.05 ≥ LOD N/A ND Pass
Chlordane* 0.03 / 0.08 ≥ LOD N/A ND Pass
Chlorfenapyr* 0.03 / 0.10 ≥ LOD N/A ND Pass
Chlorpyrifos 0.02 / 0.06 ≥ LOD N/A ND Pass
Coumaphos 0.02 / 0.07 ≥ LOD N/A ND Pass
Daminozide 0.02 / 0.07 ≥ LOD N/A ND Pass
Dichlorvos (DDVP) 0.03 / 0.09 ≥ LOD N/A ND Pass
Dimethoate 0.03 / 0.08 ≥ LOD N/A ND Pass
Ethoprophos 0.03 / 0.10 ≥ LOD N/A ND Pass
Etofenprox 0.02 / 0.06 ≥ LOD N/A ND Pass
Fenoxycarb 0.03 / 0.08 ≥ LOD N/A ND Pass
Fipronil 0.03 / 0.08 ≥ LOD N/A ND Pass
Imazalil 0.02 / 0.06 ≥ LOD N/A ND Pass
Methiocarb 0.02 / 0.07 ≥ LOD N/A ND Pass
Mevinphos 0.03 / 0.09 ≥ LOD N/A ND Pass
Paclobutrazol 0.02 / 0.05 ≥ LOD N/A ND Pass
Parathion-methyl 0.03 / 0.10 ≥ LOD N/A ND Pass
Propoxur 0.03 / 0.09 ≥ LOD N/A ND Pass
Spiroxamine 0.03 / 0.08 ≥ LOD N/A ND Pass
Thiacloprid 0.03 / 0.10 ≥ LOD N/A ND Pass
Abamectin 0.03 / 0.10 0.3 N/A ND Pass
Acephate 0.02 / 0.07 5 N/A ND Pass
Acequinocyl 0.02 / 0.07 4 N/A ND Pass
Acetamiprid 0.02 / 0.05 5 N/A ND Pass
Azoxystrobin 0.02 / 0.07 40 N/A ND Pass
Bifenazate 0.01 / 0.04 5 N/A ND Pass
Bifenthrin 0.02 / 0.05 0.5 N/A ND Pass
Boscalid 0.03 / 0.09 10 N/A ND Pass
Captan 0.19 / 0.57 5 N/A ND Pass
Carbaryl 0.02 / 0.06 0.5 N/A ND Pass
Chlorantraniliprole 0.04 / 0.12 40 N/A ND Pass
Clofentezine 0.03 / 0.09 0.5 N/A ND Pass
Cyfluthrin 0.12 / 0.38 1 N/A ND Pass
Cypermethrin 0.11 / 0.32 1 N/A ND Pass
Diazinon 0.02 / 0.05 0.2 N/A ND Pass
Dimethomorph 0.03 / 0.09 20 N/A ND Pass
Etoxazole 0.02 / 0.06 1.5 N/A ND Pass
Fenhexamid 0.03 / 0.09 10 N/A ND Pass
Fenpyroximate 0.02 / 0.06 2 N/A ND Pass
Flonicamid 0.03 / 0.10 2 N/A ND Pass
Fludioxonil 0.03 / 0.10 30 N/A ND Pass
Hexythiazox 0.02 / 0.07 2 N/A ND Pass
Imidacloprid 0.04 / 0.11 3 N/A ND Pass
Kresoxim-methyl 0.02 / 0.07 1 N/A ND Pass
Malathion 0.03 / 0.09 5 N/A ND Pass
Metalaxyl 0.02 / 0.07 15 N/A ND Pass
Methomyl 0.03 / 0.10 0.1 N/A ND Pass
Myclobutanil 0.03 / 0.09 9 N/A ND Pass
Naled 0.02 / 0.07 0.5 N/A ND Pass
Oxamyl 0.04 / 0.11 0.2 N/A ND Pass
Pentachloronitrobenzene (Quintozene)* 0.03 / 0.09 0.2 N/A ND Pass
Permethrin 0.04 / 0.12 20 N/A ND Pass
Phosmet 0.03 / 0.10 0.2 N/A ND Pass
Piperonyl Butoxide 0.02 / 0.07 8 N/A ND Pass
Prallethrin 0.03 / 0.08 0.4 N/A ND Pass
Propiconazole 0.02 / 0.07 20 N/A ND Pass
Pyrethrins 0.04 / 0.12 1 N/A ND Pass
Pyridaben 0.02 / 0.07 3 N/A ND Pass
Spinetoram 0.02 / 0.07 3 N/A ND Pass
Spinosad 0.02 / 0.07 3 N/A ND Pass
Spiromesifen 0.02 / 0.05 12 N/A ND Pass
Spirotetramat 0.02 / 0.06 13 N/A ND Pass
Tebuconazole 0.02 / 0.07 2 N/A ND Pass
Thiamethoxam 0.03 / 0.10 4.5 N/A ND Pass
Trifloxystrobin 0.03 / 0.08 30 N/A ND Pass

Mycotoxin analysis utilizing high-performance liquid chromatography-mass spectrometry (HPLC-MS).

Method: QSP 1212 - Analysis of Pesticides and Mycotoxins by LC-MS

Mycotoxin Test Results

07/30/2022

PASS

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Compound LOD/LOQ
(μg/kg)
Action Limit
(μg/kg)
Measurement
Uncertainty
(μg/kg)
Result
(μg/kg)
Result
Aflatoxin B1 2.0 / 6.0 N/A ND
Aflatoxin B2 1.8 / 5.6 N/A ND
Aflatoxin G1 1.0 / 3.1 N/A ND
Aflatoxin G2 1.2 / 3.5 N/A ND
Ochratoxin A 6.3 / 19.2 20 N/A ND Pass
Total Aflatoxin 20 ± ND Pass

Residual Solvent analysis utilizing gas chromatography-mass spectrometry (GC-MS).

Method: QSP 1204 - Analysis of Residual Solvents by GC-MS

Residual Solvents Test Results

07/31/2022

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
1,2-Dichloroethane 0.05 / 0.1 1 N/A ND Pass
Benzene 0.03 / 0.09 1 N/A ND Pass
Chloroform 0.1 / 0.2 1 N/A ND Pass
Dichloromethane (Methylene Chloride) 0.3 / 0.9 1 N/A ND Pass
Ethylene Oxide 0.3 / 0.8 1 N/A ND Pass
Trichloroethylene 0.1 / 0.3 1 N/A ND Pass
2-Propanol (Isopropyl Alcohol) 10 / 40 5000 N/A ND Pass
Acetone 20 / 50 5000 N/A ND Pass
Acetonitrile 2 / 7 410 N/A ND Pass
Ethanol 20 / 50 5000 ±18.6 642 Pass
Ethyl Acetate 20 / 60 5000 N/A <LOQ Pass
Ethyl Ether 20 / 50 5000 N/A ND Pass
Methanol 50 / 200 3000 N/A ND Pass
n-Butane 10 / 50 5000 N/A ND Pass
n-Heptane 20 / 60 5000 N/A ND Pass
n-Hexane 2 / 5 290 N/A ND Pass
n-Pentane 20 / 50 5000 N/A ND Pass
Propane 10 / 20 5000 N/A ND Pass
Toluene 7 / 21 890 N/A ND Pass
Total Xylenes 50 / 160 2170 N/A ND Pass

Heavy metal analysis utilizing inductively coupled plasma-mass spectrometry (ICP-MS).

Method: QSP 1160 - Analysis of Heavy Metals by ICP-MS

Heavy Metals Test Results

07/29/2022

PASS

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Compound LOD/LOQ
(μg/g)
Action Limit
(μg/g)
Measurement
Uncertainty
(μg/g)
Result
(μg/g)
Result
Arsenic 0.02 / 0.1 1.5 N/A ND Pass
Cadmium 0.02 / 0.05 0.5 N/A ND Pass
Lead 0.04 / 0.1 0.5 N/A ND Pass
Mercury 0.002 / 0.01 3 N/A ND Pass

Analysis conducted by polymerase chain reaction (PCR) and fluorescence detection of microbiological contaminants.

Method: QSP 1221 - Analysis of Microbiological Contaminants

Microbiology Test Results (PCR)

07/30/2022

PASS

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Compound Action Limit Result Result
Salmonella spp. Not Detected in 1g ND Pass
Listeria monocytogenes ND
Shiga toxin-producing Escherichia coli Not Detected in 1g ND Pass

Visual analysis includes, but is not limited to, sand, soil, cinders, dirt, mold, hair, insect fragments, and mammalian excreta.

Method: QSP 1226 - Analysis of Foreign Material in Cannabis and Cannabis Products

Foreign Material Test Results

07/29/2022

PASS

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Compound Action Limit Result Result
Hair Count > 1 per 3 grams 0.0 Pass
Insect Fragment Count > 1 per 3 grams 0.0 Pass
Mammalian Excreta Count > 1 per 3 grams 0.0 Pass
Total Sample Area Covered by Mold >25% None Pass
Total Sample Area Covered by Sand, Soil, Cinders, or Dirt >25% None Pass
Total Sample Area Covered by an Imbedded Foreign Material >25% None Pass

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